CS219906B2 - Method of gaining the cyanurchloride - Google Patents
Method of gaining the cyanurchloride Download PDFInfo
- Publication number
- CS219906B2 CS219906B2 CS796449A CS644979A CS219906B2 CS 219906 B2 CS219906 B2 CS 219906B2 CS 796449 A CS796449 A CS 796449A CS 644979 A CS644979 A CS 644979A CS 219906 B2 CS219906 B2 CS 219906B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- cyanuric chloride
- liquid
- chloride
- solid
- condenser
- Prior art date
Links
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 title claims abstract description 139
- 238000000034 method Methods 0.000 title claims abstract description 42
- 239000007788 liquid Substances 0.000 claims abstract description 47
- 239000007787 solid Substances 0.000 claims abstract description 33
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000005829 trimerization reaction Methods 0.000 claims abstract description 10
- 238000009835 boiling Methods 0.000 claims abstract description 7
- 238000011084 recovery Methods 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims description 28
- 238000009826 distribution Methods 0.000 claims description 26
- 239000000460 chlorine Substances 0.000 claims description 16
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 12
- 229910052801 chlorine Inorganic materials 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 10
- 238000009833 condensation Methods 0.000 claims description 7
- 230000005494 condensation Effects 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 6
- 239000003380 propellant Substances 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 4
- -1 aromatic halogenated hydrocarbons Chemical class 0.000 claims description 3
- 238000001694 spray drying Methods 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims 2
- MYWUZJCMWCOHBA-VIFPVBQESA-N methamphetamine Chemical compound CN[C@@H](C)CC1=CC=CC=C1 MYWUZJCMWCOHBA-VIFPVBQESA-N 0.000 claims 1
- 230000001105 regulatory effect Effects 0.000 claims 1
- 230000003381 solubilizing effect Effects 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 abstract description 8
- 239000007789 gas Substances 0.000 description 45
- 238000001556 precipitation Methods 0.000 description 30
- 239000002826 coolant Substances 0.000 description 21
- 239000000047 product Substances 0.000 description 15
- 238000005029 sieve analysis Methods 0.000 description 11
- 239000002912 waste gas Substances 0.000 description 9
- 239000002904 solvent Substances 0.000 description 8
- 238000002425 crystallisation Methods 0.000 description 7
- 230000008025 crystallization Effects 0.000 description 7
- 239000011261 inert gas Substances 0.000 description 7
- 238000003860 storage Methods 0.000 description 7
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 238000001228 spectrum Methods 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 239000012265 solid product Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000012495 reaction gas Substances 0.000 description 4
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- 238000011144 upstream manufacturing Methods 0.000 description 4
- 239000000110 cooling liquid Substances 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- BOSAWIQFTJIYIS-UHFFFAOYSA-N 1,1,1-trichloro-2,2,2-trifluoroethane Chemical compound FC(F)(F)C(Cl)(Cl)Cl BOSAWIQFTJIYIS-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 239000003990 capacitor Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000003507 refrigerant Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- 206010053567 Coagulopathies Diseases 0.000 description 1
- 206010010071 Coma Diseases 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 101100460157 Drosophila melanogaster nenya gene Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000722270 Regulus Species 0.000 description 1
- 244000007853 Sarothamnus scoparius Species 0.000 description 1
- 206010039509 Scab Diseases 0.000 description 1
- XKTUVNRQONVSGB-UHFFFAOYSA-N [C-]#N.N#CC#N Chemical compound [C-]#N.N#CC#N XKTUVNRQONVSGB-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 210000000436 anus Anatomy 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 125000004965 chloroalkyl group Chemical group 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000035602 clotting Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 230000000994 depressogenic effect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- ATADHKWKHYVBTJ-UHFFFAOYSA-N hydron;4-[1-hydroxy-2-(methylamino)ethyl]benzene-1,2-diol;chloride Chemical compound Cl.CNCC(O)C1=CC=C(O)C(O)=C1 ATADHKWKHYVBTJ-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000012716 precipitator Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- FKENQMMABCRJMK-RITPCOANSA-N sulbactam Chemical compound O=S1(=O)C(C)(C)[C@H](C(O)=O)N2C(=O)C[C@H]21 FKENQMMABCRJMK-RITPCOANSA-N 0.000 description 1
