CN1730044A - Preparation method of quick-acting cardialgia spraying agent - Google Patents
Preparation method of quick-acting cardialgia spraying agent Download PDFInfo
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- CN1730044A CN1730044A CN 200510088364 CN200510088364A CN1730044A CN 1730044 A CN1730044 A CN 1730044A CN 200510088364 CN200510088364 CN 200510088364 CN 200510088364 A CN200510088364 A CN 200510088364A CN 1730044 A CN1730044 A CN 1730044A
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- 206010002383 Angina Pectoris Diseases 0.000 title claims abstract description 34
- 238000005507 spraying Methods 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title abstract 3
- 239000007921 spray Substances 0.000 claims abstract description 76
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 238000003825 pressing Methods 0.000 claims abstract description 18
- 229920001903 high density polyethylene Polymers 0.000 claims abstract description 15
- 239000004700 high-density polyethylene Substances 0.000 claims abstract description 15
- 239000000463 material Substances 0.000 claims abstract description 7
- 239000000443 aerosol Substances 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 144
- 238000002156 mixing Methods 0.000 claims description 36
- 238000003756 stirring Methods 0.000 claims description 32
- 239000000284 extract Substances 0.000 claims description 24
- -1 filter Substances 0.000 claims description 24
- 239000000706 filtrate Substances 0.000 claims description 24
- 239000006228 supernatant Substances 0.000 claims description 24
- 239000000341 volatile oil Substances 0.000 claims description 24
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 13
- 238000005267 amalgamation Methods 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 12
- 238000004821 distillation Methods 0.000 claims description 12
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 12
- 229920000053 polysorbate 80 Polymers 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 8
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- 239000003814 drug Substances 0.000 abstract description 12
- 229940079593 drug Drugs 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 239000012567 medical material Substances 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 208000002193 Pain Diseases 0.000 description 3
- CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 2
- 206010013954 Dysphoria Diseases 0.000 description 2
- 206010048245 Yellow skin Diseases 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 230000017531 blood circulation Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 239000003380 propellant Substances 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052729 chemical element Inorganic materials 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 230000008058 pain sensation Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention belongs to the field of medical Chinese patent medicines, in particular to a preparation method of a quick-acting cardialgia spraying agent, which aims to fill medicinal liquid prepared by a specific preparation method into a special spraying bottle by using medicinal materials in a prescription of a quick-acting cardialgia aerosol, and manually pressing a valve to spray medicine when in use; the spray bottle is made of high-density polyethylene or PET, the medicine in the bottle is in a normal pressure state, the carrying is light, convenient and safe, and the quick-acting cardialgia spraying agent is prepared by a specific process and has the characteristics of convenience in carrying and safety in use.
Description
One, technical field:
The invention belongs to the medical science technical field of Chinese patent medicine, relate to a kind of method for making of quick-acting cardiac pain spray specifically.
Two, background technology:
The prescription of quick-acting cardiac pain spray derives from " quick-acting cardiac pain aerosol ", and the quick-acting cardiac pain aerosol is after liquid medicine filling is sealed in high voltage bearing canister, to charge into propellant (freon CF
2C1
2), press movable valve during use, lean on the pressure of propellant that medicinal liquid is sprayed.Freon contains chemical element " fluorine " and " chlorine ", to the toxic effect of human body, the ozone layer in the atmosphere is had great destruction.The inner tool elevated pressures of aluminium pot that is used for liquid drug, non-refractory is squeezed, collision can cause breakage, blasts, and certain risk is arranged.
Three, summary of the invention:
The objective of the invention is the prescription medical material with " quick-acting cardiac pain aerosol ", a kind of quick-acting cardiac pain spray that adopts specific method for making that liquid medicine filling is made in special spray bottle is to overcome above-mentioned deficiency.
The objective of the invention is to realize by following technical scheme:
A kind of method for making of quick-acting cardiac pain spray, prescription derives from " quick-acting cardiac pain aerosol ", is characterized in: quick-acting cardiac pain spray is got Cortex Moutan, the Rhizoma Chuanxiong pulverize separately becomes coarse powder in process of production; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, add ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing filters, and the filtrate embedding forms in special spray bottle;
Quick-acting cardiac pain spray is got Cortex Moutan, the Rhizoma Chuanxiong pulverize separately becomes coarse powder in process of production; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, adds ethanol, stirs, and leaves standstill, and draws supernatant, filters, and filtrate and above-mentioned concentrated solution merge.Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing adds above-mentioned amalgamation liquid, mixing, water is adjusted total amount to 1000ml, mixing filters, and the filtrate embedding is in special spray bottle, spray bottle adopts the spraying of manual pressing control fog-spray nozzle, and whenever pressing spray amount can form for 0.01ml～0.5ml;
Quick-acting cardiac pain spray is got Cortex Moutan, the Rhizoma Chuanxiong pulverize separately becomes coarse powder in process of production; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, adds ethanol, stirs, and leaves standstill, and draws supernatant, filters, and filtrate and above-mentioned concentrated solution merge.Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing adds above-mentioned amalgamation liquid, mixing, water is adjusted total amount to 1000ml, and mixing filters, the filtrate embedding is in special spray bottle, used spray bottle adopts the quantitative fog-spray nozzle spraying of manual pressing control, and the spray bottle material can be made by high density polyethylene (HDPE), PET or aluminum, and whenever pressing spray amount can form for 0.05ml～0.3ml;
Quick-acting cardiac pain spray in process of production, Cortex Moutan, Rhizoma Chuanxiong pulverize separately become coarse powder; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, add ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, with Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum is used dissolve with ethanol respectively, adds the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing, filter, the filtrate embedding is in special spray bottle, and used spray bottle adopts the quantitative fog-spray nozzle spraying of manual pressing control, the spray bottle material is made by high density polyethylene (HDPE) or PET, and whenever pressing spray amount is that 0.13ml ± 0.02ml forms.
The invention discloses a kind of clearing away heat and cooling blood, the medicine of promoting blood circulation and stopping pain is made the method for spray, and quick-acting cardiac pain spray is used for that the partial heat type is light, the moderate obstruction of qi in the chest and cardialgia, the double dysphoria with smothery sensation of pain, the tongue fur yellow skin, in special spray bottle, manual pressing valve sprays medicine during use with liquid medicine filling; Spray bottle adopts high density polyethylene (HDPE) or PET to make, and a medicine is in atmospheric pressure state in the bottle, carries light and handy, convenient, safety etc., and quick-acting cardiac pain spray has characteristics easy to carry, safe in utilization with specific prepared.
Four, the specific embodiment:
The quick-acting cardiac pain spray prescription is as follows:
Cortex Moutan 40g, Rhizoma Chuanxiong 401g, Borneolum Syntheticum 26g
Quick-acting cardiac pain spray adopts following method for making:
Get above three flavor medical materials, Cortex Moutan 40g, Rhizoma Chuanxiong 401g pulverize separately become coarse powder; Cortex Moutan 40g extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, with 90% ethanol 4000ml, stirred 4 hours for the second time, left standstill 12 hours, draw supernatant, filter, reclaim ethanol to volume and be about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, adds ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, and Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum 26g are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing adds above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing, filter, the filtrate embedding is in special spray bottle, promptly.
Embodiment one
Get above three flavor medical materials, Cortex Moutan 40g, Rhizoma Chuanxiong 401g pulverize separately become coarse powder; Cortex Moutan 40g extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, with 90% ethanol 4000ml, stirred 4 hours for the second time, left standstill 12 hours, draw supernatant, filter, reclaim ethanol to volume and be about 500ml.Rhizoma Chuanxiong extracts volatile oil, aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, adds ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum 26g are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing, filter, the filtrate embedding is in special spray bottle, and spray bottle adopts the spraying of manual pressing control fog-spray nozzle, whenever presses spray amount and can be 0.01ml～0.5ml.
Embodiment two
Get above three flavor medical materials, Cortex Moutan 40g, Rhizoma Chuanxiong 401g pulverize separately become coarse powder; Cortex Moutan 40g extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, with 90% ethanol 4000ml, stirred 4 hours for the second time, left standstill 12 hours, draw supernatant, filter, reclaim ethanol to volume and be about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, add ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, with Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum 26g uses dissolve with ethanol respectively, adds the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing, filter, the filtrate embedding is in special spray bottle, and used spray bottle adopts the quantitative fog-spray nozzle spraying of manual pressing control, the spray bottle material can be by high density polyethylene (HDPE), PET or aluminum are made, and whenever press spray amount and can be 0.05ml～0.3ml.
Embodiment three
Get above three flavor medical materials, Cortex Moutan 40g, Rhizoma Chuanxiong 401g pulverize separately become coarse powder; Cortex Moutan 40g extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, with 90% ethanol 4000ml, stirred 4 hours for the second time, left standstill 12 hours, draw supernatant, filter, reclaim ethanol to volume and be about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, add ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, with Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum 26g uses dissolve with ethanol respectively, adds the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing, filter, the filtrate embedding is in special spray bottle, and used spray bottle adopts the quantitative fog-spray nozzle spraying of manual pressing control, the spray bottle material is made by high density polyethylene (HDPE) or PET, and whenever pressing spray amount is 0.13ml ± 0.02ml.
The invention discloses a kind of clearing away heat and cooling blood, the medicine of promoting blood circulation and stopping pain is made the method for spray.Quick-acting cardiac pain spray is used for light, the moderate obstruction of qi in the chest and cardialgia of partial heat type, the pain dysphoria with smothery sensation of holding concurrently, tongue fur yellow skin.Quick-acting cardiac pain spray has characteristics easy to carry, safe in utilization with specific prepared.
