DE102007038929B4 - Polyphenylensulfid-(Per-)Fluorpolymer-Materialien und Verfahren zu ihrer Herstellung und Verwendung - Google Patents
Polyphenylensulfid-(Per-)Fluorpolymer-Materialien und Verfahren zu ihrer Herstellung und Verwendung Download PDFInfo
- Publication number
- DE102007038929B4 DE102007038929B4 DE102007038929A DE102007038929A DE102007038929B4 DE 102007038929 B4 DE102007038929 B4 DE 102007038929B4 DE 102007038929 A DE102007038929 A DE 102007038929A DE 102007038929 A DE102007038929 A DE 102007038929A DE 102007038929 B4 DE102007038929 B4 DE 102007038929B4
- Authority
- DE
- Germany
- Prior art keywords
- per
- pps
- fluoropolymer
- modified
- groups
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000004734 Polyphenylene sulfide Substances 0.000 title claims abstract description 120
- 229920000069 polyphenylene sulfide Polymers 0.000 title claims abstract description 120
- 229920002313 fluoropolymer Polymers 0.000 title claims abstract description 99
- 239000004811 fluoropolymer Substances 0.000 title claims abstract description 99
- 239000000463 material Substances 0.000 title claims abstract description 49
- 238000000034 method Methods 0.000 title claims description 34
- 238000002360 preparation method Methods 0.000 title claims description 6
- 230000008569 process Effects 0.000 title claims description 5
- 229920000642 polymer Polymers 0.000 claims abstract description 46
- 239000011159 matrix material Substances 0.000 claims abstract description 25
- 230000004048 modification Effects 0.000 claims abstract description 22
- 238000012986 modification Methods 0.000 claims abstract description 22
- 239000000155 melt Substances 0.000 claims abstract description 20
- 239000002245 particle Substances 0.000 claims abstract description 17
- 238000006243 chemical reaction Methods 0.000 claims abstract description 14
- 125000000524 functional group Chemical group 0.000 claims abstract description 12
- 230000002085 persistent effect Effects 0.000 claims abstract description 12
- 238000012412 chemical coupling Methods 0.000 claims abstract description 10
- 125000000864 peroxy group Chemical group O(O*)* 0.000 claims abstract description 8
- TXEYQDLBPFQVAA-UHFFFAOYSA-N tetrafluoromethane Chemical compound FC(F)(F)F TXEYQDLBPFQVAA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 44
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 44
- 239000000843 powder Substances 0.000 claims description 30
- 150000003573 thiols Chemical class 0.000 claims description 20
- 150000007944 thiolates Chemical group 0.000 claims description 19
- 238000013329 compounding Methods 0.000 claims description 13
- 239000000126 substance Substances 0.000 claims description 11
- 238000010128 melt processing Methods 0.000 claims description 10
- -1 polytetrafluoroethylene Polymers 0.000 claims description 10
- 229920002493 poly(chlorotrifluoroethylene) Polymers 0.000 claims description 8
- 239000005023 polychlorotrifluoroethylene (PCTFE) polymer Substances 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 8
- 229920001169 thermoplastic Polymers 0.000 claims description 7
- 239000004416 thermosoftening plastic Substances 0.000 claims description 7
- 239000000654 additive Substances 0.000 claims description 6
- 230000000996 additive effect Effects 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000001301 oxygen Substances 0.000 claims description 6
- 229910052760 oxygen Inorganic materials 0.000 claims description 6
- 125000002843 carboxylic acid group Chemical group 0.000 claims description 5
- 238000007385 chemical modification Methods 0.000 claims description 5
- 230000005855 radiation Effects 0.000 claims description 5
