DE19632925A1 - Reaktionsfähige Massen mit hoher Topfzeit - Google Patents
Reaktionsfähige Massen mit hoher TopfzeitInfo
- Publication number
- DE19632925A1 DE19632925A1 DE19632925A DE19632925A DE19632925A1 DE 19632925 A1 DE19632925 A1 DE 19632925A1 DE 19632925 A DE19632925 A DE 19632925A DE 19632925 A DE19632925 A DE 19632925A DE 19632925 A1 DE19632925 A1 DE 19632925A1
- Authority
- DE
- Germany
- Prior art keywords
- nco
- weight
- compositions according
- prepolymer
- reactive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
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- 150000001875 compounds Chemical class 0.000 claims description 23
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- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 17
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- 125000001931 aliphatic group Chemical group 0.000 claims description 8
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- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 description 4
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 4
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 4
- HGQSXVKHVMGQRG-UHFFFAOYSA-N dioctyltin Chemical compound CCCCCCCC[Sn]CCCCCCCC HGQSXVKHVMGQRG-UHFFFAOYSA-N 0.000 description 4
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- 238000000034 method Methods 0.000 description 4
- 239000000178 monomer Substances 0.000 description 4
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- 229910052718 tin Inorganic materials 0.000 description 4
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 4
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- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- SJRJJKPEHAURKC-UHFFFAOYSA-N N-Methylmorpholine Chemical compound CN1CCOCC1 SJRJJKPEHAURKC-UHFFFAOYSA-N 0.000 description 3
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000012190 activator Substances 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 3
- 239000012975 dibutyltin dilaurate Substances 0.000 description 3
- 125000005442 diisocyanate group Chemical group 0.000 description 3
- PWEVMPIIOJUPRI-UHFFFAOYSA-N dimethyltin Chemical compound C[Sn]C PWEVMPIIOJUPRI-UHFFFAOYSA-N 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 3
- 239000000543 intermediate Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
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- 235000013772 propylene glycol Nutrition 0.000 description 3
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- ARXKVVRQIIOZGF-UHFFFAOYSA-N 1,2,4-butanetriol Chemical compound OCCC(O)CO ARXKVVRQIIOZGF-UHFFFAOYSA-N 0.000 description 2
- IUYYVMKHUXDWEU-UHFFFAOYSA-N 2,2,4-trimethylpentane-1,1-diol Chemical compound CC(C)CC(C)(C)C(O)O IUYYVMKHUXDWEU-UHFFFAOYSA-N 0.000 description 2
- BWZVCCNYKMEVEX-UHFFFAOYSA-N 2,4,6-Trimethylpyridine Chemical compound CC1=CC(C)=NC(C)=C1 BWZVCCNYKMEVEX-UHFFFAOYSA-N 0.000 description 2
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- NIAAGQAEVGMHPM-UHFFFAOYSA-N 4-methylbenzene-1,2-dithiol Chemical compound CC1=CC=C(S)C(S)=C1 NIAAGQAEVGMHPM-UHFFFAOYSA-N 0.000 description 2
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- KOUKXHPPRFNWPP-UHFFFAOYSA-N pyrazine-2,5-dicarboxylic acid;hydrate Chemical compound O.OC(=O)C1=CN=C(C(O)=O)C=N1 KOUKXHPPRFNWPP-UHFFFAOYSA-N 0.000 description 1
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- CRHIAMBJMSSNNM-UHFFFAOYSA-N tetraphenylstannane Chemical compound C1=CC=CC=C1[Sn](C=1C=CC=CC=1)(C=1C=CC=CC=1)C1=CC=CC=C1 CRHIAMBJMSSNNM-UHFFFAOYSA-N 0.000 description 1
