DE10057678A1 - Verfahren zur Herstellung von schmelzfähigen Polyestern - Google Patents
Verfahren zur Herstellung von schmelzfähigen PolyesternInfo
- Publication number
- DE10057678A1 DE10057678A1 DE10057678A DE10057678A DE10057678A1 DE 10057678 A1 DE10057678 A1 DE 10057678A1 DE 10057678 A DE10057678 A DE 10057678A DE 10057678 A DE10057678 A DE 10057678A DE 10057678 A1 DE10057678 A1 DE 10057678A1
- Authority
- DE
- Germany
- Prior art keywords
- acid
- anhydride
- polyester
- rigid
- semi
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 229920000728 polyester Polymers 0.000 title claims abstract description 37
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 23
- 238000000034 method Methods 0.000 title claims abstract description 16
- 229920000642 polymer Polymers 0.000 claims abstract description 37
- 150000008064 anhydrides Chemical class 0.000 claims abstract description 27
- 239000000155 melt Substances 0.000 claims abstract description 16
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims abstract description 11
- 125000004122 cyclic group Chemical group 0.000 claims abstract description 10
- 239000000835 fiber Substances 0.000 claims abstract description 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 5
- 125000004185 ester group Chemical group 0.000 claims abstract description 4
- 229920001400 block copolymer Polymers 0.000 claims abstract 5
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 17
- -1 hydroquinone diacetate dihydric phenols Chemical class 0.000 claims description 17
- 238000006243 chemical reaction Methods 0.000 claims description 12
- ITMVZTDHPFXUDY-UHFFFAOYSA-N 2-(1-carboxypentyl)-1,3-dioxoisoindole-5-carboxylic acid Chemical compound C1=C(C(O)=O)C=C2C(=O)N(C(CCCC)C(O)=O)C(=O)C2=C1 ITMVZTDHPFXUDY-UHFFFAOYSA-N 0.000 claims description 10
- GDBUZIKSJGRBJP-UHFFFAOYSA-N 4-acetoxy benzoic acid Chemical compound CC(=O)OC1=CC=C(C(O)=O)C=C1 GDBUZIKSJGRBJP-UHFFFAOYSA-N 0.000 claims description 9
- 238000006068 polycondensation reaction Methods 0.000 claims description 9
- 229920003055 poly(ester-imide) Polymers 0.000 claims description 8
- AKOGNYJNGMLDOA-UHFFFAOYSA-N (4-acetyloxyphenyl) acetate Chemical compound CC(=O)OC1=CC=C(OC(C)=O)C=C1 AKOGNYJNGMLDOA-UHFFFAOYSA-N 0.000 claims description 7
- 239000000178 monomer Substances 0.000 claims description 7
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims description 6
- 239000004952 Polyamide Substances 0.000 claims description 5
- 229920002647 polyamide Polymers 0.000 claims description 5
- KHJOWOCSERMQKF-UHFFFAOYSA-N 2-[6-(5-carboxy-1,3-dioxoisoindol-2-yl)hexyl]-1,3-dioxoisoindole-5-carboxylic acid Chemical compound O=C1C2=CC=C(C(O)=O)C=C2C(=O)N1CCCCCCN1C(=O)C2=CC=C(C(=O)O)C=C2C1=O KHJOWOCSERMQKF-UHFFFAOYSA-N 0.000 claims description 4
- 125000001931 aliphatic group Chemical group 0.000 claims description 3
- 229920001634 Copolyester Polymers 0.000 claims description 2
- 150000001491 aromatic compounds Chemical class 0.000 claims description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 2
- 150000003972 cyclic carboxylic anhydrides Chemical class 0.000 claims description 2
- 229920002959 polymer blend Polymers 0.000 claims description 2
- CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical class NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 claims 1
- GCAIYLBJUFLNDP-UHFFFAOYSA-N 4-acetyloxyphthalic acid Chemical compound CC(=O)OC1=CC=C(C(O)=O)C(C(O)=O)=C1 GCAIYLBJUFLNDP-UHFFFAOYSA-N 0.000 claims 1
- 239000004698 Polyethylene Substances 0.000 claims 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000001718 carbodiimides Chemical class 0.000 claims 1
- 238000010276 construction Methods 0.000 claims 1
- 238000005755 formation reaction Methods 0.000 claims 1
- 150000002918 oxazolines Chemical class 0.000 claims 1
- 229920001707 polybutylene terephthalate Polymers 0.000 claims 1
- 229920000573 polyethylene Polymers 0.000 claims 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 14
- 239000011159 matrix material Substances 0.000 abstract description 5
- 230000002787 reinforcement Effects 0.000 abstract description 5
- 238000012545 processing Methods 0.000 abstract description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 6
- 229920001577 copolymer Polymers 0.000 description 6
- 230000007717 exclusion Effects 0.000 description 5
