CN1820780A - Method for preparing Fuyankang extract - Google Patents
Method for preparing Fuyankang extract Download PDFInfo
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- CN1820780A CN1820780A CN 200510033261 CN200510033261A CN1820780A CN 1820780 A CN1820780 A CN 1820780A CN 200510033261 CN200510033261 CN 200510033261 CN 200510033261 A CN200510033261 A CN 200510033261A CN 1820780 A CN1820780 A CN 1820780A
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Abstract
The Fuyankang extract is prepared with 12 kinds of Chinese medicinal materials, including phellodendron bark, corydalis tuber, flavescent sophora root, red peony root, glabrous green brier rhizome, burreed rhizome, chinaberry fruit, zedoary, etc. in certain weight proportion. The preparation process includes the following steps: mixing the first mentioned three kinds of Chinese medicinal materials, crushing into 5-20 mesh, wetting with NaHCO3 in 5 %, percolating with 40-85 % concentration alcohol aqua in 9 time volume of the medicine materials, collecting the percolate, decompression concentrating to obtain extractum while recovering alcohol, and crushing to obtain powder; crushing the other 9 kinds of Chinese medicinal materials into 5-20 mesh, percolating with 40-85 % concentration alcohol aqua in 9 time volume of the medicine materials, collecting the percolate, decompression concentrating to obtain extractum while recovering alcohol, and crushing to obtain powder, etc.
Description
Technical field
The present invention is a kind of new preparation technology of famous-brand and high-quality Chinese patent medicine FUYANKANG.
Background technology
FUYANKANG is that the Jilin Prov. Inst. of Chinese Medicine and Chinese Medical Science began from 1978, according to Traditional Chinese medical theory, and the scientific method that utilization is modern, a kind of compound preparation of development.Health ministry approval in 1984 is produced, and two during the last ten years clinically treating on women's adnexitis, the gynecopathy such as pelvic inflammatory disease, receives significant curative effect, and be subjected to patient's favorable comment.
Be monarch drug with rhizoma sparganic, Rhizoma Curcumae in the side, the rhizoma sparganic toil is sweet flat, and the arduous temperature of Rhizoma Curcumae is all returned liver, spleen channel.Rhizoma sparganic removing blood stasis, circulation of qi promoting, removing food stagnancy, pain relieving.Rhizoma Curcumae also has the merit of removing blood stasis, promoting the circulation of QI to relieve pain, every normal and rhizoma sparganic compatibility, and all through vinegar system, the enhancing removing blood stasis is arranged, the effect of promoting the circulation of QI to relieve pain.Minister is with Radix Angelicae Sinensis, Radix Salviae Miltiorrhizae, Radix Paeoniae Rubra, Rhizoma Cyperi.Chinese angelica blood supplementing and blood, the Radix Salviae Miltiorrhizae blood circulation promoting and blood stasis dispelling, Radix Paeoniae Rubra is bitter, and cold has the clots absorbing pain relieving, the merit of cool seroma; The little hardship of Rhizoma Cyperi property is sweet flat, depressed liver-energy dispersing and QI regulating.The auxilliary altogether monarch drug of above-mentioned all ministerial drugs is with the energy of mediate reason blood circulation promoting and blood stasis dispelling circulation of qi promoting.Rhizoma Smilacis Glabrae is sweet light flat, detoxifcation, dehumidifying.Cortex Phellodendri bitter cold, heat clearing away, dampness.Radix Sophorae Flavescentis " main stagnation of QI in chest and abdomen ， mass in the abdomen knot is poly-" (" herbal classic ").Semen Euryales is sweet puckery flat, reinforcing the kindey to control nocturnal emission, spleen reinforcing antidiarrheal.The Fructus Toosendan bitter cold, except that damp and hot, clearing away liver-fire, pain relieving.Rhizoma Corydalis can be invigorated blood circulation, dissipating blood stasis, and circulation of qi promoting, pain relieving with a Fructus Toosendan Sichuan Chinaberry Powder of associating with, has soothing the liver heat clearing away, the merit of promoting blood circulation and stopping pain.Below be adjuvant drug altogether, assist monarch drug one with heat clearing away, detoxifcation, dampness; One with spleen benefiting and strengthen kidney; One with the promoting flow of QI and blood pain relieving.There is blood circulation promoting and blood stasis dispelling full side, and heat-clearing and toxic substances removing consolidates the effect of dehumidifying, is applicable to that hysteromyoma and female chronic inflammation belong to qi depression to blood stasis, retention of damp-heat in the interior, stasis of blood poison knot card person mutually.
