DE136097C - - Google Patents

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Publication number

DE136097C

DE136097C DENDAT136097D DE136097DA DE136097C DE 136097 C DE136097 C DE 136097C DE NDAT136097 D DENDAT136097 D DE NDAT136097D DE 136097D A DE136097D A DE 136097DA DE 136097 C DE136097 C DE 136097C

Authority

DE

Germany

Prior art keywords

blue

green

diamidoanthraquinone

diamidoanthraquinones

crude

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• 238000000034 method Methods 0.000 claims description 7
• WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 2
• GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 2
• 229910052794 bromium Inorganic materials 0.000 claims description 2
• 238000007792 addition Methods 0.000 claims 1
• 125000001309 chloro group Chemical class Cl* 0.000 claims 1
• 150000002366 halogen compounds Chemical class 0.000 claims 1
• 238000012986 modification Methods 0.000 claims 1
• 230000004048 modification Effects 0.000 claims 1
• 239000000975 dye Substances 0.000 description 10
• PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 8
• RZXMPPFPUUCRFN-UHFFFAOYSA-N p-toluidine Chemical compound CC1=CC=C(N)C=C1 RZXMPPFPUUCRFN-UHFFFAOYSA-N 0.000 description 8
• CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 5
• 244000172533 Viola sororia Species 0.000 description 5
• VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
• AFBPFSWMIHJQDM-UHFFFAOYSA-N N-methyl-N-phenylamine Natural products CNC1=CC=CC=C1 AFBPFSWMIHJQDM-UHFFFAOYSA-N 0.000 description 4
• 150000004982 aromatic amines Chemical class 0.000 description 3
• 239000007859 condensation product Substances 0.000 description 3
• 239000000155 melt Substances 0.000 description 3
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
• 238000001816 cooling Methods 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
• VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
• 241000394591 Hybanthus Species 0.000 description 1
• 244000061775 Olea africana Species 0.000 description 1
• 235000002852 Olea africana Nutrition 0.000 description 1
• 240000007817 Olea europaea Species 0.000 description 1
• 239000002253 acid Substances 0.000 description 1
• IQOSMFFCVGASLF-UHFFFAOYSA-N aniline nitrobenzene Chemical compound NC1=CC=CC=C1.NC1=CC=CC=C1.[N+](=O)([O-])C1=CC=CC=C1 IQOSMFFCVGASLF-UHFFFAOYSA-N 0.000 description 1
• CEVLPYIIUNVBAT-UHFFFAOYSA-N anthracene-9,10-dione;hydron;bromide Chemical compound Br.C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 CEVLPYIIUNVBAT-UHFFFAOYSA-N 0.000 description 1
• 150000001454 anthracenes Chemical class 0.000 description 1
• PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 1
• 150000004056 anthraquinones Chemical class 0.000 description 1
• 229910052796 boron Inorganic materials 0.000 description 1
• 230000031709 bromination Effects 0.000 description 1
• 238000005893 bromination reaction Methods 0.000 description 1
• 239000003795 chemical substances by application Substances 0.000 description 1
• 150000001804 chlorine Chemical class 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 229910052736 halogen Inorganic materials 0.000 description 1
• 150000002367 halogens Chemical class 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 238000006396 nitration reaction Methods 0.000 description 1
• 239000000049 pigment Substances 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• ORFSSYGWXNGVFB-UHFFFAOYSA-N sodium 4-amino-6-[[4-[4-[(8-amino-1-hydroxy-5,7-disulfonaphthalen-2-yl)diazenyl]-3-methoxyphenyl]-2-methoxyphenyl]diazenyl]-5-hydroxynaphthalene-1,3-disulfonic acid Chemical compound COC1=C(C=CC(=C1)C2=CC(=C(C=C2)N=NC3=C(C4=C(C=C3)C(=CC(=C4N)S(=O)(=O)O)S(=O)(=O)O)O)OC)N=NC5=C(C6=C(C=C5)C(=CC(=C6N)S(=O)(=O)O)S(=O)(=O)O)O.[Na+] ORFSSYGWXNGVFB-UHFFFAOYSA-N 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 150000003460 sulfonic acids Chemical class 0.000 description 1
• 229950003937 tolonium Drugs 0.000 description 1
• 210000002268 wool Anatomy 0.000 description 1
• 238000010626 work up procedure Methods 0.000 description 1