CN1935751A - Microelement foliage fertilizer containing bamboo vinegar and its production method - Google Patents
Microelement foliage fertilizer containing bamboo vinegar and its production method Download PDFInfo
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- CN1935751A CN1935751A CNA2006100538166A CN200610053816A CN1935751A CN 1935751 A CN1935751 A CN 1935751A CN A2006100538166 A CNA2006100538166 A CN A2006100538166A CN 200610053816 A CN200610053816 A CN 200610053816A CN 1935751 A CN1935751 A CN 1935751A
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- Prior art keywords
- bamboo vinegar
- salt
- liquid
- foliage fertilizer
- vinegar liquid
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- 239000000052 vinegar Substances 0.000 title claims abstract description 64
- 235000021419 vinegar Nutrition 0.000 title claims abstract description 64
- 235000017166 Bambusa arundinacea Nutrition 0.000 title claims abstract description 61
- 235000017491 Bambusa tulda Nutrition 0.000 title claims abstract description 61
- 241001330002 Bambuseae Species 0.000 title claims abstract description 61
- 235000015334 Phyllostachys viridis Nutrition 0.000 title claims abstract description 61
- 239000011425 bamboo Substances 0.000 title claims abstract description 61
- 239000003337 fertilizer Substances 0.000 title claims abstract description 38
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000011573 trace mineral Substances 0.000 claims abstract description 43
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 229910052796 boron Inorganic materials 0.000 claims abstract description 10
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 9
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 9
- 150000002696 manganese Chemical class 0.000 claims abstract description 9
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 8
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000011733 molybdenum Substances 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 62
- 239000000463 material Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 239000003352 sequestering agent Substances 0.000 claims description 9
- 150000003751 zinc Chemical class 0.000 claims description 8
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical group OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 7
- 238000007664 blowing Methods 0.000 claims description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 6
- 229910000365 copper sulfate Inorganic materials 0.000 claims description 5
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 5
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 5
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical compound [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 claims description 5
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims description 4
- 239000013078 crystal Substances 0.000 claims description 4
- 239000011790 ferrous sulphate Substances 0.000 claims description 4
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 4
- -1 polyoxyethylene Polymers 0.000 claims description 4
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 4
- 244000215068 Acacia senegal Species 0.000 claims description 3
- 235000006491 Acacia senegal Nutrition 0.000 claims description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 3
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
- 239000011609 ammonium molybdate Substances 0.000 claims description 3
- 235000018660 ammonium molybdate Nutrition 0.000 claims description 3
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims description 3
- 229940010552 ammonium molybdate Drugs 0.000 claims description 3
- IMBKASBLAKCLEM-UHFFFAOYSA-L ferrous ammonium sulfate (anhydrous) Chemical compound [NH4+].[NH4+].[Fe+2].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O IMBKASBLAKCLEM-UHFFFAOYSA-L 0.000 claims description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 claims description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 3
- RZLVQBNCHSJZPX-UHFFFAOYSA-L zinc sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Zn+2].[O-]S([O-])(=O)=O RZLVQBNCHSJZPX-UHFFFAOYSA-L 0.000 claims description 3
- 244000144730 Amygdalus persica Species 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- 229910021538 borax Inorganic materials 0.000 claims description 2
- NCFDZIXJQHJTKI-UHFFFAOYSA-N boric acid;molybdenum Chemical compound [Mo].OB(O)O NCFDZIXJQHJTKI-UHFFFAOYSA-N 0.000 claims description 2
- 229960003280 cupric chloride Drugs 0.000 claims description 2
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 claims description 2
- CNFDGXZLMLFIJV-UHFFFAOYSA-L manganese(II) chloride tetrahydrate Chemical compound O.O.O.O.[Cl-].[Cl-].[Mn+2] CNFDGXZLMLFIJV-UHFFFAOYSA-L 0.000 claims description 2
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims description 2
- VLAPMBHFAWRUQP-UHFFFAOYSA-L molybdic acid Chemical compound O[Mo](O)(=O)=O VLAPMBHFAWRUQP-UHFFFAOYSA-L 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims description 2
