DE1568867C3 - Verfahren zum Auskristallisieren von p-Xylol - Google Patents

Verfahren zum Auskristallisieren von p-Xylol

Info

Publication number
DE1568867C3
DE1568867C3 DE1568867A DE1568867A DE1568867C3 DE 1568867 C3 DE1568867 C3 DE 1568867C3 DE 1568867 A DE1568867 A DE 1568867A DE 1568867 A DE1568867 A DE 1568867A DE 1568867 C3 DE1568867 C3 DE 1568867C3
Authority
DE
Germany
Prior art keywords
cooling
xylene
coolant
liquid
finger
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE1568867A
Other languages
German (de)
English (en)
Other versions
DE1568867A1 (de
Inventor
Jerzy Konrad Williamson John Skrebowski
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Publication of DE1568867A1 publication Critical patent/DE1568867A1/de
Application granted granted Critical
Publication of DE1568867C3 publication Critical patent/DE1568867C3/de
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0013Crystallisation cooling by heat exchange by indirect heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/005Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/30Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using agents to prevent the granules sticking together; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/14Purification; Separation; Use of additives by crystallisation; Purification or separation of the crystals
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S585/00Chemistry of hydrocarbon compounds
    • Y10S585/949Miscellaneous considerations
    • Y10S585/95Prevention or removal of corrosion or solid deposits
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S585/00Chemistry of hydrocarbon compounds
    • Y10S585/949Miscellaneous considerations
    • Y10S585/953Pulsed, sonic, or plasma process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DE1568867A 1965-08-18 1966-08-18 Verfahren zum Auskristallisieren von p-Xylol Expired DE1568867C3 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB35367/65A GB1104508A (en) 1965-08-18 1965-08-18 Refrigeration processes
GB918766 1966-03-02
GB2922666 1966-06-29

Publications (2)

Publication Number Publication Date
DE1568867A1 DE1568867A1 (de) 1970-04-02
DE1568867C3 true DE1568867C3 (de) 1974-07-04

Family

ID=27255327

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1568867A Expired DE1568867C3 (de) 1965-08-18 1966-08-18 Verfahren zum Auskristallisieren von p-Xylol

Country Status (5)

Country Link
US (1) US3513212A (US07368563-20080506-C00056.png)
BE (1) BE685705A (US07368563-20080506-C00056.png)
DE (1) DE1568867C3 (US07368563-20080506-C00056.png)
GB (1) GB1104508A (US07368563-20080506-C00056.png)
NL (1) NL6611631A (US07368563-20080506-C00056.png)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110433523A (zh) * 2019-09-02 2019-11-12 齐鲁师范学院 基于声波干预的硫酸铜结晶方法

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1326903A (en) * 1970-10-21 1973-08-15 Atomic Energy Authority Uk Crystallisation methods and apparatus therefor
US4704873A (en) * 1985-11-14 1987-11-10 Taiyo Sanso Co., Ltd. Method and apparatus for producing microfine frozen particles
DE4410347A1 (de) * 1994-03-25 1995-09-28 Rene Leutwyler Verfahren zum Entfernen von anorganischen Metallverbindungen aus Lösungen
DE4431872C1 (de) * 1994-09-07 1996-01-11 Santrade Ltd Anwendung von Ultraschall bei der Verfestigung von Schmelzen oder übersättigten Lösungen auf Förderbändern oder Aufnahmetrommeln
EP1033357A1 (en) * 1999-03-02 2000-09-06 Aerospace Propulsion Products B.V. Process for the production of crystalline energetic materials
FI127136B (en) 2016-11-22 2017-12-15 Lappeenrannan Teknillinen Yliopisto Ultrasonic crystallization device and ultrasonic crystallization system