- 239000012779 reinforcing material Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 4
- 229920000840 ethylene tetrafluoroethylene copolymer Polymers 0.000 claims description 4
- 239000000945 filler Substances 0.000 claims description 4
- 238000000465 moulding Methods 0.000 claims description 4
- 239000002667 nucleating agent Substances 0.000 claims description 4
- 125000003396 thiol group Chemical group [H]S* 0.000 claims description 4
- 239000011248 coating agent Substances 0.000 claims description 3
- 230000002209 hydrophobic effect Effects 0.000 claims description 3
- 150000007942 carboxylates Chemical class 0.000 claims description 2
- 239000006185 dispersion Substances 0.000 claims description 2
- 125000006551 perfluoro alkylene group Chemical group 0.000 claims description 2
- 239000012758 reinforcing additive Substances 0.000 claims description 2
- 150000003568 thioethers Chemical class 0.000 claims description 2
- 229920001187 thermosetting polymer Polymers 0.000 claims 1
- 238000005859 coupling reaction Methods 0.000 description 10
- 230000008878 coupling Effects 0.000 description 8
- 238000010168 coupling process Methods 0.000 description 8
- RMVRSNDYEFQCLF-UHFFFAOYSA-N thiophenol Chemical compound SC1=CC=CC=C1 RMVRSNDYEFQCLF-UHFFFAOYSA-N 0.000 description 6
- 229920013633 Fortron Polymers 0.000 description 5
- 239000004738 Fortron® Substances 0.000 description 5
- 238000003379 elimination reaction Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000006114 decarboxylation reaction Methods 0.000 description 3
- 230000008030 elimination Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- IYRWEQXVUNLMAY-UHFFFAOYSA-N carbonyl fluoride Chemical group FC(F)=O IYRWEQXVUNLMAY-UHFFFAOYSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 2
- 238000011065 in-situ storage Methods 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- SYNPRNNJJLRHTI-UHFFFAOYSA-N 2-(hydroxymethyl)butane-1,4-diol Chemical compound OCCC(CO)CO SYNPRNNJJLRHTI-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 239000004609 Impact Modifier Substances 0.000 description 1
- 238000001994 activation Methods 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000007824 aliphatic compounds Chemical class 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001728 carbonyl compounds Chemical class 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- MVPPADPHJFYWMZ-IDEBNGHGSA-N chlorobenzene Chemical group Cl[13C]1=[13CH][13CH]=[13CH][13CH]=[13CH]1 MVPPADPHJFYWMZ-IDEBNGHGSA-N 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 238000007306 functionalization reaction Methods 0.000 description 1
- 230000004313 glare Effects 0.000 description 1
- 239000012761 high-performance material Substances 0.000 description 1
- 229910000039 hydrogen halide Inorganic materials 0.000 description 1
- 239000012433 hydrogen halide Substances 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 238000005453 pelletization Methods 0.000 description 1
- 239000006069 physical mixture Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- ODZPKZBBUMBTMG-UHFFFAOYSA-N sodium amide Chemical compound [NH2-].[Na+] ODZPKZBBUMBTMG-UHFFFAOYSA-N 0.000 description 1
- 229910052979 sodium sulfide Inorganic materials 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
- 238000000371 solid-state nuclear magnetic resonance spectroscopy Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000007725 thermal activation Methods 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- 150000007970 thio esters Chemical class 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/0286—Chemical after-treatment
- C08G75/029—Modification with organic compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L81/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing sulfur with or without nitrogen, oxygen or carbon only; Compositions of polysulfones; Compositions of derivatives of such polymers
- C08L81/02—Polythioethers; Polythioether-ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/26—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers modified by chemical after-treatment
- C08L23/28—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers modified by chemical after-treatment by reaction with halogens or halogen-containing compounds
- C08L23/283—Iso-olefin halogenated homopolymers or copolymers
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102007038929A DE102007038929B4 (de) | 2007-08-13 | 2007-08-13 | Polyphenylensulfid-(Per-)Fluorpolymer-Materialien und Verfahren zu ihrer Herstellung und Verwendung |
| PCT/EP2008/060467 WO2009021922A1 (de) | 2007-08-13 | 2008-08-08 | Polyphenylensulfid-(per-)fluorpolymer-materialien und verfahren zu ihrer herstellung und verwendung |
| CN200880103398A CN101784611A (zh) | 2007-08-13 | 2008-08-08 | 聚苯硫醚全氟聚合物材料及其制备方法和应用 |
| US12/673,362 US20110040017A1 (en) | 2007-08-13 | 2008-08-08 | Polyphenylene sulfide (per)fluoropolymer materials and process for preparation and use therof |
| JP2010520547A JP2010535922A (ja) | 2007-08-13 | 2008-08-08 | ポリフェニレンスルフィド（ペル）フルオロポリマー材料ならびにその製造方法および使用 |
| EP08802981.4A EP2178981B1 (de) | 2007-08-13 | 2008-08-08 | Polyphenylensulfid-(per-)fluorpolymer-materialien und verfahren zu ihrer herstellung und verwendung |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102007038929A DE102007038929B4 (de) | 2007-08-13 | 2007-08-13 | Polyphenylensulfid-(Per-)Fluorpolymer-Materialien und Verfahren zu ihrer Herstellung und Verwendung |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE102007038929A1 DE102007038929A1 (de) | 2009-02-19 |
| DE102007038929B4 true DE102007038929B4 (de) | 2010-01-14 |
Family
ID=39938693
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE102007038929A Expired - Fee Related DE102007038929B4 (de) | 2007-08-13 | 2007-08-13 | Polyphenylensulfid-(Per-)Fluorpolymer-Materialien und Verfahren zu ihrer Herstellung und Verwendung |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20110040017A1 (https=) |
| EP (1) | EP2178981B1 (https=) |
| JP (1) | JP2010535922A (https=) |
| CN (1) | CN101784611A (https=) |
| DE (1) | DE102007038929B4 (https=) |
| WO (1) | WO2009021922A1 (https=) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009014974A1 (de) | 2009-03-18 | 2010-09-23 | Elringklinger Ag | Polymercompound sowie Bauteile, hergestellt unter Verwendung des Compounds |
| DE102009018637A1 (de) * | 2009-04-17 | 2010-10-21 | Elringklinger Ag | Gleitlager |
| EP2949705A4 (en) * | 2013-01-23 | 2016-08-17 | Toray Industries | POLYPHENYLENE SULFIDE RESIN COMPOSITION, METHOD FOR THE MANUFACTURE THEREOF AND SHAPED PRODUCT THEREOF |
| JP6015846B2 (ja) * | 2013-03-19 | 2016-10-26 | ダイキン工業株式会社 | 電気絶縁部品 |
| CN104098899A (zh) * | 2014-07-08 | 2014-10-15 | 安徽宁国市高新管业有限公司 | 一种耐腐蚀阻燃耐热的电缆护套材料 |
| CN107353645B (zh) * | 2017-06-28 | 2020-01-10 | 四川大学 | 一种易结晶的聚苯硫醚自润滑树脂组合物及其制备方法 |
| KR102442843B1 (ko) | 2018-05-25 | 2022-09-14 | 다이킨 고교 가부시키가이샤 | 수지 조성물 |
| CN114058183B (zh) * | 2021-12-17 | 2023-12-01 | 特塑（大连）高分子材料有限公司 | 一种聚苯硫醚改性材料及其制备方法和应用 |
| CN116988102B (zh) * | 2023-07-26 | 2024-04-09 | 江苏大学 | 一种纳米输运碱性电解水隔膜及制造方法 |
| CN119361691A (zh) * | 2024-11-21 | 2025-01-24 | 浙江锂威能源科技有限公司 | 一种改性磷酸铁锰锂材料及其制备方法和锂离子电池 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5376996A (en) * | 1992-12-16 | 1994-12-27 | International Business Machines Corporation | Polyphenylene sulfide-PTFE coating for fuser roll |