- 239000004328 sodium tetraborate Substances 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 239000011592 zinc chloride Substances 0.000 claims description 2
- 235000005074 zinc chloride Nutrition 0.000 claims description 2
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 2
- 229960001763 zinc sulfate Drugs 0.000 claims description 2
- 235000013399 edible fruits Nutrition 0.000 abstract description 9
- 238000001816 cooling Methods 0.000 abstract description 2
- 238000007599 discharging Methods 0.000 abstract 3
- 238000002156 mixing Methods 0.000 abstract 3
- 239000002738 chelating agent Substances 0.000 abstract 1
- 150000001879 copper Chemical class 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- 239000007921 spray Substances 0.000 description 14
- 239000000203 mixture Substances 0.000 description 6
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 230000012010 growth Effects 0.000 description 4
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 4
- 235000009754 Vitis X bourquina Nutrition 0.000 description 3
- 235000012333 Vitis X labruscana Nutrition 0.000 description 3
- 240000006365 Vitis vinifera Species 0.000 description 3
- 235000014787 Vitis vinifera Nutrition 0.000 description 3
- 244000045947 parasite Species 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 235000007516 Chrysanthemum Nutrition 0.000 description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 2
- 241000220324 Pyrus Species 0.000 description 2
- 150000001299 aldehydes Chemical class 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000035584 blastogenesis Effects 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 239000011785 micronutrient Substances 0.000 description 2
- 235000013369 micronutrients Nutrition 0.000 description 2
- 235000021017 pears Nutrition 0.000 description 2
- 230000008635 plant growth Effects 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 230000002269 spontaneous effect Effects 0.000 description 2
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- ALKWJXWZUTYERW-UHFFFAOYSA-L O.O.O.O.[Mn](=O)(Cl)Cl Chemical class O.O.O.O.[Mn](=O)(Cl)Cl ALKWJXWZUTYERW-UHFFFAOYSA-L 0.000 description 1
- 102000019197 Superoxide Dismutase Human genes 0.000 description 1
- 108010012715 Superoxide dismutase Proteins 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 241000219094 Vitaceae Species 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 235000010419 agar Nutrition 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 230000000507 anthelmentic effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- BEGBSFPALGFMJI-UHFFFAOYSA-N ethene;sodium Chemical group [Na].C=C BEGBSFPALGFMJI-UHFFFAOYSA-N 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 230000035784 germination Effects 0.000 description 1
- 235000021021 grapes Nutrition 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N hydrochloric acid Substances Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000005082 stem growth Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 235000009529 zinc sulphate Nutrition 0.000 description 1
Landscapes
- Fertilizers (AREA)
Abstract
The invention is a bamboo vinegar liquor-containing trace element leaf-surface fertilizer, mixed of at least two ones of ferrous salt 2-20 weight shares, copper salt 2-20 weight shares, manganese salt 1-10 weight shares, boron 2-40 weight shares, and molybdenum 0.2-2 weight shares, and enough dissolving bamboo vinegar raw liquor; in production, firstly adding bamboo vinegar raw liquor into a reaction kettle, then adding the selected trace element raw materials into the reaction kettle one by one, and blending fully in the whole course, dissolving, discharging and barrelling to make it, or not discharging but adding in chelating agent, fully blending and completely dissolving, heating the reaction kettle to 70-90 deg.C, adding in film forming agent, fully blending and completely dissolving, cooling to normal temperature, discharging and barrelling to make it. As using it, adding in water and diluting by 1000-4000 times, spraying on leaves of crops, fruit trees, etc.
Description
Technical field
The present invention relates to a kind of microelement foliage fertilizer and production method thereof that crop is had the bamboo vinegar liquid that promotes growth, antibacterial, expelling parasite, fertilizer efficiency function.
Background technology
Bamboo vinegar liquid has various chemical components, and organic acid wherein, ketone, aldehydes, aldehydes matter itself just have antibacterial and anthelmintic action; The Polyphenols thing content of bamboo vinegar liquid is abundant, the superoxide dismutase activity height, and good in oxidation resistance promotes useful microbial growth in the soil, favourable root of the crop, stem growth, increasing both production and income improves the mouthfeel and the local flavor of fruit and vegetable; Short molten, short osmosis that ketone in the bamboo vinegar liquid, alcohols thing have.Bamboo vinegar liquid and trace element are organically combined, and each brings into play its strong point, produces a kind of foliage fertilizer, has its original realistic meaning.