Because the taking dose of former preparation is bigger than normal, the patient quite feels inconvenience, and the effective ingredient of medicine is not fully utilized, and its therapeutic effect still can not be satisfactory.
Summary of the invention
The objective of the invention is the extractive technique of application of advanced, essence is proposed active ingredient, dwindles dosage, improves curative effect, makes things convenient for the patient to carry and takes.
The object of the present invention is achieved like this:
The preparation method of Fuyankang extract, comprise and select Radix Paeoniae Rubra for use, Rhizoma Smilacis Glabrae, rhizoma sparganic, Fructus Toosendan, Rhizoma Curcumae, Rhizoma Corydalis, Semen Euryales, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Cyperi, Cortex Phellodendri, Chinese crude drugs such as Radix Salviae Miltiorrhizae are as raw material, its special character is: the raw material weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=3.1～9.1%: 7.2～13.2%: 3.1～9.1%: 3.1～9.1%: 3.1～9.1%: 3.1～9.1%: 7.2～13.2%: 7.2～13.2%: 3.1～9.1%: 1.1～7.1%: 3.1～9.1%: 7.2～13.2%, its preparation method is: at first with the Cortex Phellodendri in the raw material, Rhizoma Corydalis and Radix Sophorae Flavescentis mix and are ground into 5～20 order coarse powder, use 5%NaHCO
3Moistening back extracts effective ingredient with 4～85% ethanol water percolation, collect the percolate of 7～9 times of amounts, after reclaiming ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder, other 9 flavor medical materials mixing also are ground into 5～20 order coarse powder, extract effective ingredient with 40～85% ethanol water percolation, collect the percolate of 7～9 times of amounts, behind the recovery ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder.
According to the present invention, its special character is: its raw material optimum weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=6.1%: 10.2%: 6.1%: 6.1%: 6.1%: 6.1%: 10.2%: 10.2%: 6.1%: 4.1%: 6.1%: 10.2%.
According to the present invention, its special character is: described 12 flavor medical materials all are broken into 5～20 order coarse powder, and Cortex Phellodendri, Rhizoma Corydalis and Radix Sophorae Flavescentis powder are used earlier 5% NaHCO
3Moistening back was flooded 18-36 hour at 20～40 ℃ with alcoholic solution, or was 24 hours, and repercolation extracts; Other nine flavor medicinal material coarse powder were flooded 18-36 hour with alcoholic solution, or after being 24 hours, extracted with the alcoholic solution percolation.
According to the present invention, its special character is: also be included in concentrating under reduced pressure below 80 ℃ and be dried to the dry extract solid.
According to the present invention, its special character is: raw material Radix Paeoniae Rubra can the Radix Paeoniae Alba replaces, and Rhizoma Smilacis Glabrae can Poria, Polyporus replaces, Fructus Toosendan can replace by Cortex Meliae, and Rhizoma Curcumae can replace by Radix Curcumae, and Semen Euryales can replace by Semen Nelumbinis, Rhizoma Cyperi can replace by dried tuber, and Cortex Phellodendri can replace by Rhizoma Coptidis.
According to the present invention, its special character is: granulate with suitable adhesive, add an amount of adjuvant and make tablet and sugar coating or film-coat or hard capsule or pill or granule or soft capsule, every or every in the preparation of making can be 0.20～0.60 gram.
The Fuyankang extract dry powder that the present invention produces is granulated with suitable adhesive, adds an amount of adjuvant and makes tablet and sugar coating or film-coat; Hard capsule; Pill; Granule and soft capsule.These preparations are used for the treatment of the gynaecopathia pelvic inflammatory disease, adnexitis, cervicitis and male's prostatitis.To Radix Paeoniae Rubra to extract compositions such as comprising paeoniflorin, to Rhizoma Smilacis Glabrae to extract active ingredients such as flavonol, flavone, resveratrol, to rhizoma sparganic, Rhizoma Curcumae, Radix Angelicae Sinensis and Rhizoma Cyperi to propose the volatile oil composition, to Rhizoma Corydalis, Radix Sophorae Flavescentis and Cortex Phellodendri to extract the alkaloid composition that is present in these medical materials, to Fructus Toosendan to extract terpenoid, Semen Euryales is comprised steroidal glucoside chemical compound to extract, the chemical substance that Radix Salviae Miltiorrhizae is extracted with other the available above-mentioned solvent that extracts the tanshinone chemical analysis and exist in these medical materials.The present invention selects 40～85% ethanol waters for use, is very beneficial for alcoholic acid recycling.
The specific embodiment
Embodiment 1
The preparation method of Fuyankang extract, comprise and select Radix Paeoniae Rubra for use, Rhizoma Smilacis Glabrae, rhizoma sparganic, Fructus Toosendan, Rhizoma Curcumae, Rhizoma Corydalis, Semen Euryales, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Cyperi, Cortex Phellodendri, Chinese crude drugs such as Radix Salviae Miltiorrhizae are as raw material, its special character is: the raw material weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=3.1%: 7.2%: 3.1%: 3.1%: 3.1%: 3.1%: 7.2%: 7.2%: 3.1%: 1.1%: 3.1%: 7.2%, its preparation method is: at first with the Cortex Phellodendri in the raw material, Rhizoma Corydalis and Radix Sophorae Flavescentis mix and are ground into 5～20 order coarse powder, use 5%NaHCO
3After moistening, in medicinal material coarse powder: the ratio of alcoholic solution (w/v)=1: 9, extract effective ingredient with 40～85% ethanol water percolation, collect the percolate of 7 times of amounts, after reclaiming ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder, other 9 flavor medical materials mix and also to be ground into 5～20 order coarse powder, and in medicinal material coarse powder: the ratio of alcoholic solution (w/v)=1: 9 extracts effective ingredient with 40～85% ethanol water percolation, collect the percolate of 7 times of amounts, after reclaiming ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder.
Embodiment 2
Other is with embodiment 1, but the raw material weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=9.1%: 13.2%: 9.1%: 9.1%: 9.1%: 9.1%: 13.2%: 13.2%: 9.1%: 7.1%: 9.1%: 13.2%, its preparation method is: at first the Cortex Phellodendri in the raw material, Rhizoma Corydalis and Radix Sophorae Flavescentis are mixed and be ground into 5～20 order coarse powder, use 5%NaHCO
3Moistening back extracts effective ingredient with 40～85% ethanol water percolation, collect the percolate of 9 times of amounts, after reclaiming ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder, other 9 flavor medical materials mixing also are ground into 5～20 order coarse powder, extract effective ingredient with 40～85% ethanol water percolation, collect the percolate of 9 times of amounts, behind the recovery ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder.
Embodiment 3
Other is with embodiment 1, the raw material weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=6.1%: 10.2%: 6.1%: 6.1%: 6.1%: 6.1%: 10.2%: 10.2%: 6.1%: 4.1%: 6.1%: 10.2%, its preparation method is: at first the Cortex Phellodendri in the raw material, Rhizoma Corydalis and Radix Sophorae Flavescentis are mixed and be ground into 20 order coarse powder, use 5%NaHCO
3Moistening back extracts effective ingredient with 40～85% ethanol water percolation, collect the percolate of 8 times of amounts, after reclaiming ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder, other 9 flavor medical materials mixing also are ground into 20 order coarse powder, extract effective ingredient with 40～85% ethanol water percolation, collect the percolate of 8 times of amounts, behind the recovery ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder.
Embodiment 4
Other is with embodiment 3, but raw material medicated powder essence to 15 order.
Embodiment 5
Other is with embodiment 3, but its preparation method is: described medical material all through being ground into 5～20 purpose coarse powder, with Cortex Phellodendri, Rhizoma Corydalis and Radix Sophorae Flavescentis mixed powder, is used 5%NaHCO earlier
3Moistening back was flooded 24 hours at 20～40 ℃ with 40～85% ethanol waters, and reuse 40～85% ethanol water percolation extract; Other 9 flavor medical material mixings coarse powder, with 40～85% ethanol waters 20～40 ℃ of dippings 24 hours, the extraction of reuse 40～85% ethanol water percolation, and concentrating under reduced pressure below 80 ℃ be dried to the dry extract solid.
Embodiment 6
Other is with embodiment 5, but the dip time of corresponding medical material is 18 hours.
Embodiment 7
Other is with embodiment 5, but the dip time of corresponding medical material is 36 hours.
Embodiment 8
Other is with embodiment 5, and raw material Radix Paeoniae Rubra is replaced by the Radix Paeoniae Alba, and Rhizoma Smilacis Glabrae is replaced by Poria or Polyporus, and Fructus Toosendan is replaced by Cortex Meliae, and Rhizoma Curcumae is replaced by Radix Curcumae, and Semen Euryales is replaced by Semen Nelumbinis, and Rhizoma Cyperi is replaced by dried tuber, and Cortex Phellodendri is replaced by Rhizoma Coptidis.
Embodiment 9
Other is with embodiment 5, and extract powder is granulated with starch slurry, adds an amount of adjuvant and makes tablet and sugar coating or film-coat or hard capsule or pill or granule or soft capsule, and every or every in the preparation of making can be 0.20～0.60 gram.