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 239000004744 fabric Substances 0.000 description 4
- 229920000578 graft copolymer Polymers 0.000 description 4
- 239000008187 granular material Substances 0.000 description 4
- 239000000395 magnesium oxide Substances 0.000 description 4
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 4
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 229920000139 polyethylene terephthalate Polymers 0.000 description 4
- 239000005020 polyethylene terephthalate Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000007792 addition Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 239000011888 foil Substances 0.000 description 3
- 238000011065 in-situ storage Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 239000004793 Polystyrene Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229920002223 polystyrene Polymers 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000012549 training Methods 0.000 description 2
- PSSBVORCFWWHFQ-UHFFFAOYSA-N (7-acetyloxy-1,3-dioxo-2-benzofuran-4-yl) acetate Chemical compound CC(=O)OC1=CC=C(OC(C)=O)C2=C1C(=O)OC2=O PSSBVORCFWWHFQ-UHFFFAOYSA-N 0.000 description 1
- QMMJWQMCMRUYTG-UHFFFAOYSA-N 1,2,4,5-tetrachloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=C(Cl)C(Cl)=CC(Cl)=C1Cl QMMJWQMCMRUYTG-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 239000004953 Aliphatic polyamide Substances 0.000 description 1
- LFVLUOAHQIVABZ-UHFFFAOYSA-N Iodofenphos Chemical compound COP(=S)(OC)OC1=CC(Cl)=C(I)C=C1Cl LFVLUOAHQIVABZ-UHFFFAOYSA-N 0.000 description 1
- 229920002292 Nylon 6 Polymers 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920003231 aliphatic polyamide Polymers 0.000 description 1
- 229920003232 aliphatic polyester Polymers 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000004760 aramid Substances 0.000 description 1
- 229920003235 aromatic polyamide Polymers 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001010 compromised effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000000877 morphologic effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229920006287 phenoxy resin Polymers 0.000 description 1
- 239000013034 phenoxy resin Substances 0.000 description 1
- 229920001230 polyarylate Polymers 0.000 description 1
- 229920006149 polyester-amide block copolymer Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/78—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolycondensation products
- D01F6/82—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolycondensation products from polyester amides or polyether amides
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Polyesters Or Polycarbonates (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10057678A DE10057678A1 (de) | 2000-11-21 | 2000-11-21 | Verfahren zur Herstellung von schmelzfähigen Polyestern |
| PCT/DE2001/004294 WO2002042353A2 (de) | 2000-11-21 | 2001-11-20 | Verfahren zur herstellung von schmelzfähigen polyestern |
| AT01997516T ATE288455T1 (de) | 2000-11-21 | 2001-11-20 | Verfahren zur herstellung von schmelzfähigen polyestern |
| EP01997516A EP1339773B1 (de) | 2000-11-21 | 2001-11-20 | Verfahren zur herstellung von schmelzfähigen polyestern |
| US10/399,189 US7009027B2 (en) | 2000-11-21 | 2001-11-20 | Method for producing meltable polyesters |
| JP2002545066A JP2004519532A (ja) | 2000-11-21 | 2001-11-20 | 溶融性ポリエステルの製造方法 |
| DE50105266T DE50105266D1 (de) | 2000-11-21 | 2001-11-20 | Verfahren zur herstellung von schmelzfähigen polyestern |
| AU2002215854A AU2002215854A1 (en) | 2000-11-21 | 2001-11-20 | Method for producing meltable polyesters |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10057678A DE10057678A1 (de) | 2000-11-21 | 2000-11-21 | Verfahren zur Herstellung von schmelzfähigen Polyestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE10057678A1 true DE10057678A1 (de) | 2002-05-29 |
Family
ID=7664069
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE10057678A Ceased DE10057678A1 (de) | 2000-11-21 | 2000-11-21 | Verfahren zur Herstellung von schmelzfähigen Polyestern |
| DE50105266T Expired - Lifetime DE50105266D1 (de) | 2000-11-21 | 2001-11-20 | Verfahren zur herstellung von schmelzfähigen polyestern |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE50105266T Expired - Lifetime DE50105266D1 (de) | 2000-11-21 | 2001-11-20 | Verfahren zur herstellung von schmelzfähigen polyestern |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7009027B2 (https=) |
