DE1570989B1 - Verfahren zur Wiedergewinnung von Acrylnitril und einem oder mehreren anderen Vinylmonomeren aus einer durch Polymerisation erhaltenen Aufschlaemmung - Google Patents

Verfahren zur Wiedergewinnung von Acrylnitril und einem oder mehreren anderen Vinylmonomeren aus einer durch Polymerisation erhaltenen Aufschlaemmung

Info

Publication number
DE1570989B1
DE1570989B1 DE1965M0066336 DEM0066336A DE1570989B1 DE 1570989 B1 DE1570989 B1 DE 1570989B1 DE 1965M0066336 DE1965M0066336 DE 1965M0066336 DE M0066336 A DEM0066336 A DE M0066336A DE 1570989 B1 DE1570989 B1 DE 1570989B1
Authority
DE
Germany
Prior art keywords
acrylonitrile
monomers
polymerization
slurry
steam
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE1965M0066336
Other languages
German (de)
English (en)
Inventor
Eberhardt Wayne Richard
Cheape Jun Dudley Willis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Co
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of DE1570989B1 publication Critical patent/DE1570989B1/de
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C08F6/003—Removal of residual monomers by physical means from polymer solutions, suspensions, dispersions or emulsions without recovery of the polymer therefrom
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/14—Treatment of polymer emulsions
    • C08F6/16—Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/0077—Baffles attached to the reactor wall inclined

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE1965M0066336 1964-08-24 1965-08-16 Verfahren zur Wiedergewinnung von Acrylnitril und einem oder mehreren anderen Vinylmonomeren aus einer durch Polymerisation erhaltenen Aufschlaemmung Ceased DE1570989B1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US39168964A 1964-08-24 1964-08-24

Publications (1)

Publication Number Publication Date
DE1570989B1 true DE1570989B1 (de) 1977-08-04

Family

ID=23547564

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1965M0066336 Ceased DE1570989B1 (de) 1964-08-24 1965-08-16 Verfahren zur Wiedergewinnung von Acrylnitril und einem oder mehreren anderen Vinylmonomeren aus einer durch Polymerisation erhaltenen Aufschlaemmung

Country Status (8)

Country Link
US (1) US3454542A (enExample)
BE (1) BE668280A (enExample)
CH (1) CH465878A (enExample)
DE (1) DE1570989B1 (enExample)
GB (1) GB1105185A (enExample)
IL (1) IL24053A (enExample)
LU (1) LU49327A1 (enExample)
NL (2) NL6510965A (enExample)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT990993B (it) * 1973-07-06 1975-07-10 Sir Soc Italiana Resine Spa Perfezionamenti nei procedimenti per la preparazione di polimeri o copolimeri dell acrilonitrile
DE2420471B2 (de) * 1974-04-27 1979-01-25 Bayer Ag, 5090 Leverkusen Verfahren zur Abtrennung und Rückgewinnung von Restmonomeren aus wäßrigen Dispersionen von Acrylnitrilpolymerisaten
FR2291987A1 (fr) * 1974-11-25 1976-06-18 Solvay Procede pour l'elimination des residus de monomere dans les polymeres de l'acrylonitrile
US3926927A (en) * 1974-11-25 1975-12-16 Monsanto Co Stripping monomers from a slurry of copolymerized acrylonitrile
DE2521780C2 (de) * 1975-05-16 1982-10-21 Hoechst Ag, 6000 Frankfurt Verfahren zur kontinuierlichen Entfernung von Monomeren aus einer wäßrigen Dispersion eines Polymeren
FR2397429A1 (fr) * 1977-07-13 1979-02-09 Charbonnages Ste Chimique Procede pour purifier des gaz de recirculation de particules condensees de polymere
US4147859A (en) * 1977-10-11 1979-04-03 The B. F. Goodrich Company Process for removal of chloroform and carbon tetrachloride from chlorinated polyvinyl chloride
US4153787A (en) * 1978-03-23 1979-05-08 Monsanto Company Method for removing unreacted monomers from a slurry
US4193903A (en) * 1978-05-17 1980-03-18 Standard Oil Company Rapid removal of residual monomers from acrylonitrile copolymers
US5430127A (en) * 1993-11-02 1995-07-04 National Starch And Chemical Investment Holding Corporation Process for minimizing residual monomers
KR20000015969A (ko) * 1996-05-24 2000-03-25 스타르크, 카르크 분산액 탈취용 칼럼 및 방법
JP4330253B2 (ja) * 2000-06-29 2009-09-16 株式会社クラレ エチレン−酢酸ビニル共重合体およびそのケン化物の製造方法
DE10237061A1 (de) * 2002-08-09 2004-02-19 Basf Ag Verfahren zur Reinigung von Apparaten, in welchen(Meth)acrylsäure enthaltende organische Lösungsmittel behandelt und/oder erzeugt wurden
CN106317296B (zh) * 2015-06-18 2018-07-06 中国石油化工股份有限公司 用于干法腈纶的单体回收工艺
EP4029585A4 (en) * 2019-09-09 2023-10-25 Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences PROCESS FOR REMOVING POLYMERIC IMPURITIES BASED ON STEAM DISTILLATION
CN111895722B (zh) * 2020-09-04 2024-03-01 江西智联塑化科技有限公司 一种用于季戊四醇硬脂酸脂制备的导热油降温装置
KR102782581B1 (ko) * 2020-10-05 2025-03-14 주식회사 엘지화학 스트리핑 장치 및 스트리핑 방법

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3002958A (en) * 1958-07-30 1961-10-03 Du Pont Process for polymerizing monomeric mixtures
FR1362947A (fr) * 1962-07-11 1964-06-05 Asahi Chemical Ind Perfectionnements apportés aux procédés pour la récupération de monomère d'acrylonitrile ou analogues

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2462013A (en) * 1942-11-07 1949-02-15 Standard Oil Dev Co Stripping of emulsion polymerization latcies
US2556851A (en) * 1948-09-10 1951-06-12 Standard Oil Dev Co Use of recycle aqueous acrylonitrile condensate in butadiene-1,3 emulsion polymerization
US2807573A (en) * 1954-04-28 1957-09-24 Escambia Chem Corp Purification of acrylonitrile by extractive distillation
US3153024A (en) * 1959-12-23 1964-10-13 Monsanto Co Shortstopping agents for vinyl polymerizations
US3084143A (en) * 1960-05-02 1963-04-02 Monsanto Chemicals Vinyl polymerization shortstopping process
US3192189A (en) * 1961-09-21 1965-06-29 American Cyanamid Co Method for recovering monomeric materials by a stripping operation in the presence of a chloroxy salt

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3002958A (en) * 1958-07-30 1961-10-03 Du Pont Process for polymerizing monomeric mixtures
FR1362947A (fr) * 1962-07-11 1964-06-05 Asahi Chemical Ind Perfectionnements apportés aux procédés pour la récupération de monomère d'acrylonitrile ou analogues

Also Published As

Publication number Publication date
GB1105185A (en) 1968-03-06
LU49327A1 (enExample) 1966-02-17
BE668280A (enExample) 1966-02-14
CH465878A (fr) 1968-11-30
US3454542A (en) 1969-07-08
NL129660C (enExample)
NL6510965A (enExample) 1966-02-25
IL24053A (en) 1969-03-27

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