- 125000003396 thiol group Chemical group [H]S* 0.000 description 1
- NBOMNTLFRHMDEZ-UHFFFAOYSA-N thiosalicylic acid Chemical compound OC(=O)C1=CC=CC=C1S NBOMNTLFRHMDEZ-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
- D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
- C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4804—Two or more polyethers of different physical or chemical nature
- C08G18/4812—Mixtures of polyetherdiols with polyetherpolyols having at least three hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6603—Compounds of groups C08G18/42, C08G18/48, or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
- C08G18/6607—Compounds of groups C08G18/42, C08G18/48, or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6666—Compounds of group C08G18/48 or C08G18/52
- C08G18/667—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
- C08G18/6674—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
- C08G18/6677—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203 having at least three hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19632925A DE19632925A1 (de) | 1996-08-16 | 1996-08-16 | Reaktionsfähige Massen mit hoher Topfzeit |
| ES97113456T ES2210431T3 (es) | 1996-08-16 | 1997-08-05 | Uso de masas reactivas con una vida util prolongada. |
| EP97113456A EP0825209B1 (de) | 1996-08-16 | 1997-08-05 | Verwendung reaktionsfähiger Massen mit langer Topfzeit |
| DE59710942T DE59710942D1 (de) | 1996-08-16 | 1997-08-05 | Verwendung reaktionsfähiger Massen mit langer Topfzeit |
| US08/908,655 US6624282B2 (en) | 1996-08-16 | 1997-08-07 | Reactive compositions with an extended pot life |
| JP9230467A JPH1087772A (ja) | 1996-08-16 | 1997-08-13 | 長期可使時間を有する反応性組成物 |
| CA002212900A CA2212900C (en) | 1996-08-16 | 1997-08-13 | Reactive compositions with an extended pot life |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19632925A DE19632925A1 (de) | 1996-08-16 | 1996-08-16 | Reaktionsfähige Massen mit hoher Topfzeit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE19632925A1 true DE19632925A1 (de) | 1998-02-19 |
Family
ID=7802718
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19632925A Withdrawn DE19632925A1 (de) | 1996-08-16 | 1996-08-16 | Reaktionsfähige Massen mit hoher Topfzeit |
| DE59710942T Expired - Lifetime DE59710942D1 (de) | 1996-08-16 | 1997-08-05 | Verwendung reaktionsfähiger Massen mit langer Topfzeit |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE59710942T Expired - Lifetime DE59710942D1 (de) | 1996-08-16 | 1997-08-05 | Verwendung reaktionsfähiger Massen mit langer Topfzeit |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6624282B2 (enExample) |
| EP (1) | EP0825209B1 (enExample) |
| JP (1) | JPH1087772A (enExample) |
| CA (1) | CA2212900C (enExample) |
| DE (2) | DE19632925A1 (enExample) |
| ES (1) | ES2210431T3 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000014138A1 (de) * | 1998-09-04 | 2000-03-16 | Bayer Aktiengesellschaft | Reaktivbindemittel mit verlängerter topfzeit |
| EP2236662A1 (de) * | 2009-03-26 | 2010-10-06 | Benecke-Kaliko AG | Polymermischung, enthaltend ein Isocyanat-Präpolymer |
| EP3628694A1 (de) | 2018-09-26 | 2020-04-01 | Covestro Deutschland AG | Lösemittelarme beschichtungssysteme für textilien |
| WO2020156937A1 (de) | 2019-01-29 | 2020-08-06 | Covestro Intellectual Property Gmbh & Co. Kg | Isocyanatterminierte präpolymere für textilbeschichtungen |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10009407A1 (de) | 2000-02-28 | 2001-08-30 | Bayer Ag | Polyurethan-Beschichtungen |
