CN2552934Y - Pressure circulating ultra-high pressure cell rupture device - Google Patents

Pressure circulating ultra-high pressure cell rupture device Download PDF

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Publication number
CN2552934Y
CN2552934Y CN02238058U CN02238058U CN2552934Y CN 2552934 Y CN2552934 Y CN 2552934Y CN 02238058 U CN02238058 U CN 02238058U CN 02238058 U CN02238058 U CN 02238058U CN 2552934 Y CN2552934 Y CN 2552934Y
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piston
pressure
oil cylinder
roller
ultra
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Expired - Fee Related
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CN02238058U
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Chinese (zh)
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苏奎荣
苏茂华
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Abstract

The utility model relates to a pressure circulation ultra high pressure cell explosion device for controlling an ultra high pressure liquid medium to release the pressure for an instant. The utility model mainly comprises an ultra high pressure instantaneous release device comprising a vessel body, a pressure sensor, a piston, a liquid control one-way valve, a pin roll, a support, a bedplate, a bumper, a secure cover, an L-shaped lever, a roller and a portal shaped buckle, and an automatic pressure circulation system comprising control cylinder A, B, C and D. The utility model can solve the technical problem that the ultra high pressure below hundreds of MPa is securely released for an instant of hundreds of microseconds, and also design the pressure circulation system, thus the utility model can routinize and repeatedly pressurize to explode. The device is used for the cell wall breaking of the raw material of a Chinese herbal medicine, and the physical grinding degree of the raw material can be directly improved. In addition, the device also can be applied to the cosmetics, health food, gene engineering and inactive microorganism fields and other fields.

Description

Pressure cycling ultra-high voltage cell blasting assembly
Technical field
The utility model relates to a kind of cell wall breaking device, belongs to the processing or the microorganism deactivated equipment of herbal medicine.
Background technology
Chinese medicine is the big rarity of one in Chinese nation's wealth.The working method of present domestic herbal medicine mainly contains traditional comminuting method, immersion adds decocting and endures method and supercritical CO 2 high pressure extraction method.The method of pulverizing medicine material can not make its cell wall rupture, and the effective ingredient of medicine is difficult for being absorbed by the body; Add decocting and endure and to make the part effective ingredient see through cell walls to infiltrate in the soup, but decocting under the high temperature can make some effective ingredient evaporations, sex change or decomposition; Domestic in recent years become in many factory's utilization commonplace be a kind of method of supercritical CO 2 high pressure extraction medicine, owing to be subjected to the restriction of technology and equipment condition, can only and carry out pressure release in the several seconds at tens MPa pressure, it is to penetrate cell walls and dissolve in the liquid carbonic acid gas in order to have improved raw material Chinese traditional medicine effective ingredient that circulation increases pressure release, and the cell walls breakage rate of raw material is extremely low.Because fracturing cell walls is refined patent medicine by these general traditional methods effectively, very big, the famousr and precious medicinal material of effective medicinal component waste in the raw material is subjected to the restriction of natural resource, and loss is just bigger.In medical field, certain micro-organisms inactivation in the blood products there is particular requirement, also need a kind of low cost method.In other field, urge old, food sterilizing, device sterilization etc. all to need the present technique method of high efficient and reliable, easy cheapness as extracting genetic stew, drinks.
Summary of the invention
The utility model is that process object (medicine material, blood products etc.) is placed ultra high pressure liquid medium up to 400Mpa (commonly used have pure water), at a terrific speed the pressure abrupt release of ultra high pressure liquid medium is fallen through after the pressurize of appropriate time, make inside and outside huge pressure reduction, the fried breaking cell wall of producing of cell in the object; The automatic pressure recycle system of design makes the explosion of cell walls more thoroughly reliable.This is a kind of cell physics blasting gear, is mainly used in and fully extracts useful composition, fields such as destroy microorganisms coating kill virus and bacterium behind the herbal medicine starting material cell wall breaking.
The utility model has designed a pressure abrupt release device and pressure automatic circulating system for achieving the above object, the purpose of the explosion cell walls of having realized pressurizeing repeatedly.Concrete structure and principle are: the kettle that can bear the ultra-high voltage reaction that adopts a superior alloy steel to make, kettle is installed on the standoff platen, a ultra high pressure liquid medium pressurization mouth and a treatment solution discharge port are arranged at the kettle bottom, the kettle middle part is provided with pressure transmitter and is used for measuring and controlling the still internal pressure, kettle top is added with a piston that is tightly connected, the piston upper end that can move along the still chamber is processed to the inclined-plane, beveled top end is pushed down last roller by a planer-type button, two arms of planer-type button handle extend through platen downwards, be located by connecting on by bearing pin on the support on platen lower kettle both sides, the planer-type button is swinging around bearing pin, the planer-type button was having born huge pressure in the still, because can be unmovable by the bearing pin lock piston after roller was pushed down piston.After putting into the liquid or effective object that is mixed with process object in the reactor, by programme controlled hydraulic work system, at first added relief cover (the steel lid of buffer substance is housed) and gone out, just can inject ultra high pressure liquid medium (generally using pure water) after covering piston and buckling roller to prevent the piston behind the pressurized.When super-pressure pump injects the ultra high pressure liquid medium in still, after making the interior liquid pressure of still reach preset value and keep an appropriate time, program control hydraulic efficiency system adds an external force again makes the planer-type button angle of skew, when the planer-type button can not be pushed down piston effectively to last roller, pressure powerful in the still has produced a bigger transverse thrust by inclined-plane, piston upper end pair roller, fast crossbeam is pushed on one side, lose the rapid upper punch of external force equilibrated piston, the pressure that makes the intravital ultra high pressure liquid medium of still becomes negative pressure in a few microsecond moment suddenly from the ultra-high voltage of hundreds of MPa.