Embodiment 10
Other just uses the alcoholic solution heating and refluxing extraction with embodiment 3, collects backflow, and decompression recycling ethanol also concentrates and be dried to the dry extract solid.
Embodiment 11
Other is with embodiment 5, is ground into 5～20 purpose coarse powder after just earlier Rhizoma Curcumae, rhizoma sparganic, Radix Angelicae Sinensis and Rhizoma Cyperi being mixed, and extracts volatile oil with distillating method, the volatile oil that obtains directly spray into dry extract with or to mix with dry extract again behind the beta-cyclodextrin inclusion compound.Medicinal residues after the extraction and other medicinal material coarse powder merge back alcoholic solution diafiltration or reflux, extract.
Experiment condition and method can determine that the sample of each step all needs weighing and record by practical situation.Except the TLC developing solvent, do not use CHCl during experiment as far as possible
3, toxic solvent such as benzene.From the angle of analysis of components and Quality Control, alkaloidal detection can be guaranteed the medical material input of Cortex Phellodendri, Rhizoma Corydalis and Radix Sophorae Flavescentis.Flavone, flavonol and quinones detect may command Radix Salviae Miltiorrhizae and Rhizoma Smilacis Glabrae reinforced.The existence of analysis decidable Radix Angelicae Sinensis, Rhizoma Cyperi, Rhizoma Curcumae and the rhizoma sparganic of volatile oil and polysaccharide composition.The analysis of Saponin class can be understood the actual content of Radix Paeoniae Rubra, Fructus Toosendan, Semen Euryales and Rhizoma Dioscoreae.
Claims (9)
1, the preparation method of Fuyankang extract, comprise and select Radix Paeoniae Rubra for use, Rhizoma Smilacis Glabrae, rhizoma sparganic, Fructus Toosendan, Rhizoma Curcumae, Rhizoma Corydalis, Semen Euryales, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Cyperi, Cortex Phellodendri, Chinese crude drugs such as Radix Salviae Miltiorrhizae are as raw material, it is characterized in that: the raw material weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=3.1～～9.1%: 7.2～13.2%: 3.1～9.1%: 3.1～9.1%: 3.1～9.1%: 3.1～9.1%: 7.2～13.2%: 7.2～13.2%: 3.1～9.1%: 1.1～7.1%: 3.1～9.1%: 7.2～13.2%, its preparation method is: at first with the Cortex Phellodendri in the raw material, Rhizoma Corydalis and Radix Sophorae Flavescentis mix and are ground into 5～20 order coarse powder, use 5%NaHCO
3Moistening back extracts effective ingredient with 40～85% ethanol water percolation, collect the percolate of 7～9 times of amounts, after reclaiming ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder, other 9 flavor medical materials mixing also are ground into 5～20 order coarse powder, extract effective ingredient with 40～85% ethanol water percolation, collect the percolate of 7～9 times of amounts, behind the recovery ethanol, concentrating under reduced pressure is dried to the extractum solid, and pulverize dry powder.
2. by the preparation method of the described Fuyankang extract of claim 1, it is characterized in that: its raw material weight proportioning is: Radix Paeoniae Rubra: Rhizoma Smilacis Glabrae: rhizoma sparganic: Fructus Toosendan: Rhizoma Curcumae: Rhizoma Corydalis: Semen Euryales: Radix Angelicae Sinensis: Radix Sophorae Flavescentis: Rhizoma Cyperi: Cortex Phellodendri: Radix Salviae Miltiorrhizae=6.1%: 10.2%: 6.1%: 6.1%: 6.1%: 6.1%: 10.2%: 10.2%: 6.1%: 4.1%: 6.1%: 10.2%.
3. by the preparation method of claim 1 or 2 described Fuyankang extracts, it is characterized in that described 12 flavor medical materials all are broken into 5～20 order coarse powder, Cortex Phellodendri, Rhizoma Corydalis and Radix Sophorae Flavescentis powder are used 5%NaHCO earlier
3Moistening back was flooded 18-36 hour at 20～40 ℃ with alcoholic solution, and repercolation extracts; Other nine flavor medicinal material coarse powder, are extracted with the alcoholic solution percolation after 18-36 hour with the alcoholic solution dipping.
4. by the preparation method of the described Fuyankang extract of claim 3, it is characterized in that described 12 flavor medical materials all are broken into 5～20 order coarse powder, Cortex Phellodendri, Rhizoma Corydalis and Radix Sophorae Flavescentis powder are used 5%NaHCO earlier
3Moistening back was flooded 24 hours at 20～40 ℃ with alcoholic solution, and repercolation extracts; Other nine flavor medicinal material coarse powder, are extracted with the alcoholic solution percolation after 24 hours with the alcoholic solution dipping.