| DE10131463A1 (de) * | 2001-06-29 | 2003-01-09 | Bayer Ag | Hitzehärtbare Zwei-Komponenten-Beschichtungssysteme |
| US20100267892A1 (en) * | 2007-11-13 | 2010-10-21 | Patrick Henry Corcoran | Isocyanate terminated polytrimethylene ether polyol and process for making same |
| JP5330871B2 (ja) * | 2009-03-17 | 2013-10-30 | 株式会社ポリシス | ポリウレタン樹脂組成物及びポリウレタン成型体の製造方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1534536A (fr) * | 1966-08-22 | 1968-07-26 | Ici Ltd | Production d'élastomères synthétiques |
| US3945981A (en) * | 1974-11-08 | 1976-03-23 | Uniroyal, Inc. | Light stable polyurethane elastomer prepared from aliphatic isocyanate using thio tin organic compound containing sulfur attached to tin as heat activated catalyst |
| GB1535783A (en) | 1975-02-10 | 1978-12-13 | Interox Chemicals Ltd | Preparation of urethane polymers |
| US4119594A (en) | 1977-05-31 | 1978-10-10 | General Motors Corporation | Catalyzed one-shot system for molding thermoset polyurethanes |
| DE2902090A1 (de) | 1979-01-19 | 1980-07-24 | Bayer Ag | Hitzehaertbare beschichtungsmassen und verfahren zur beschichtung von substraten |
| DE3120596A1 (de) | 1981-05-23 | 1982-12-23 | Bayer Ag, 5090 Leverkusen | Loesungsmittelarme, hitzehaertbare polyurethan-reaktivbeschichtungsmasse, verfahren zu ihrer herstellung und ihre verwendung in direkt- und umkehr-beschichtungsverfahren |
| FR2577935B1 (fr) * | 1985-02-26 | 1988-06-17 | Saint Gobain Vitrage | Couche adhesive a base de polyurethane et son utilisation dans les vitrages feuilletes |
| DE3930523A1 (de) * | 1989-09-13 | 1991-03-21 | Bayer Ag | Polyurethanelastomere mit geringer haerte |
| TW264487B (enExample) * | 1992-02-18 | 1995-12-01 | Takeda Pharm Industry Co Ltd | |
| US5175230A (en) * | 1992-03-27 | 1992-12-29 | Air Products And Chemicals, Inc. | Alkyl substituted difunctional cyclohexylisocyanates |
-
1996
- 1996-08-16 DE DE19632925A patent/DE19632925A1/de not_active Withdrawn
-
1997
- 1997-08-05 DE DE59710942T patent/DE59710942D1/de not_active Expired - Lifetime
- 1997-08-05 EP EP97113456A patent/EP0825209B1/de not_active Expired - Lifetime
- 1997-08-05 ES ES97113456T patent/ES2210431T3/es not_active Expired - Lifetime
- 1997-08-07 US US08/908,655 patent/US6624282B2/en not_active Expired - Fee Related
- 1997-08-13 JP JP9230467A patent/JPH1087772A/ja active Pending
- 1997-08-13 CA CA002212900A patent/CA2212900C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000014138A1 (de) * | 1998-09-04 | 2000-03-16 | Bayer Aktiengesellschaft | Reaktivbindemittel mit verlängerter topfzeit |
| US6548615B1 (en) | 1998-09-04 | 2003-04-15 | Bayer Aktiengesellschaft | Reactive binding agent with an extended pot life |
| EP2236662A1 (de) * | 2009-03-26 | 2010-10-06 | Benecke-Kaliko AG | Polymermischung, enthaltend ein Isocyanat-Präpolymer |
| EP3628694A1 (de) | 2018-09-26 | 2020-04-01 | Covestro Deutschland AG | Lösemittelarme beschichtungssysteme für textilien |
| WO2020064631A1 (de) | 2018-09-26 | 2020-04-02 | Covestro Deutschland Ag | Lösemittelarme beschichtungssysteme für textilien |
| WO2020156937A1 (de) | 2019-01-29 | 2020-08-06 | Covestro Intellectual Property Gmbh & Co. Kg | Isocyanatterminierte präpolymere für textilbeschichtungen |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0825209A1 (de) | 1998-02-25 |
| EP0825209B1 (de) | 2003-11-05 |
| CA2212900C (en) | 2008-01-22 |
| US20020177682A1 (en) | 2002-11-28 |
| ES2210431T3 (es) | 2004-07-01 |
| DE59710942D1 (de) | 2003-12-11 |
| US6624282B2 (en) | 2003-09-23 |
| JPH1087772A (ja) | 1998-04-07 |
| CA2212900A1 (en) | 1998-02-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee |