DE102005061382A1 - Umwandlung eines Präkatalysators in eine katalytisch aktive Silber-Vanadiumoxid-Bronze - Google Patents

Umwandlung eines Präkatalysators in eine katalytisch aktive Silber-Vanadiumoxid-Bronze Download PDF

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Publication number
DE102005061382A1
DE102005061382A1 DE102005061382A DE102005061382A DE102005061382A1 DE 102005061382 A1 DE102005061382 A1 DE 102005061382A1 DE 102005061382 A DE102005061382 A DE 102005061382A DE 102005061382 A DE102005061382 A DE 102005061382A DE 102005061382 A1 DE102005061382 A1 DE 102005061382A1
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DE
Germany
Prior art keywords
catalyst
carbon source
acid
amount
precatalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
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DE102005061382A
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German (de)
English (en)
Inventor
Samuel Dr. Neto
Hartmut Prof. Dr. Hibst
Frank Dr. Rosowski
Sebastian Dr. Storck
Jürgen Dr. Zühlke
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BASF SE
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BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to DE102005061382A priority Critical patent/DE102005061382A1/de
Priority to BRPI0620101A priority patent/BRPI0620101A2/pt
Priority to US12/158,858 priority patent/US20090291845A1/en
Priority to JP2008546459A priority patent/JP4956548B2/ja
Priority to KR1020087017842A priority patent/KR20080090440A/ko
Priority to CN2006800514865A priority patent/CN101360561B/zh
Priority to EP06830762A priority patent/EP1968743B1/de
Priority to DE502006009180T priority patent/DE502006009180D1/de
Priority to PCT/EP2006/070041 priority patent/WO2007071749A1/de
Priority to AT06830762T priority patent/ATE502696T1/de
Priority to TW095148222A priority patent/TW200727984A/zh
Publication of DE102005061382A1 publication Critical patent/DE102005061382A1/de
Withdrawn legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/66—Silver or gold
    • B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/682—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium, tantalum or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/66—Silver or gold
    • B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0219—Coating the coating containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00—Compounds of vanadium
    • C01G31/006—Compounds containing vanadium, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/34—Mechanical properties
    • B01J35/38—Abrasion or attrition resistance
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0221—Coating of particles
    • B01J37/0223—Coating of particles by rotation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
DE102005061382A 2005-12-21 2005-12-21 Umwandlung eines Präkatalysators in eine katalytisch aktive Silber-Vanadiumoxid-Bronze Withdrawn DE102005061382A1 (de)

Priority Applications (11)

Application Number Priority Date Filing Date Title
DE102005061382A DE102005061382A1 (de) 2005-12-21 2005-12-21 Umwandlung eines Präkatalysators in eine katalytisch aktive Silber-Vanadiumoxid-Bronze
BRPI0620101A BRPI0620101A2 (pt) 2005-12-21 2006-12-20 processo para converter um pré-catalisador
US12/158,858 US20090291845A1 (en) 2005-12-21 2006-12-20 Conversion of a precatalyst to a catalytically active silver-vanadium oxide bronze
JP2008546459A JP4956548B2 (ja) 2005-12-21 2006-12-20 触媒活性の銀−酸化バナジウム−ブロンズへの触媒前駆体の変換
KR1020087017842A KR20080090440A (ko) 2005-12-21 2006-12-20 전촉매의 촉매 활성 은-바나듐 산화물 브론즈로의 전환
CN2006800514865A CN101360561B (zh) 2005-12-21 2006-12-20 预催化剂向催化活性银钒氧化物青铜的转化
EP06830762A EP1968743B1 (de) 2005-12-21 2006-12-20 Umwandlung eines präkatalysators in eine katalytisch aktive silber-vanadiumoxid-bronze
DE502006009180T DE502006009180D1 (de) 2005-12-21 2006-12-20 Umwandlung eines präkatalysators in eine katalytisch aktive silber-vanadiumoxid-bronze
PCT/EP2006/070041 WO2007071749A1 (de) 2005-12-21 2006-12-20 Umwandlung eines präkatalysators in eine katalytisch aktive silber-vanadiumoxid-bronze
AT06830762T ATE502696T1 (de) 2005-12-21 2006-12-20 Umwandlung eines präkatalysators in eine katalytisch aktive silber-vanadiumoxid-bronze
TW095148222A TW200727984A (en) 2005-12-21 2006-12-21 Conversion of a precatalyst to a catalytically active silver vanadium oxide bronze

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102005061382A DE102005061382A1 (de) 2005-12-21 2005-12-21 Umwandlung eines Präkatalysators in eine katalytisch aktive Silber-Vanadiumoxid-Bronze

Publications (1)

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DE102005061382A1 true DE102005061382A1 (de) 2007-06-28

Family

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Family Applications (2)

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DE102005061382A Withdrawn DE102005061382A1 (de) 2005-12-21 2005-12-21 Umwandlung eines Präkatalysators in eine katalytisch aktive Silber-Vanadiumoxid-Bronze
DE502006009180T Active DE502006009180D1 (de) 2005-12-21 2006-12-20 Umwandlung eines präkatalysators in eine katalytisch aktive silber-vanadiumoxid-bronze

Family Applications After (1)

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DE502006009180T Active DE502006009180D1 (de) 2005-12-21 2006-12-20 Umwandlung eines präkatalysators in eine katalytisch aktive silber-vanadiumoxid-bronze

Country Status (10)

Country Link
US (1) US20090291845A1 (https=)
EP (1) EP1968743B1 (https=)
JP (1) JP4956548B2 (https=)
KR (1) KR20080090440A (https=)
CN (1) CN101360561B (https=)
AT (1) ATE502696T1 (https=)
BR (1) BRPI0620101A2 (https=)
DE (2) DE102005061382A1 (https=)
TW (1) TW200727984A (https=)
WO (1) WO2007071749A1 (https=)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010072721A3 (de) * 2008-12-22 2010-10-28 Basf Se Katalysatorformkörper und verfahren zur herstellung von maleinsäureanhydrid
DE102012003236A1 (de) 2012-02-20 2013-08-22 Clariant Produkte (Deutschland) Gmbh Vorvergoldung von Pd-Au-gecoateten Schalenkatalysatoren

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BRPI0910954A2 (pt) * 2008-04-07 2016-01-05 Basf Se método para iniciar um reator de oxidação em fase gasosa
TWI491087B (zh) * 2009-08-26 2015-07-01 Univ Nat Taiwan 用於有機光電元件之過渡金屬氧化物的懸浮液或溶液、其製作方法與應用

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19705326A1 (de) * 1997-02-12 1998-08-13 Basf Ag Verfahren zur selektiven Oxidation von nicht-cyclischen ungesättigten Kohlenwasserstoffen mittels Katalysatoren auf Basis von Silben-Vanadium-Mischoxiden
DE19851786A1 (de) * 1998-11-10 2000-05-11 Basf Ag Silber- und Vanadiumoxid enthaltendes Multimetalloxid und dessen Verwendung
DE10334132A1 (de) * 2003-07-25 2005-04-07 Basf Ag Silber, Vanadium und ein Promotormetall enthaltendes Multimetalloxid und dessen Verwendung
DE102004014918A1 (de) * 2004-03-26 2005-10-13 Basf Ag Katalysator mit einer Silber-Vanadiumoxidphase und einer Promotorphase

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010072721A3 (de) * 2008-12-22 2010-10-28 Basf Se Katalysatorformkörper und verfahren zur herstellung von maleinsäureanhydrid
DE102012003236A1 (de) 2012-02-20 2013-08-22 Clariant Produkte (Deutschland) Gmbh Vorvergoldung von Pd-Au-gecoateten Schalenkatalysatoren
WO2013124293A1 (de) 2012-02-20 2013-08-29 Clariant Produkte (Deutschland) Gmbh Vorvergoldung von pd-au-gecoateten schalenkatalysatoren
US9555397B2 (en) 2012-02-20 2017-01-31 Clariant Produkte (Deutschland) Gmbh Pre-gold-plating Pd-Au-coated shell catalysts

Also Published As

Publication number Publication date
US20090291845A1 (en) 2009-11-26
CN101360561B (zh) 2011-11-09
BRPI0620101A2 (pt) 2016-11-16
EP1968743A1 (de) 2008-09-17
KR20080090440A (ko) 2008-10-08
TW200727984A (en) 2007-08-01
JP2009520588A (ja) 2009-05-28
ATE502696T1 (de) 2011-04-15
EP1968743B1 (de) 2011-03-23
DE502006009180D1 (de) 2011-05-05
WO2007071749A1 (de) 2007-06-28
CN101360561A (zh) 2009-02-04
JP4956548B2 (ja) 2012-06-20

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Owner name: BASF SE, 67063 LUDWIGSHAFEN, DE

8139 Disposal/non-payment of the annual fee