DE102012020217A1 - Bindemittelfreie kompakte zeolithische Formkörper und Verfahren zu deren Herstellung - Google Patents

Bindemittelfreie kompakte zeolithische Formkörper und Verfahren zu deren Herstellung Download PDF

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Publication number
DE102012020217A1
DE102012020217A1 DE102012020217.2A DE102012020217A DE102012020217A1 DE 102012020217 A1 DE102012020217 A1 DE 102012020217A1 DE 102012020217 A DE102012020217 A DE 102012020217A DE 102012020217 A1 DE102012020217 A1 DE 102012020217A1
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Germany
Prior art keywords
zeolite
compact
zeolitic
shaped bodies
moldings
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE102012020217.2A
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German (de)
English (en)
Inventor
Kristin Schumann
Baldur Unger
Dr. Brandt Alfons
Gundula Fischer
Hannes Richter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BAD KOESTRITZ CHEMIEWERK GmbH
Chemiewerk Bad Kostritz GmbH
Original Assignee
BAD KOESTRITZ CHEMIEWERK GmbH
Chemiewerk Bad Kostritz GmbH
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Application filed by BAD KOESTRITZ CHEMIEWERK GmbH, Chemiewerk Bad Kostritz GmbH filed Critical BAD KOESTRITZ CHEMIEWERK GmbH
Priority to DE102012020217.2A priority Critical patent/DE102012020217A1/de
Priority to JP2015536100A priority patent/JP6539207B2/ja
Priority to EP13774164.1A priority patent/EP2906341B1/de
Priority to PCT/EP2013/070957 priority patent/WO2014060246A1/de
Priority to US14/435,948 priority patent/US20150298096A1/en
Publication of DE102012020217A1 publication Critical patent/DE102012020217A1/de
Ceased legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B01J20/186—Chemical treatments in view of modifying the properties of the sieve, e.g. increasing the stability or the activity, also decreasing the activity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28042—Shaped bodies; Monolithic structures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28042—Shaped bodies; Monolithic structures
    • B01J20/28045—Honeycomb or cellular structures; Solid foams or sponges
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3007—Moulding, shaping or extruding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3042—Use of binding agents; addition of materials ameliorating the mechanical properties of the produced sorbent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3071—Washing or leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • B01J29/082—X-type faujasite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • B01J29/084—Y-type faujasite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7003—A-type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B01D2253/1085—Zeolites characterized by a silicon-aluminium ratio
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/56—Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional [3D] monoliths
    • B01J35/57—Honeycombs

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
DE102012020217.2A 2012-10-15 2012-10-15 Bindemittelfreie kompakte zeolithische Formkörper und Verfahren zu deren Herstellung Ceased DE102012020217A1 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE102012020217.2A DE102012020217A1 (de) 2012-10-15 2012-10-15 Bindemittelfreie kompakte zeolithische Formkörper und Verfahren zu deren Herstellung
JP2015536100A JP6539207B2 (ja) 2012-10-15 2013-10-08 バインダーフリー緻密ゼオライトプリフォームおよびそれらの製造方法
EP13774164.1A EP2906341B1 (de) 2012-10-15 2013-10-08 Bindemittelfreie kompakte zeolithische formkörper und verfahren zu deren herstellung
PCT/EP2013/070957 WO2014060246A1 (de) 2012-10-15 2013-10-08 Bindemittelfreie kompakte zeolithische formkörper und verfahren zu deren herstellung
US14/435,948 US20150298096A1 (en) 2012-10-15 2013-10-08 Binder-free compact zeolite preforms and method for the production thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102012020217.2A DE102012020217A1 (de) 2012-10-15 2012-10-15 Bindemittelfreie kompakte zeolithische Formkörper und Verfahren zu deren Herstellung

Publications (1)

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DE102012020217A1 true DE102012020217A1 (de) 2014-04-17

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DE102012020217.2A Ceased DE102012020217A1 (de) 2012-10-15 2012-10-15 Bindemittelfreie kompakte zeolithische Formkörper und Verfahren zu deren Herstellung

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Country Link
US (1) US20150298096A1 (https=)
EP (1) EP2906341B1 (https=)
JP (1) JP6539207B2 (https=)
DE (1) DE102012020217A1 (https=)
WO (1) WO2014060246A1 (https=)

Families Citing this family (8)

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Publication number Priority date Publication date Assignee Title
JP6895783B2 (ja) * 2017-03-28 2021-06-30 古河電気工業株式会社 蓄熱装置
CN109647329A (zh) * 2019-01-29 2019-04-19 大连理工大学盘锦产业技术研究院 一种无粘结剂复合分子筛制备方法及其在油品吸附脱硫中的应用
FR3103393B1 (fr) * 2019-11-27 2022-07-01 Arkema France Séparation des gaz de l’air
CN111036187B (zh) * 2019-12-23 2021-03-30 中国科学院过程工程研究所 一种蜂窝载体及其制备方法与应用
FR3117379A1 (fr) 2020-12-15 2022-06-17 IFP Energies Nouvelles Procede de preparation d'un materiau microporeux zeolithique contenant plus de 95% de zeolithe x et ayant une bonne resistance mecanique
EP4523791A1 (en) 2023-09-13 2025-03-19 Technische Universität München Kits and methods for preservation of biological samples
DE102023135343A1 (de) * 2023-12-15 2025-06-18 Volkswagen Aktiengesellschaft Verfahren zur Herstellung eines Sorbentelements zur Abtrennung von einem Gas und/oder Luftfeuchte aus einer fluiden Phase
DE102024107287A1 (de) * 2024-03-14 2025-09-18 Volkswagen Aktiengesellschaft Zeolithisches Granulat, Verfahren zu dessen Herstellung und dessen Verwendung als Adsorptionsmittel

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US4381256A (en) 1981-01-14 1983-04-26 W. R. Grace & Co. Method of producing binderless zeolite extrudates
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US20090318283A1 (en) 2008-06-20 2009-12-24 General Electric Company Catalyst composition and method
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JPS62283812A (ja) 1986-06-03 1987-12-09 Nippon Chem Ind Co Ltd:The ゼオライト成形体およびその製造法
US5387564A (en) 1991-01-07 1995-02-07 Takeda Chemical Industries, Ltd. Molding and calcining of zeolite powder
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DE19815564A1 (de) 1998-03-31 1999-10-07 Grace Gmbh Formkörper aus Zeolith, Verfahren zu seiner Herstellung und dessen Verwendung
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US20100304957A1 (en) 2007-11-30 2010-12-02 Steven Bolaji Ogunwumi Zeolite-Based Honeycomb Body
DE102008046155A1 (de) 2008-03-03 2009-09-10 Chemiewerk Bad Köstritz GmbH Adsorptionsmittelgranulat und Verfahren zu dessen Herstellung
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A. Hauer, Dissertation, TU Berlin, 2002
A. Pfenninger in "Molecular Sieves - Science and Technology", Band 2, Springer-Verlag, 1999, 163
D. Bathen, M. Breitbach, "Adsorptionstechnik", Springer-Verlag, 2001, 13
D. W. Breck, Zeolite Molecular Sieves, John Wiley & Sons, New York, 1976, S. 86
F. Scheffler, R. Herrmann, W. Schwieger, M. Scheffler, Microporous and Mesoporous Materials, 67, 2004, 53-59
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