DE10308111A1 - Verfahren zum Abtrennen von gelösten oder kolloidalen Feststoffen aus nicht wässrigen Lösungen - Google Patents

Verfahren zum Abtrennen von gelösten oder kolloidalen Feststoffen aus nicht wässrigen Lösungen Download PDF

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Publication number
DE10308111A1
DE10308111A1 DE10308111A DE10308111A DE10308111A1 DE 10308111 A1 DE10308111 A1 DE 10308111A1 DE 10308111 A DE10308111 A DE 10308111A DE 10308111 A DE10308111 A DE 10308111A DE 10308111 A1 DE10308111 A1 DE 10308111A1
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DE
Germany
Prior art keywords
membrane
complex compounds
flow
catalyst
dissolved
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE10308111A
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German (de)
English (en)
Inventor
Gregor Dr. Dudziak
Andreas Nickel
Kerstin Baumarth
Martina Mutter
Olaf Dr. Stange
Rafael Warsitz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer Technology Services GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Technology Services GmbH filed Critical Bayer Technology Services GmbH
Priority to DE10308111A priority Critical patent/DE10308111A1/de
Priority to US10/774,778 priority patent/US20040168981A1/en
Priority to JP2006501848A priority patent/JP2006519093A/ja
Priority to PCT/EP2004/001419 priority patent/WO2004076039A1/de
Priority to EP04710858A priority patent/EP1599275A1/de
Publication of DE10308111A1 publication Critical patent/DE10308111A1/de
Withdrawn legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4061—Regeneration or reactivation of catalysts containing metals involving membrane separation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/027—Nanofiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/024—Oxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
    • B01J31/2419—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member
    • B01J31/2428—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member with more than one complexing phosphine-P atom
    • B01J31/2433—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member with more than one complexing phosphine-P atom comprising aliphatic or saturated rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
    • B01J31/2442—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems
    • B01J31/2447—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems and phosphine-P atoms as substituents on a ring of the condensed system or on a further attached ring
    • B01J31/2452—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems and phosphine-P atoms as substituents on a ring of the condensed system or on a further attached ring with more than one complexing phosphine-P atom
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4023—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper
    • B01J31/4038—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4023—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper
    • B01J31/4038—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing noble metals
    • B01J31/4046—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing noble metals containing rhodium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/02—Details relating to pores or porosity of the membranes
    • B01D2325/022—Asymmetric membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/02—Details relating to pores or porosity of the membranes
    • B01D2325/0283—Pore size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/38—Hydrophobic membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/02—Compositional aspects of complexes used, e.g. polynuclearity
    • B01J2531/0261—Complexes comprising ligands with non-tetrahedral chirality
    • B01J2531/0266—Axially chiral or atropisomeric ligands, e.g. bulky biaryls such as donor-substituted binaphthalenes, e.g. "BINAP" or "BINOL"
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/70—Complexes comprising metals of Group VII (VIIB) as the central metal
    • B01J2531/72—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/821—Ruthenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/822—Rhodium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/824—Palladium

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Nanotechnology (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Catalysts (AREA)
DE10308111A 2003-02-26 2003-02-26 Verfahren zum Abtrennen von gelösten oder kolloidalen Feststoffen aus nicht wässrigen Lösungen Withdrawn DE10308111A1 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE10308111A DE10308111A1 (de) 2003-02-26 2003-02-26 Verfahren zum Abtrennen von gelösten oder kolloidalen Feststoffen aus nicht wässrigen Lösungen
US10/774,778 US20040168981A1 (en) 2003-02-26 2004-02-09 Process for separating dissolved or colloidal solids from a nonaqueous solvent
JP2006501848A JP2006519093A (ja) 2003-02-26 2004-02-13 非水溶媒から溶解した形態またはコロイド形態の固体を分離する方法
PCT/EP2004/001419 WO2004076039A1 (de) 2003-02-26 2004-02-13 Verfahren zum abtrennen von gelösten oder kolloidalen feststoffen aus nicht wässrigem lösemittel
EP04710858A EP1599275A1 (de) 2003-02-26 2004-02-13 Verfahren zum abtrennen von gelösten oder kolloidalen feststoffen aus nicht wässrigem lösemittel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10308111A DE10308111A1 (de) 2003-02-26 2003-02-26 Verfahren zum Abtrennen von gelösten oder kolloidalen Feststoffen aus nicht wässrigen Lösungen

Publications (1)

Publication Number Publication Date
DE10308111A1 true DE10308111A1 (de) 2004-09-09

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DE10308111A Withdrawn DE10308111A1 (de) 2003-02-26 2003-02-26 Verfahren zum Abtrennen von gelösten oder kolloidalen Feststoffen aus nicht wässrigen Lösungen

Country Status (5)

Country Link
US (1) US20040168981A1 (enExample)
EP (1) EP1599275A1 (enExample)
JP (1) JP2006519093A (enExample)
DE (1) DE10308111A1 (enExample)
WO (1) WO2004076039A1 (enExample)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010097428A1 (de) 2009-02-27 2010-09-02 Evonik Oxeno Gmbh Verfahren zur abtrennung und teilweisen rückführung von rhodium bzw. dessen katalytisch wirksamen komplexverbindungen aus prozessströmen
DE102011082441A1 (de) 2011-09-09 2013-03-14 Evonik Oxeno Gmbh Strahlschlaufenreaktor mit Nanofiltration
WO2013124176A1 (de) 2012-02-23 2013-08-29 Evonik Oxeno Gmbh Verfahren und vorrichtung zur hydroformylierung von isobuten und zum auftrennen des produktgemisches
DE102012223572A1 (de) 2012-12-18 2014-06-18 Evonik Industries Ag Steuerung der Viskosität von Reaktionslösungen in Hydroformylierungverfahren
DE102014206520A1 (de) 2013-05-03 2014-11-06 Evonik Industries Ag Neue vierzähnige Phosphor-Liganden mit Hostanox O3 Leitstruktur
DE102013221708A1 (de) 2013-10-25 2015-04-30 Evonik Industries Ag Strahlschlaufenreaktor mit Nanofiltration und Gasseparator