- 229960005256 sulbactam Drugs 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/28—Only halogen atoms, e.g. cyanuric chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Treating Waste Gases (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2843381A DE2843381B2 (de) | 1978-10-05 | 1978-10-05 | Verfahren zur Gewinnung von Cyanurchlorid in fester und flüssiger Form |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS219906B2 true CS219906B2 (en) | 1983-03-25 |
Family
ID=6051426
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS796449A CS219906B2 (en) | 1978-10-05 | 1979-09-24 | Method of gaining the cyanurchloride |
Country Status (23)
| Country | Link |
|---|---|
| US (1) | US4245091A (ro) |
| JP (1) | JPS5551074A (ro) |
| AT (1) | AT364370B (ro) |
| BE (1) | BE879181A (ro) |
| BR (1) | BR7905299A (ro) |
| CA (1) | CA1105018A (ro) |
| CH (1) | CH641787A5 (ro) |
| CS (1) | CS219906B2 (ro) |
| DD (1) | DD146183A5 (ro) |
| DE (1) | DE2843381B2 (ro) |
| ES (1) | ES481918A1 (ro) |
| FR (1) | FR2439776A1 (ro) |
| GB (1) | GB2035305B (ro) |
| HU (1) | HU182945B (ro) |
| IL (1) | IL58263A (ro) |
| IN (1) | IN153152B (ro) |
| IT (1) | IT1119120B (ro) |
| MX (1) | MX152745A (ro) |
| NL (1) | NL7904980A (ro) |
| RO (1) | RO77778A (ro) |
| SE (1) | SE446000B (ro) |
| YU (1) | YU40221B (ro) |
| ZA (1) | ZA794823B (ro) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10123072B4 (de) * | 2001-05-11 | 2004-12-30 | Degussa Ag | Vorrichtung zur Aufreinigung von Cyanurchlorid |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE599669A (fr) * | 1960-02-02 | 1961-05-16 | Lonza Usines Electr Et Chim Sa | Procédé de purification du chlorure de cyanuryle par distillation |
| US3256070A (en) * | 1960-10-12 | 1966-06-14 | Geigy Chem Corp | Desublimation using a rotating cooling drum containing particulate tumbling and grinding media |
| FR1411816A (fr) * | 1964-08-11 | 1965-09-24 | Electro Chimie Soc D | Procédé d'obtention de chlorure de cyanuryle purifié à partir de mélanges gazeux le contenant |
| GB1095454A (ro) * | 1965-08-21 | |||
| US3539565A (en) * | 1968-01-29 | 1970-11-10 | Geigy Chem Corp | Method for producing a solution of cyanuric chloride from gaseous cyanuric chloride |
| CH534686A (de) * | 1970-02-13 | 1973-03-15 | Ciba Geigy Ag | Kontinuierliches Verfahren zur Herstellung von Cyanurchlorid |
| DD111378A5 (ro) * | 1973-06-27 | 1975-02-12 | ||
| DE2537673C2 (de) * | 1975-08-23 | 1977-09-29 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zur Herstellung von feinteiligem, festem Cyanurchlorid |
-
1978
- 1978-10-05 DE DE2843381A patent/DE2843381B2/de not_active Ceased
-
1979
- 1979-06-12 YU YU1376/76A patent/YU40221B/xx unknown
- 1979-06-26 ES ES481918A patent/ES481918A1/es not_active Expired
- 1979-06-26 NL NL7904980A patent/NL7904980A/nl not_active Application Discontinuation
- 1979-08-01 MX MX178732A patent/MX152745A/es unknown
- 1979-08-06 IT IT68619/79A patent/IT1119120B/it active
- 1979-08-17 BR BR7905299A patent/BR7905299A/pt not_active IP Right Cessation
- 1979-08-29 IN IN891/CAL/79A patent/IN153152B/en unknown
- 1979-09-12 ZA ZA00794823A patent/ZA794823B/xx unknown
- 1979-09-18 IL IL58263A patent/IL58263A/xx unknown
- 1979-09-20 DD DD215677A patent/DD146183A5/de not_active IP Right Cessation
- 1979-09-24 CS CS796449A patent/CS219906B2/cs unknown
- 1979-09-25 US US06/078,832 patent/US4245091A/en not_active Expired - Lifetime
- 1979-10-01 GB GB7933913A patent/GB2035305B/en not_active Expired
- 1979-10-03 BE BE6/46960A patent/BE879181A/fr not_active IP Right Cessation
- 1979-10-04 SE SE7908236A patent/SE446000B/sv not_active IP Right Cessation
- 1979-10-04 AT AT0648879A patent/AT364370B/de not_active IP Right Cessation
- 1979-10-04 CA CA336,982A patent/CA1105018A/en not_active Expired
- 1979-10-04 HU HU79DE1016A patent/HU182945B/hu not_active IP Right Cessation
- 1979-10-04 CH CH896479A patent/CH641787A5/de not_active IP Right Cessation
- 1979-10-05 JP JP12810079A patent/JPS5551074A/ja active Granted
- 1979-10-05 RO RO7998862A patent/RO77778A/ro unknown
- 1979-10-05 FR FR7924909A patent/FR2439776A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| IT7968619A0 (it) | 1979-08-06 |
| BR7905299A (pt) | 1980-04-29 |
| IL58263A (en) | 1982-12-31 |
| GB2035305A (en) | 1980-06-18 |
| IT1119120B (it) | 1986-03-03 |
| GB2035305B (en) | 1983-03-23 |
| ATA648879A (de) | 1981-03-15 |
| CH641787A5 (de) | 1984-03-15 |
| HU182945B (en) | 1984-03-28 |
| DE2843381B2 (de) | 1980-07-10 |
| AT364370B (de) | 1981-10-12 |
| BE879181A (fr) | 1980-04-03 |
| DE2843381A1 (de) | 1980-04-17 |
| ES481918A1 (es) | 1980-02-16 |
| RO77778A (ro) | 1982-02-26 |
| FR2439776B1 (ro) | 1983-04-01 |
| SE446000B (sv) | 1986-08-04 |
| MX152745A (es) | 1985-11-07 |
| JPS5551074A (en) | 1980-04-14 |
| SE7908236L (sv) | 1980-04-06 |
| DD146183A5 (de) | 1981-01-28 |
| CA1105018A (en) | 1981-07-14 |
| JPH0127067B2 (ro) | 1989-05-26 |
| FR2439776A1 (fr) | 1980-05-23 |
| YU40221B (en) | 1985-08-31 |
| IL58263A0 (en) | 1979-12-30 |
| ZA794823B (en) | 1981-01-28 |
| YU137679A (en) | 1982-08-31 |
| NL7904980A (nl) | 1980-04-09 |
| US4245091A (en) | 1981-01-13 |
| IN153152B (ro) | 1984-06-09 |
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