The drastic change of still internal pressure makes the cell of process object or microorganism coating that explosion for the first time take place.In the time of need pressurizeing once more by predefined cycle index, at first open hydraulic control one-way valve, to be that the unnecessary liquid that produces when pressurizeing injection ultra high pressure liquid medium is discharged in the still, hoist cylinder pushes back original position to the piston that rushes to, and swinging to planer-type button on one side setting upright, roller has been pushed down piston tip again again, close hydraulic control one-way valve again, just can inject the ultra high pressure liquid medium once more this moment in still, realize explosion next time, circulates till the cycle index of setting is finished with this.The object of handling well can be discharged from the discharge port of opening valve, also can open the relief cover on the kettle, mentions piston and takes out process object from kettle.
The utility model compared with prior art, make the field at Chinese patent medicine, because decompression rate has improved 2 to 3 orders of magnitude, can be at normal temperatures abundant explosion cell walls, thereby significantly improved the ability of abundant extraction herbal medicine effective ingredient, having easier, economic, energy-conservation, advantage fast, is the once leap of Chinese medicine abstraction technique; In microorganism deactivated Application Areas, also can receive good effect, the virus killing sterilization is reliable, and expense is cheap.This device still is the effective means that biotechnology extracts genetic stew.
Description of drawings
Fig. 1 is a structural representation of the present utility model: mainly buckled 12 and control oil cylinder A, B, C, D by kettle 1, pressure transmitter 2, piston 3, hydraulic control one-way valve 4, bearing pin 5, support 6, platen 7, cushion plate 8, relief cover 9, L type lever 10, roller 11, planer-type.
Fig. 2 is piston 3 synoptic diagram, and three convex shoulders play safety effect.
Fig. 3 is the planer-type button 12 and the bearing pin 5 of roller 11 on the support 6, the swing synoptic diagram under oil cylinder C effect.
Fig. 4 is that oil cylinder A control relief cover 9 rotates 60 degree, prevents the safety effect synoptic diagram that piston 3 is gone out.
Fig. 5 is a pressure cycling hydraulic efficiency system synoptic diagram of the present utility model: mainly carry out time variable control by one group of magnetic valve.
Oil cylinder A is the switch oil cylinder of relief cover;
Oil cylinder B pushes the oil cylinder that L type lever is pushed roller open;
Oil cylinder C buckles the oil cylinder of setting upright together with roller swinging to planer-type on one side when carrying out pressure cycling;
Oil cylinder D is that piston promotes and puts into and use oil cylinder.
Embodiment
Below in conjunction with description of drawings pressure cycling ultra-high voltage cell blasting assembly embodiment:
Kettle 1 is fixed on the platen 7, the opening and the piston 3 on the top, still chamber in the kettle 1 are tightly connected, piston 3 tops are processed to the inclined-plane, the top on inclined-plane can be pushed down the roller 11 on 12 by the planer-type button, the planer-type button extends through platen 7 to 12 two arms and is connected with two supports 6 of platen 7 lower kettles 1 two sides, and be positioned at movingly on the bracket holes by bearing pin 5, the planer-type button drives rollers 11 to 12 can be around bearing pin 5 swings.
During work, process object (raw material) is put into kettle 1, to be lifted at piston 3 on one side by oil cylinder D and put into the still chamber from the opening part on kettle 1 top, oil cylinder A forwards relief cover 9 to safety position, relief cover 9 and cushion plate 8 can stop effectively that piston 3 goes out from kettle 1, oil cylinder C sinciput planer-type is buckled the arm 12, set upright being poured on roller 11 on one side, make roller 11 push down piston 3 effectively, the pressurization mouth by kettle 1 bottom injects the still chamber with high-pressure pump with the ultra high pressure liquid medium.
After pressure transmitter 2 records the still internal pressure and has reached predefined force value, close high-pressure pump earlier, keep after the still internal pressure hydraulic control system task more on schedule, at first go up top L type lever 10 and promote roller 11 by oil cylinder B, just can not push down piston 3 effectively after very little angle of roller 11 skews, immense pressure in the kettle 1 has produced a bigger transverse thrust by piston 3 upper inclined surface again to the roller 11 that is offset, roller 11 is pushed to 12 on one side fast together with the planer-type button, lose external force equilibrated piston 3 rapid upper punches, make the pressure of the ultra high pressure liquid medium of the intravital hundreds of MPa of still become negative pressure in a few microsecond moment.
The drastic change of still internal pressure makes the cell of process object or microorganism coating that explosion for the first time take place.In the time of need pressurizeing once more by predefined cycle index, at first open hydraulic control one-way valve 4, to be that the unnecessary liquid that produces when pressurizeing injection ultra high pressure liquid medium is discharged in the still, hoist cylinder D pushes back original position to the piston that rushes to, by oil cylinder C the planer-type of swinging to one side is buckled again and set upright 12, roller 11 has been pushed down the top of piston 3 again, close hydraulic control one-way valve again, just can inject the ultra high pressure liquid medium once more this moment in still, realize explosion next time, circulate till the cycle index of setting is finished with this.
Finish pressure cycling, after confirming to have reverted to normal pressure in the kettlies 1 by pressure transmitter 2, can the object of handling well be discharged, also can open relief cover 9 on the kettle 1 by oil cylinder A from the discharge port of opening valve, mention piston 3 by oil cylinder D, take out process object from kettle 1 top.

Claims (4)

1. pressure cycling ultra-high voltage cell blasting assembly, on the kettle of making by superior alloy steel that can bear ultra-high voltage reaction pressure transmitter, piston, hydraulic control one-way valve, bearing pin, support, platen, cushion plate, relief cover, L type lever, roller and planer-type are installed and buckle handle, the oil cylinder A of solenoid control, oil cylinder B, oil cylinder C and oil cylinder D.It is characterized in that: rack-mount planer-type button is swung around bearing pin driving roller, and the control roller resets in order to push down piston under the effect of oil cylinder C, promotes roller and discharge the piston of being pressed under the effect of oil cylinder B.
2. pressure cycling ultra-high voltage cell blasting assembly according to claim 1, it is characterized in that: the piston tip that is tightly connected with kettle is processed to the Duckbill type inclined-plane, and the major axis of beveled top end sleeve configuration platform is parallel with the roller axis.Oil cylinder B buckles passing certain distance coupled planer-type by L type lever pushing roller, drive support and put an angle around bearing pin, when having huge pressure to promote the piston upper punch in the still chamber, the ramp effect of piston tip produces a bigger thrust on roller, make the related planer-type button of roller swinging to fast on one side, piston loses the without hindrance upper punch of outer force balance, and pressure huge in the still chamber is produced onepull by abrupt release.
3. pressure cycling ultra-high voltage cell blasting assembly according to claim 1 is characterized in that: there is the convex shoulder of three five equilibriums at the piston middle part, and the convex ridge groove of three corresponding piston convex shoulders is also arranged on the relief cover, and relief cover convex ridge inboard also is added with cushion plate.Under the lift action of oil cylinder D, piston can be put into the still chamber from the position of relief cover correspondence, and after oil cylinder A promoted relief cover rotation sextant, the convex ridge on the relief cover is the convex shoulder of corresponding upper piston just in time, and relief cover is in safety position.As lose external force equilibrated piston upper punch, because relief cover convex ridge and cushion plate be to the effect of piston convex shoulder, piston can not gone out the still chamber.
4. pressure cycling ultra-high voltage cell blasting assembly according to claim 1 is characterized in that: after the pressure transmitter that kettle is installed records the still cavity pressure and reaches preset value, by solenoid control oil cylinder B work, produce onepull.The unnecessary ultra high pressure liquid medium that will inject when hydraulic control one-way valve will boost in the still chamber is discharged, and the roller of being set upright behind the piston return of upper punch is pushed down once more, promptly begins to pressurize explosion next time, thereby realizes pressure cycling.
CN02238058U 2002-07-01 2002-07-01 Pressure circulating ultra-high pressure cell rupture device Expired - Fee Related CN2552934Y (en)

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CN02238058U CN2552934Y (en) 2002-07-01 2002-07-01 Pressure circulating ultra-high pressure cell rupture device

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Application Number Priority Date Filing Date Title
CN02238058U CN2552934Y (en) 2002-07-01 2002-07-01 Pressure circulating ultra-high pressure cell rupture device

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104435007A (en) * 2014-12-04 2015-03-25 东北师范大学 Method for breaking ganoderma spore wall rapidly and efficiently
CN109082364A (en) * 2018-08-01 2018-12-25 东南大学 A kind of micro-structural device of physical method clasmatosis and its clasmatosis and processing method
CN111701271A (en) * 2020-04-29 2020-09-25 漳州职业技术学院 Cucumber polyphenol extraction device and preparation method of cucumber polyphenol magnesium complex
CN111821718A (en) * 2020-04-29 2020-10-27 漳州职业技术学院 Magnolia liliiflora polysaccharide strontium antiallergic agent production line and preparation method thereof
CN111921224A (en) * 2020-06-12 2020-11-13 漳州职业技术学院 Nitrite scavenging additive production line and preparation method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104435007A (en) * 2014-12-04 2015-03-25 东北师范大学 Method for breaking ganoderma spore wall rapidly and efficiently
CN109082364A (en) * 2018-08-01 2018-12-25 东南大学 A kind of micro-structural device of physical method clasmatosis and its clasmatosis and processing method
CN109082364B (en) * 2018-08-01 2019-07-30 东南大学 A kind of micro-structural device of physical method clasmatosis and its clasmatosis and processing method
CN111701271A (en) * 2020-04-29 2020-09-25 漳州职业技术学院 Cucumber polyphenol extraction device and preparation method of cucumber polyphenol magnesium complex
CN111821718A (en) * 2020-04-29 2020-10-27 漳州职业技术学院 Magnolia liliiflora polysaccharide strontium antiallergic agent production line and preparation method thereof
CN111921224A (en) * 2020-06-12 2020-11-13 漳州职业技术学院 Nitrite scavenging additive production line and preparation method thereof
CN111921224B (en) * 2020-06-12 2021-10-29 漳州职业技术学院 Nitrite scavenging additive production line and preparation method thereof

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