| US5684088A (en) * | 1992-11-05 | 1997-11-04 | Daikin Industries, Ltd. | Polyphenylene sulfide resin compositions and process for preparation of same |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5750626A (en) * | 1992-12-10 | 1998-05-12 | Daikin Industries, Ltd. | Thermoplastic resin composition |
| JP4077332B2 (ja) * | 1992-12-10 | 2008-04-16 | ダイキン工業株式会社 | 熱可塑性樹脂組成物 |
| JPH07268126A (ja) * | 1994-03-31 | 1995-10-17 | Ntn Corp | 潤滑性樹脂組成物 |
| CA2168794A1 (en) * | 1994-06-09 | 1995-12-14 | Takayuki Araki | Fluoroolefin, fluoropolymer, and thermoplastic resin composition containing the polymer |
| US5576106A (en) | 1994-07-28 | 1996-11-19 | E. I. Du Pont De Nemours And Company | Grafted fluoropolymer powders |
| JP2878977B2 (ja) * | 1994-11-29 | 1999-04-05 | ニチアス株式会社 | 摺動用樹脂組成物 |
| US6476125B1 (en) * | 1995-08-24 | 2002-11-05 | Asahi Glass Company Ltd. | Fluorine-containing polymer alloy, and method for its preparation and method for its molding |
| JPH10158456A (ja) * | 1996-11-27 | 1998-06-16 | Ntn Corp | 潤滑性樹脂組成物 |
| JP3961103B2 (ja) * | 1997-02-25 | 2007-08-22 | Ｎｔｎ株式会社 | 摺動材用樹脂組成物および樹脂製歯車 |
| DE19823609A1 (de) * | 1998-05-27 | 1999-12-02 | Inst Polymerforschung Dresden | Compounds aus Polyamid- und Perfluoralkylsubstanz(en) und Mischungen dieser Compounds mit weiteren Polymersubstanzen, Verfahren zu ihrer Herstellung und Verwendung |
| JP4081914B2 (ja) * | 1999-04-08 | 2008-04-30 | 日立電線株式会社 | 改質ふっ素樹脂、改質ふっ素樹脂組成物及び改質ふっ素樹脂成形体 |
| JP4668375B2 (ja) * | 1999-08-19 | 2011-04-13 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 低溶融粘度ポリテトラフルオロエチレン組成物 |
| JP4033599B2 (ja) * | 2000-04-14 | 2008-01-16 | Ｎｔｎ株式会社 | 定着ローラ用断熱スリーブ |
| JP2002221277A (ja) * | 2001-01-25 | 2002-08-09 | Ntn Corp | ディスクバルブおよびディスクバルブ用樹脂組成物 |
| JP2003014141A (ja) * | 2001-06-28 | 2003-01-15 | Ntn Corp | ディスクバルブおよびディスクバルブ用樹脂組成物 |
| JP4226249B2 (ja) * | 2002-02-13 | 2009-02-18 | Ｎｔｎ株式会社 | 樹脂製ナットおよびすべりねじ装置 |
| DE10351813B4 (de) * | 2003-10-30 | 2006-04-13 | Leibniz-Institut Für Polymerforschung Dresden E.V. | Radikalisch gekoppelte PTFE-Polymer-Pulver und Verfahren zu ihrer Herstellung |
| DE10351814A1 (de) * | 2003-10-30 | 2005-06-16 | Institut Für Polymerforschung Dresden E.V. | Radikalisch gekoppelte PTFE-Polymer-Compounds und Verfahren zu ihrer Herstellung |
| DE102004016873B4 (de) * | 2004-03-29 | 2014-09-25 | Leibniz-Institut Für Polymerforschung Dresden E.V. | Radikalisch gekoppelte Perfluorpolymer-Polymer-Materialien und Verfahren zu ihrer Herstellung |
-
2007
- 2007-08-13 DE DE102007038929A patent/DE102007038929B4/de not_active Expired - Fee Related
-
2008
- 2008-08-08 CN CN200880103398A patent/CN101784611A/zh active Pending
- 2008-08-08 WO PCT/EP2008/060467 patent/WO2009021922A1/de not_active Ceased
- 2008-08-08 JP JP2010520547A patent/JP2010535922A/ja active Pending
- 2008-08-08 EP EP08802981.4A patent/EP2178981B1/de active Active
- 2008-08-08 US US12/673,362 patent/US20110040017A1/en not_active Abandoned
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5684088A (en) * | 1992-11-05 | 1997-11-04 | Daikin Industries, Ltd. | Polyphenylene sulfide resin compositions and process for preparation of same |
| US5376996A (en) * | 1992-12-16 | 1994-12-27 | International Business Machines Corporation | Polyphenylene sulfide-PTFE coating for fuser roll |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2010535922A (ja) | 2010-11-25 |
| US20110040017A1 (en) | 2011-02-17 |
| EP2178981B1 (de) | 2016-03-09 |
| DE102007038929A1 (de) | 2009-02-19 |
| CN101784611A (zh) | 2010-07-21 |
| WO2009021922A1 (de) | 2009-02-19 |
| EP2178981A1 (de) | 2010-04-28 |
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