| EP (1) | EP1339773B1 (https=) |
| JP (1) | JP2004519532A (https=) |
| AT (1) | ATE288455T1 (https=) |
| AU (1) | AU2002215854A1 (https=) |
| DE (2) | DE10057678A1 (https=) |
| WO (1) | WO2002042353A2 (https=) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7666963B2 (en) * | 2005-07-21 | 2010-02-23 | Akzo Nobel N.V. | Hybrid copolymers |
| NO20073834L (no) * | 2006-07-21 | 2008-01-22 | Akzo Nobel Chemicals Int Bv | Sulfonerte podede kopolymerer |
| NO20073821L (no) * | 2006-07-21 | 2008-01-22 | Akzo Nobel Chemicals Int Bv | Podede kopolymerer med lav molekylvekt |
| EP2064179B1 (en) * | 2006-09-07 | 2012-08-29 | Lubrizol Limited | Dispersants containing terminal acidic groups |
| JP5645937B2 (ja) | 2009-07-31 | 2014-12-24 | アクゾ ノーベル ナムローゼ フェンノートシャップＡｋｚｏ Ｎｏｂｅｌ Ｎ．Ｖ． | パーソナルケア用途のためのハイブリッドコポリマー組成物 |
| US8841246B2 (en) | 2011-08-05 | 2014-09-23 | Ecolab Usa Inc. | Cleaning composition containing a polysaccharide hybrid polymer composition and methods of improving drainage |
| US8679366B2 (en) | 2011-08-05 | 2014-03-25 | Ecolab Usa Inc. | Cleaning composition containing a polysaccharide graft polymer composition and methods of controlling hard water scale |
| US8853144B2 (en) | 2011-08-05 | 2014-10-07 | Ecolab Usa Inc. | Cleaning composition containing a polysaccharide graft polymer composition and methods of improving drainage |
| US8636918B2 (en) | 2011-08-05 | 2014-01-28 | Ecolab Usa Inc. | Cleaning composition containing a polysaccharide hybrid polymer composition and methods of controlling hard water scale |
| BR112014009040A2 (pt) | 2011-11-04 | 2017-05-09 | Akzo Nobel Chemicals Int Bv | copolímero obtenível através da polimerização de pelo menos um primeiro monômero etilenicamente não saturado e pelo menos um segundo monômero etilenicamente não saturado; composição de copolímero; e processo para preparação do copolímero de dendrito |
| IN2014DN03123A (https=) | 2011-11-04 | 2015-05-22 | Akzo Nobel Chemicals Int Bv | |
| US8945314B2 (en) | 2012-07-30 | 2015-02-03 | Ecolab Usa Inc. | Biodegradable stability binding agent for a solid detergent |
| US9365805B2 (en) | 2014-05-15 | 2016-06-14 | Ecolab Usa Inc. | Bio-based pot and pan pre-soak |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3617515A (en) | 1969-05-26 | 1971-11-02 | Lummus Co | Production of needle coke from coal for pitch |
| DE3718396A1 (de) | 1987-06-02 | 1988-12-22 | Bayer Ag | Thermotrope polyesterimide mit ausgezeichneter verarbeitbarkeit, verfahren zu ihrer herstellung und ihre verwendung zur herstellung von formkoerpern, filamenten, fasern und folien |
| NL8901737A (nl) | 1989-07-07 | 1991-02-01 | Stamicarbon | Polymeersamenstelling op basis van een vloeibaar kristallijn polymeer en een polyamide. |
| WO1994019410A1 (fr) * | 1993-02-17 | 1994-09-01 | Mitsubishi Gas Chemical Company, Inc. | Composition de resine |
| DE4342705C2 (de) * | 1993-12-15 | 2000-08-10 | Thueringisches Inst Textil | Verfahren zur Herstellung von Polyamidblockcopolymeren insbesondere Polyamidseitenketten-gepfropften steif- und halbsteifkettigen Polymeren |
| EP0771848B1 (en) * | 1995-04-27 | 2004-02-18 | Polyplastics Co. Ltd. | Thermoplastic resin composition and process for production thereof |
-
2000
- 2000-11-21 DE DE10057678A patent/DE10057678A1/de not_active Ceased
-
2001
- 2001-11-20 JP JP2002545066A patent/JP2004519532A/ja active Pending
- 2001-11-20 AU AU2002215854A patent/AU2002215854A1/en not_active Abandoned
- 2001-11-20 US US10/399,189 patent/US7009027B2/en not_active Expired - Fee Related
- 2001-11-20 WO PCT/DE2001/004294 patent/WO2002042353A2/de not_active Ceased
- 2001-11-20 DE DE50105266T patent/DE50105266D1/de not_active Expired - Lifetime
- 2001-11-20 AT AT01997516T patent/ATE288455T1/de not_active IP Right Cessation
- 2001-11-20 EP EP01997516A patent/EP1339773B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP1339773B1 (de) | 2005-02-02 |
| AU2002215854A1 (en) | 2002-06-03 |
| JP2004519532A (ja) | 2004-07-02 |
| EP1339773A2 (de) | 2003-09-03 |
| US20040039137A1 (en) | 2004-02-26 |
| WO2002042353A3 (de) | 2002-09-19 |
| DE50105266D1 (de) | 2005-03-10 |
| US7009027B2 (en) | 2006-03-07 |
| ATE288455T1 (de) | 2005-02-15 |
| WO2002042353A2 (de) | 2002-05-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| 8131 | Rejection |