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2578338A1 (en) * 2004-07-16 2006-09-14 California Institute Of Technology Water treatment by dendrimer-enhanced filtration
DE102006003618A1 (de) * 2006-01-26 2007-08-02 Oxeno Olefinchemie Gmbh Verfahren zur Abtrennung von Metall-Komplexkatalysatoren aus Telomerisationsgemischen
DE102006050381A1 (de) * 2006-10-25 2008-05-08 Bayer Materialscience Ag Verfahren zur Abtrennung einer organischen von einer elektrolythaltigen wässrigen und organischen Phase
CN102633378A (zh) * 2012-03-30 2012-08-15 神华集团有限责任公司 一种从煤化工废液中回收催化剂的方法及系统
WO2014001791A1 (en) * 2012-06-26 2014-01-03 Fujifilm Manufacturing Europe Bv Gas separation membrane with an intermediate layer comprising siloxane and|metal complexes
RU2741385C2 (ru) * 2016-03-07 2021-01-25 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Способ извлечения металлического компонента
KR20210062642A (ko) * 2018-10-01 2021-05-31 쉘 인터내셔날 리써취 마트샤피지 비.브이. 나노여과에 의해 촉매 미립자를 제거하는 방법
CN113318608B (zh) * 2021-05-17 2022-07-08 浙江理工大学 一种动态催化的水处理陶瓷膜及其应用

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5288818A (en) * 1991-08-20 1994-02-22 Exxon Chemical Patents Inc. Method for separating a water soluble noble metal catalyst from a noble metal catalyzed hydroformylation reaction
KR970703805A (ko) * 1995-05-01 1997-08-09 유니온 카바이드 케미칼즈 앤드 플라스틱스 테크놀러지 코포레이션 막 분리방법(Membrane Separation)
JPH11285625A (ja) * 1998-02-09 1999-10-19 Toray Ind Inc 触媒分離膜、触媒反応方法および化合物の製造方法
US6252123B1 (en) * 1998-07-09 2001-06-26 Union Carbide Chemicals & Plastics Technology Corporation Membrane separation process for metal complex catalysts
DE19947505A1 (de) * 1999-10-01 2001-04-05 Degussa Verfahren zur Herstellung organischer Verbindungen im Membranreaktor
US6440309B1 (en) * 2000-05-17 2002-08-27 Yoram Cohen Ceramic-supported polymer (CSP) pervaporation membrane

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010097428A1 (de) 2009-02-27 2010-09-02 Evonik Oxeno Gmbh Verfahren zur abtrennung und teilweisen rückführung von rhodium bzw. dessen katalytisch wirksamen komplexverbindungen aus prozessströmen
DE102009001230A1 (de) 2009-02-27 2010-09-02 Evonik Oxeno Gmbh Verfahren zur Abtrennung und teilweiser Rückführung von Übergangsmetallen bzw. deren katalytisch wirksamen Komplexverbindungen aus Prozessströmen
US8748643B2 (en) 2009-02-27 2014-06-10 Evonik Oxeno Gmbh Method for separation and partial return of rhodium and catalytically effective complex compounds thereof from process streams
WO2013034690A1 (de) 2011-09-09 2013-03-14 Evonik Oxeno Gmbh Strahlschlaufenreaktor mit nanofiltration
DE102011082441A1 (de) 2011-09-09 2013-03-14 Evonik Oxeno Gmbh Strahlschlaufenreaktor mit Nanofiltration
WO2013124176A1 (de) 2012-02-23 2013-08-29 Evonik Oxeno Gmbh Verfahren und vorrichtung zur hydroformylierung von isobuten und zum auftrennen des produktgemisches
DE102012202779A1 (de) 2012-02-23 2013-08-29 Evonik Oxeno Gmbh Verfahren und Vorrichtung zur technischen Hydroformylierung von Isobuten und zum Auftrennen des Produktgemisches
DE102012223572A1 (de) 2012-12-18 2014-06-18 Evonik Industries Ag Steuerung der Viskosität von Reaktionslösungen in Hydroformylierungverfahren
WO2014095452A1 (de) 2012-12-18 2014-06-26 Evonik Industries Ag Steuerung der viskosität von reaktionslösungen in hydroformylierungverfahren
DE102014206520A1 (de) 2013-05-03 2014-11-06 Evonik Industries Ag Neue vierzähnige Phosphor-Liganden mit Hostanox O3 Leitstruktur
EP3112373A1 (de) 2013-05-03 2017-01-04 Evonik Degussa GmbH Neuer vierzähniger phosphor-ligand mit hostanox o3 leitstruktur
DE102013221708A1 (de) 2013-10-25 2015-04-30 Evonik Industries Ag Strahlschlaufenreaktor mit Nanofiltration und Gasseparator
US9694341B2 (en) 2013-10-25 2017-07-04 Evonik Degussa Gmbh Jet loop reactor with nanofiltration and gas separator

Also Published As

Publication number Publication date
EP1599275A1 (de) 2005-11-30
WO2004076039A1 (de) 2004-09-10
JP2006519093A (ja) 2006-08-24
US20040168981A1 (en) 2004-09-02

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