5. by the preparation method of the described Fuyankang extract of claim 4, it is characterized in that, also be included in concentrating under reduced pressure below 80 ℃ and be dried to the dry extract solid.
6,, it is characterized in that extracting and to collect 7～9 times reflux extracting liquid for going out active ingredient with the alcoholic solution heating and refluxing extraction with the alcoholic solution diafiltration by the preparation method of the described Fuyankang extract of claim 4.
7, the preparation method of the described Fuyankang extract of claim 4, its feature also is, be ground into 5～20 purpose coarse powder after earlier Rhizoma Curcumae, rhizoma sparganic, Radix Angelicae Sinensis and Rhizoma Cyperi being mixed, extract volatile oil with distillating method, the volatile oil that obtains directly sprays into dry extract usefulness or to mix with dry extract behind the beta-cyclodextrin inclusion compound, the medicinal residues after the extraction and other medicinal material coarse powder merge back alcoholic solution diafiltration or reflux, extract, again.
8. the preparation method of the described Fuyankang extract of claim 4, it is characterized in that raw material Radix Paeoniae Rubra can replace by the Radix Paeoniae Alba, Rhizoma Smilacis Glabrae can Poria, Polyporus replaces, Fructus Toosendan can replace by Cortex Meliae, Rhizoma Curcumae can replace by Radix Curcumae, Semen Euryales can replace by Semen Nelumbinis, and Rhizoma Cyperi can replace by dried tuber, and Cortex Phellodendri can replace by Rhizoma Coptidis.
9. press the preparation method of the described Fuyankang extract of claim 4, it is characterized in that, the dry extract that obtains is granulated with suitable adhesive, add an amount of adjuvant and make tablet and sugar coating or film-coat or hard capsule or pill or granule or soft capsule, every or every in the preparation of making is 0.20～0.60 gram.
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| CN 200510033261 CN1820780A (en) | 2005-02-19 | 2005-02-19 | Method for preparing Fuyankang extract |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100455309C (en) * | 2006-11-03 | 2009-01-28 | 赵全成 | Compound Chinese medicinal preparation for treating gynecological inflammation and preparation method thereof |
| CN103157062A (en) * | 2012-11-09 | 2013-06-19 | 深圳市国源药业有限公司 | Medicine composition curing gynaecological mass diseases such as fibroids and preparation method and application thereof |
| CN103861044A (en) * | 2014-04-02 | 2014-06-18 | 湖南湘泉药业股份有限公司 | Method for preparing soft material of gynecologic inflammation treatment preparation |
| CN106770830A (en) * | 2016-12-28 | 2017-05-31 | 贵阳中医学院第二附属医院 | A kind of detection method of the Chinese medicine preparation for treating fibroid |
| CN109464633A (en) * | 2018-12-29 | 2019-03-15 | 广东罗浮山国药股份有限公司 | A kind of application of Chinese medicine composition in the drug of preparation treatment softening hard masses Jie , lumps in the chest and abdomen |
-
2005
- 2005-02-19 CN CN 200510033261 patent/CN1820780A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100455309C (en) * | 2006-11-03 | 2009-01-28 | 赵全成 | Compound Chinese medicinal preparation for treating gynecological inflammation and preparation method thereof |
| CN103157062A (en) * | 2012-11-09 | 2013-06-19 | 深圳市国源药业有限公司 | Medicine composition curing gynaecological mass diseases such as fibroids and preparation method and application thereof |
| CN103157062B (en) * | 2012-11-09 | 2015-03-18 | 深圳市国源药业有限公司 | Medicine composition curing gynaecological mass diseases such as fibroids and preparation method and application thereof |
| CN103861044A (en) * | 2014-04-02 | 2014-06-18 | 湖南湘泉药业股份有限公司 | Method for preparing soft material of gynecologic inflammation treatment preparation |
| CN103861044B (en) * | 2014-04-02 | 2016-02-24 | 湖南湘泉药业股份有限公司 | A kind of preparation method of FUYANKANG soft material |
| CN106770830A (en) * | 2016-12-28 | 2017-05-31 | 贵阳中医学院第二附属医院 | A kind of detection method of the Chinese medicine preparation for treating fibroid |
| CN109464633A (en) * | 2018-12-29 | 2019-03-15 | 广东罗浮山国药股份有限公司 | A kind of application of Chinese medicine composition in the drug of preparation treatment softening hard masses Jie , lumps in the chest and abdomen |
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