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2514797A (en) * 1946-01-24 1950-07-11 Raytheon Mfg Co Heat exchanger
NL75853C (US07368563-20080506-C00056.png) * 1949-08-12
US2614134A (en) * 1950-06-21 1952-10-14 Standard Oil Dev Co Purification of crystalline substances
US2769852A (en) * 1953-04-01 1956-11-06 California Research Corp Separation of xylene isomers by fractional crystallization
US2816938A (en) * 1954-06-18 1957-12-17 Texas Co Fractional crystallization under pressure
US2794840A (en) * 1955-02-07 1957-06-04 Phillips Petroleum Co Fractional crystallization process and apparatus
US2815364A (en) * 1955-02-21 1957-12-03 Phillips Petroleum Co Fractional crystallization process and apparatus
BE550451A (US07368563-20080506-C00056.png) * 1955-08-22
US2846292A (en) * 1955-08-23 1958-08-05 Sun Oil Co Continuous crystallization apparatus
US3266263A (en) * 1962-06-11 1966-08-16 Phillips Petroleum Co Concentration of aqueous solutions by crystallization with sonic defoaming
US3395547A (en) * 1962-06-28 1968-08-06 Phillips Petroleum Co Fractional crystallization system
US3261170A (en) * 1963-05-10 1966-07-19 Phillips Petroleum Co Multi-stage crystallization process and apparatus
NL6507068A (US07368563-20080506-C00056.png) * 1964-06-10 1965-12-13

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110433523A (zh) * 2019-09-02 2019-11-12 齐鲁师范学院 基于声波干预的硫酸铜结晶方法

Also Published As

Publication number Publication date
US3513212A (en) 1970-05-19
BE685705A (US07368563-20080506-C00056.png) 1967-02-20
DE1568867A1 (de) 1970-04-02
GB1104508A (en) 1968-02-28
NL6611631A (US07368563-20080506-C00056.png) 1967-02-20

Similar Documents

Publication Publication Date Title
DE840098C (de) Verfahren und Vorrichtung zur Verbesserung des Waermeaustauschs
DE1568867C3 (de) Verfahren zum Auskristallisieren von p-Xylol
EP0218545B1 (de) Kristallisationsvorrichtung und deren Verwendung
DE1285983B (de) Kuehlungskristallisator
DE2935701A1 (de) Vorrichtung zum abkratzen von ablagerungen von der innenflaeche langer rohre
DE3486375T2 (de) Wärmepumpe.
DE69413688T2 (de) Wärmeübertragungsgerät mit direkt angetriebenem, umlaufendem schlagstab
DE19717397A1 (de) Gerät zur Einkopplung von Ultraschall in ein flüssiges oder pastöses Medium
DE1568867B (de) Verfahren zum Ausknstallisieren von p Xylol
EP2341119B1 (de) Verfahren und Vorrichtung zum Temperieren einer exothermen Reaktion
DE2321804C3 (de) Vorrichtung zum Waschen von Eiskristallen durch direkten Kontakt mit einem Kühlmittel
DE19707635A1 (de) Vorrichtung zum Erzeugen einer wässrigen Suspension aus kleinen Eiskristallen
DE503594C (de) Vorrichtung zum Auskristallisieren von festen Stoffen aus in eine umlaufende Bewegung versetzten Loesungen
US3335575A (en) Freeze concentration process
DE19714665C1 (de) Vorrichtung zur Beseitigung und Verhinderung von Ablagerungen mit Ultraschallwellen in flüssigen Medien
DE102013208094B4 (de) Verfahren und Vorrichtung zur Herstellung von Eisbrei
DE2804431A1 (de) Waermetauscher fuer mit feststoffen durchsetzte fluessigkeiten
DE1086211B (de) Vorrichtung und Verfahren zum Kristallisieren
DE1286507B (de) Verfahren zum Konzentrieren eines aus mehreren Bestandteilen bestehenden fluessigen Materials
DE2165346B2 (de) Kühlvorrichtung
DE1619772A1 (de) Kuehlverfahren
DE1943625A1 (de) Vorrichtung und Verfahren zur Kuehlung einer Fluessigkeit
DE199732C (US07368563-20080506-C00056.png)
DE69727791T2 (de) Vorrichtung zur Elektroplattierung eines Tiefdruckzylinders unter Verwendung von Ultraschallenergie
DE841744C (de) Kristallisationsverfahren

Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)
E77 Valid patent as to the heymanns-index 1977
EHJ Ceased/non-payment of the annual fee