CN1793066A discloses " process for competition coordination producing of high concentration trace elements leaf fertilizer " of Nanjing soil institute of the Chinese Academy of Sciences, on high density, process for competition coordination producing, give people with useful inspiration, but this method is with water as solvent, do not conform to bamboo vinegar liquid, can not save use cost with promoting growth, antibacterial, expelling parasite, fertilizer efficiency function synthesized in one.CN1545884A discloses Mr.'s Yang Guoting " wooden vinegar multi-effect plant growth promotor and preparation method thereof " patented technology, it is the three major fertilizer of using always, a kind of general fertilizer that materials such as trace element, emulsifying agent, water mix, but but the foliar spray root is irritated and seed soaking, based on key element fertilizer commonly used, the trace element total amount have only 〉=3%, index is on the low side.
By retrieval and market survey, find that as yet the simple microelement foliage fertilizer that contains bamboo vinegar liquid comes out, do not see that also relevant data delivers.
Summary of the invention
The objective of the invention is above-mentioned deficiency at prior art, provide a kind of include bamboo vinegar liquid, crop had promote growth, antibacterial, desinsection, foliage fertilizer and production method thereof the fertilizer efficiency function, that micronutrient levels is high.
The measure that realizes above-mentioned purpose is: it is formed by following raw materials according and weight part proportioning thereof: in 2-20 part molysite, 2-20 part mantoquita, 1-10 part manganese salt, 2-20 part zinc salt, 2-40 part boron, the 0.2-2 part molybdenum at least two kinds, and be enough to make the raw liquid of bamboo vinegar of its dissolved amount.The preferred version of raw material and weight part proportioning thereof is: in 4-10 part molysite, 4-10 part mantoquita, 2-6 part manganese salt, 4-10 part zinc salt, 5-20 part boron, the 0.3-1 part molybdenum at least two kinds, and the raw liquid of bamboo vinegar that is enough to make its dissolved amount.The most preferably scheme of raw material and weight part proportioning thereof is: 6-8 part molysite, 5-6 part mantoquita, 3-5 part manganese salt, 5-7 part zinc salt, 6-15 part boron, 0.4-0.6 part molybdenum, and be enough to make the raw liquid of bamboo vinegar of its dissolved amount.Said molysite is ferrous sulfate, iron protochloride, Iron nitrate, with at least a in the ferrous sulfate of two crystal water, the ferrous ammonium sulphate; Mantoquita is at least a in copper sulfate, the copper sulfate with five crystal water, cupric nitrate, the cupric chloride; Manganese salt is at least a in manganous sulfate, Manganous chloride tetrahydrate, the manganous nitrate; Zinc salt is at least a in zinc sulfate, Zinc Sulphate Heptahydrate, zinc nitrate, the zinc chloride; Boron picks up from borax and/or boric acid; Molybdenum element picks up from molybdic acid, Sodium orthomolybdate, ammonium molybdate at least a.Also be furnished with the membrane-forming agent of 0.5-10 weight part and/or the sequestrant of 1-5 weight part in the raw material.Said membrane-forming agent is at least a in polyvinyl alcohol, polyoxyethylene glycol, Sudan Gum-arabic, Zulkovsky starch, the peach gum powder; Said sequestrant is EDTA and/or EDTA-Na (being ethylenediamine tetraacetic acid (EDTA) and/or sodium ethylene diamine tetracetate).
The above-mentioned production method that contains the microelement foliage fertilizer of bamboo vinegar liquid follows these steps to carry out:
(1) will be enough to make the raw liquid of bamboo vinegar of at least two kinds of selected material dissolution amounts to add in the reactor;
(2) add the trace element materials of selecting for use one by one, whole process fully stirs, and treats to add a kind of raw material in back again after last raw material fully dissolves;
(3) dissolving is finished, the blowing barreled or blowing not, carry out subsequent step again:
(4) sequestrant of adding 1-5 weight part fully stirs, and treats to dissolve fully;
(5) reactor is heated to 70-90 ℃, adds 0.5-10 weight part membrane-forming agent again, is stirred well to dissolving fully;
(6) be cooled to normal temperature, the blowing barreled.
With the foliage fertilizer that aforesaid method makes, trace element concentration height, spray and to be diluted with water to 1000-4000 before the blade face and can to use after doubly.
The invention has the beneficial effects as follows: the microelement foliage fertilizer than commonly used because of containing bamboo vinegar liquid, has not only increased fertilizer efficiency, but also has had the multiple usefulness of antibacterial, expelling parasite, promotion plant growth; The micronutrient levels height; The adding of membrane-forming agent and sequestrant can stick to the blade face with solution effectively, reduces to drip the spontaneous evaporation of becoming estranged, and makes the dispersive of ionic state trace element chelated, has improved the fertile rate of suction on blade face.
Embodiment
The present invention will now be further detailed embodiment: bamboo vinegar liquid is the nucleus in this foliage fertilizer, liquid bamboo vinegar liquid also has the solvent function therein concurrently, so-called " being enough to make the bamboo vinegar liquid of its dissolved amount ", the amount of general requirement raw liquid of bamboo vinegar is selected more than five times of at least two kinds of material quantity sums.Bamboo vinegar liquid also can be after industry dehydration or spontaneous evaporation solid-state, with trace element materials, make foliage fertilizer with water as solvent, then the proportional quantity of solid-state bamboo vinegar liquid is the 48-580 weight part, this mode is dewatered earlier and is afterwards added water, the suspicion of making an unnecessary move is arranged, during energy charge, poor practicability does not generally adopt.
The main component of grass vinegar liquid, wood vinegar and bamboo vinegar liquid and approaching to the usefulness of crop, the above two can be thought of as the latter's surrogate.
All embodiment of the present invention are raw material with raw liquid of bamboo vinegar, commercially pure trace element materials, and dilution water is process water or tap water.
Below each raw material and proportioning weight part are listed as into table 1:
(table 1)
Embodiment 1 (raw material and corresponding proportioning weight part in the synopsis 1):
195 parts of raw liquid of bamboo vinegar are added in the reactor, for accelerating dissolution rate and increasing meltage, can be heated to about 40 ℃, insulation, the limit adds 8 parts of Iron nitrates, after the limit is stirred to dissolving, add 5 parts of copper sulfate, add 4 parts of Manganous chloride tetrahydrates after the stirring and dissolving, add 6 parts of zinc nitrates after the stirring and dissolving, treat to add 8 parts of boraxs and 7 parts of boric acid after the stirring and dissolving, add 0.6 part of ammonium molybdate after the stirring and dissolving, add 1 part of EDTA (ethylenediamine tetraacetic acid (EDTA)) after the stirring and dissolving, stirring and dissolving is heated to 70-90 ℃, add 2 parts of polyvinyl alcohol, be stirred to dissolving, cooling, the blowing barreled.
The raw material and the proportioning weight part of correspondence make this foliage fertilizer with embodiment 1 same procedure in embodiment 2,3,4,9, the 10 equal synopsis 1.Wherein embodiment 3 lower value of getting each trace element materials is carried out proportioning, and embodiment 4 capping values, embodiment 1,2 get intermediate value, and embodiment 5,6 upper and lower limits intersect value and carry out proportioning.
Embodiment 5,6 does not add membrane-forming agent and sequestrant, has then saved the twice concerned process steps among the embodiment 1; Embodiment 7,8 has saved each procedure that adds sequestrant and add membrane-forming agent respectively.
Ten embodiment in the table 1, preferred with embodiment 2, embodiment 1 more preferably.Embodiment 1-6 is Fe, Cu, Mn, Zn, the complete neat Formulation Example of six kinds of trace elements of B, Mo, and embodiment 7-10 is two kinds of Formulation Examples to five kinds of trace elements.Still it should be noted that the kind few more (as having only two kinds) of the trace element of proportioning, then should select the low salt of molecular weight (example hydrochloric acid salt) is raw material, and get the weight part higher limit, be beneficial to improve the degree of these two kinds of trace elements, reach 〉=10% requirement, meet the standard of GB/T17420-1998 about trace elements leaf fertilizer.
In the table 1 because of placed restrictions on by length, 2 aqueous ferrous sulfates in the trace element materials, 5 brochantites, 7 water zinc sulphates, ferrous ammonium sulphate; Polyoxyethylene glycol in the membrane-forming agent, Sudan Gum-arabic, agar, dextrin etc. are not listed in one by one, can only list to illustrative a part in, and the public can understand with drawing inferences about other cases from one instance and gets final product.Also because of same cause, in embodiment 7-10, to the proportioning of two kinds, three kinds, four kinds, five kinds trace elements, each only lists a kind of example, and no longer permutation and combination goes out many examples, understands to get final product, and does not give unnecessary details for this reason.
After this foliage fertilizer is made, during use, be sprayed on the crop blade face behind the dilute with water or prepare fertile interpolation fertilizer as three elements.
Below, the field test results of this foliage fertilizer is reported as follows:
The proportioning of the applicant embodiment 1,2 in Anji County, Jiande City, the Huzhou City in Zhejiang Province carry out these foliage fertilizers to chrysanthemum pears, tealeaves, grape is respectively sprayed experiment, and add trace element and contrast with independent water spray, spray bamboo vinegar liquid, water spray, its result is listed as into table 2, table 3, table 4 respectively.
1. the experimental data spray date of chrysanthemum pears: six to July, 2500 times of the extension rates in mid-term of bearing fruit, every spray in 8 days once, spray twice (95% confidence region) altogether
(table 2)
| Composition/index | Single fruit weight (jin) | Output (jin/strain) |
| Water | 0.42±0.04 | 40±4 |
| Bamboo vinegar liquid (stoste) | 0.48±0.07 | 49±6 |
| Water+trace element | 0.51±0.09 | 52±5 |
| Bamboo vinegar liquid (stoste)+trace element (example 1) | 0.61±0.10 | 60±6 |
| Bamboo vinegar liquid (stoste)+trace element (example 2) | 0.62±0.08 | 63±7 |
| Bamboo vinegar liquid (stoste)+trace element (example 3) | 0.63±0.09 | 65±6 |
| Bamboo vinegar liquid (stoste)+trace element (example 4) | 0.64±0.11 | 64±6 |
| Bamboo vinegar liquid (stoste)+trace element (example 5) | 0.67±0.13 | 69±7 |
| Bamboo vinegar liquid (stoste)+trace element (example 6) | 0.66±0.09 | 67±5 |
| This liquid fertilizer test mean value | 0.64±0.10 | 65±6 |
2. the experimental data spray date of tealeaves: 1000 times of July summer bud germination period extension rates, every spray in 8 days once, spray twice by (95% confidence region) (table 3) altogether
| Composition/index | The long speed (centimetre/day) of blastogenesis | Bud density (individual/square metre) | Output (gram/square metre) |
| Water | 0.18±0.01 | ?22±2 | ?20±1 |
| Bamboo vinegar liquid (stoste) | 0.19±0.02 | ?23±3 | ?22±2 |
| Water+trace element | 0.20±0.02 | ?26±4 | ?25±4 |
| Bamboo vinegar liquid (stoste)+trace element (example 1) | 0.24±0.04 | ?28±3 | ?31±3 |
| Bamboo vinegar liquid (stoste)+trace element (example 2) | 0.24±0.03 | ?29±6 | ?33±3 |
| Bamboo vinegar liquid (stoste)+trace element (example 3) | 0.26±0.04 | ?31±5 | ?34±5 |
| Bamboo vinegar liquid (stoste)+trace element (example 4) | 0.25±0.05 | ?30±4 | ?35±4 |
| Bamboo vinegar liquid (stoste)+trace element (example 5) | 0.28±0.05 | ?33±5 | ?37±3 |
| Bamboo vinegar liquid (stoste)+trace element (example 6) | 0.27±0.04 | ?32±3 | ?34±4 |
| This liquid fertilizer test mean value | 0.26±0.04 | ?31±4 | ?34±4 |
3. the experimental data spray date of grape: June 1500 times of the extension rates in mid-term of bearing fruit, every spray in 10 days once, spray twice (95% confidence region) test site altogether and pluck and adopt 5 string grapes and carry out following index examination:
(table 4)
| Composition/index | Gross weight (gram) | Decayed fruit (gram) | Intact fruit heavy (gram) | 100-grain weight (gram) | Infected seed (grain) |
| Water | 2100±150 | 220±15 | ?1900±140 | ?700±50 | ?34±4 |
| Bamboo vinegar liquid (stoste) | 2180±160 | 180±11 | ?2000±160 | ?760±60 | ?27±3 |
| Water+trace element | 2230±170 | 120±10 | ?2160±190 | ?810±50 | ?16±2 |
| Bamboo vinegar liquid (stoste)+trace element (example 1) | 2300±160 | 60±4 | ?2200±180 | ?900±70 | ?9±3 |
| Bamboo vinegar liquid (stoste)+trace element (example 2) | 2540±190 | 46±5 | ?2300±220 | ?920±60 | ?7±2 |
| Bamboo vinegar liquid (stoste)+trace element (example 3) | 2580±210 | 48±4 | ?2400±200 | ?940±50 | ?6±2 |
| Bamboo vinegar liquid (stoste)+trace element (example 4) | 2620±200 | 45±6 | ?2450±210 | ?950±40 | ?6±1 |
| Bamboo vinegar liquid (stoste)+trace element (example 5) | 2670±190 | 43±4 | ?2480±190 | ?940±70 | ?5±2 |
| Bamboo vinegar liquid (stoste)+trace element (example 6) | 2680±140 | 42±5 | ?2540±180 | ?930±60 | ?4±1 |
| This liquid fertilizer test mean value | 2565±182 | 47±5 | ?2395±197 | ?930±58 | ?6±2 |
Can find out from table 2: be sprayed with 0.64 ± 0.10 jin, a traditional unit of weight of the single fruit weighted average of six examples of this foliage fertilizer, 0.42～0.51 jin, a traditional unit of weight of weight than control group has notable difference, and the difference that its strain is produced is also very remarkable.
Table 3 reflects the significant difference of the long speed of the blastogenesis of summer tea, bud density, output.
Table 4 except the significant difference of gross weight, the 100-grain weight of explanation grape, from decayed fruit, intact fruit tuple according on antiviral, the fungistatic effect of this foliage fertilizer can be described; Discrepancy Description insecticidal effect from the infected seed number.
Above-mentioned experiment, the confidence level on the biostatistics meaning is measured, and confidence region reaches 95%.
Claims (7)
1, a kind of microelement foliage fertilizer of bamboo vinegar liquid, it is characterized in that forming by following raw materials according and weight part proportioning thereof: in 2-20 part ferrous salt, 2-20 part mantoquita, 1-10 part manganese salt, 2-20 part zinc salt, 2-40 part boron, the 0.2-2 part molybdenum at least two kinds, and be enough to make the raw liquid of bamboo vinegar of its dissolved amount.
2, the microelement foliage fertilizer of bamboo vinegar liquid as claimed in claim 1, the preferred version that it is characterized in that raw material and weight part proportioning thereof is: in 4-10 part ferrous salt, 4-10 part mantoquita, 2-6 part manganese salt, 4-10 part zinc salt, 5-20 part boron, the 0.3-1 part molybdenum at least two kinds, and the raw liquid of bamboo vinegar that is enough to make its dissolved amount.
3, the microelement foliage fertilizer of bamboo vinegar liquid as claimed in claim 1, the most preferably scheme that it is characterized in that raw material and weight part proportioning thereof is: 6-8 part ferrous salt, 5-6 part mantoquita, 3-5 part manganese salt, 5-7 part zinc salt, 6-15 part boron, 0.4-0.6 part molybdenum, and be enough to make the raw liquid of bamboo vinegar of its dissolved amount.
4, as the microelement foliage fertilizer of each described bamboo vinegar liquid among the claim 1-3, it is characterized in that said ferrous salt be ferrous sulfate, iron protochloride, Iron nitrate, with at least a in the ferrous sulfate of two crystal water, the ferrous ammonium sulphate; Mantoquita is at least a in copper sulfate, the copper sulfate with five crystal water, cupric nitrate, the cupric chloride; Manganese salt is at least a in manganous sulfate, Manganous chloride tetrahydrate, the manganous nitrate; Zinc salt is at least a in zinc sulfate, Zinc Sulphate Heptahydrate, zinc nitrate, the zinc chloride; Boron picks up from borax and/or boric acid; Molybdenum element picks up from molybdic acid, Sodium orthomolybdate, ammonium molybdate at least a.
5,, it is characterized in that also being furnished with in the raw material membrane-forming agent of 0.5-10 weight part and/or the sequestrant of 1-5 weight part as the microelement foliage fertilizer of each described bamboo vinegar liquid among the claim 1-3.
6, the microelement foliage fertilizer of bamboo vinegar liquid as claimed in claim 5 is characterized in that said membrane-forming agent is at least a in polyvinyl alcohol, polyoxyethylene glycol, Sudan Gum-arabic, Zulkovsky starch, the peach gum powder; Said sequestrant is EDTA and/or EDTA-Na.
7, a kind of microelement foliage fertilizer production method that contains bamboo vinegar liquid is characterized in that following these steps to produce:
(1) will be enough to make the raw liquid of bamboo vinegar of at least two kinds of selected trace element materials meltages to add in the reactor;
(2) add the trace element materials of selecting for use one by one, whole process fully stirs, and treats to add a kind of raw material in back again after last raw material dissolves fully;
(3) all dissolving is finished, the blowing barreled or blowing not, carry out subsequent step again:
(4) sequestrant of adding 1-5 weight part fully stirs, and treats to dissolve fully;
(5) reactor is heated to 70-90 ℃, adds 0.5-10 weight part membrane-forming agent again, is stirred well to dissolving fully;
(6) be cooled to normal temperature, the blowing barreled.
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