Claims (4)
1, a kind of method for making of quick-acting cardiac pain spray, prescription derives from " quick-acting cardiac pain aerosol ", is characterized in: quick-acting cardiac pain spray is got Cortex Moutan, the Rhizoma Chuanxiong pulverize separately becomes coarse powder in process of production; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, add ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing filters, and the filtrate embedding forms in special spray bottle.
2, the method for making of a kind of quick-acting cardiac pain spray according to claim 1 is characterized in: quick-acting cardiac pain spray is got Cortex Moutan, the Rhizoma Chuanxiong pulverize separately becomes coarse powder in process of production; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, adds ethanol, stirs, and leaves standstill, and draws supernatant, filters, and filtrate and above-mentioned concentrated solution merge.Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing adds above-mentioned amalgamation liquid, mixing, water is adjusted total amount to 1000ml, mixing filters, and the filtrate embedding is in special spray bottle, spray bottle adopts the spraying of manual pressing control fog-spray nozzle, and whenever pressing spray amount can form for 0.01ml～0.5ml.
3, the method for making of a kind of quick-acting cardiac pain spray according to claim 1 is characterized in: quick-acting cardiac pain spray is got Cortex Moutan, the Rhizoma Chuanxiong pulverize separately becomes coarse powder in process of production; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, adds ethanol, stirs, and leaves standstill, and draws supernatant, filters, and filtrate and above-mentioned concentrated solution merge.Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum are used dissolve with ethanol respectively, add the 4ml Tween 80, mixing adds above-mentioned amalgamation liquid, mixing, water is adjusted total amount to 1000ml, and mixing filters, the filtrate embedding is in special spray bottle, used spray bottle adopts the quantitative fog-spray nozzle spraying of manual pressing control, and the spray bottle material can be made by high density polyethylene (HDPE), PET or aluminum, and whenever pressing spray amount can form for 0.05ml～0.3ml.
4, the method for making of a kind of quick-acting cardiac pain spray according to claim 1 is characterized in: quick-acting cardiac pain spray in process of production, Cortex Moutan, Rhizoma Chuanxiong pulverize separately become coarse powder; Cortex Moutan extracts secondary with 90% ethanol merceration, for the first time with 90% ethanol 5300ml, stirs 6 hours, leaves standstill 12 hours, for the second time with 90% ethanol 4000ml, stirs 4 hours, leaves standstill 12 hours, draws supernatant, filters, and reclaims ethanol to volume and is about 500ml.Rhizoma Chuanxiong extracts volatile oil, and the aqueous solution after the distillation filters, and concentrating under reduced pressure becomes the about 120g of clear paste, add ethanol, stir, leave standstill, draw supernatant, filter, filtrate and above-mentioned concentrated solution merge, with Rhizoma Chuanxiong volatile oil, Borneolum Syntheticum is used dissolve with ethanol respectively, adds the 4ml Tween 80, mixing, add above-mentioned amalgamation liquid, mixing, water are adjusted total amount to 1000ml, mixing, filter, the filtrate embedding is in special spray bottle, and used spray bottle adopts the quantitative fog-spray nozzle spraying of manual pressing control, the spray bottle material is made by high density polyethylene (HDPE) or PET, and whenever pressing spray amount is that 0.13ml ± 0.02ml forms.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200510088364 CN1730044A (en) | 2005-08-03 | 2005-08-03 | Preparation method of quick-acting cardialgia spraying agent |
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|---|---|---|---|
| CN 200510088364 CN1730044A (en) | 2005-08-03 | 2005-08-03 | Preparation method of quick-acting cardialgia spraying agent |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104198614A (en) * | 2014-09-17 | 2014-12-10 | 上海海虹实业(集团)巢湖今辰药业有限公司 | Identification method for quick-acting cardiodynia dropping pill |
| CN104688837A (en) * | 2013-12-06 | 2015-06-10 | 天津中新药业集团股份有限公司第六中药厂 | Preparation method of Suxiaoxintong tablets |
| CN104688841A (en) * | 2013-12-06 | 2015-06-10 | 天津中新药业集团股份有限公司第六中药厂 | Preparation method of Suxiaoxintong granules |
| CN104688838A (en) * | 2013-12-06 | 2015-06-10 | 天津中新药业集团股份有限公司第六中药厂 | Preparation method of Suxiaoxintong oral liquid |
-
2005
- 2005-08-03 CN CN 200510088364 patent/CN1730044A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104688837A (en) * | 2013-12-06 | 2015-06-10 | 天津中新药业集团股份有限公司第六中药厂 | Preparation method of Suxiaoxintong tablets |
| CN104688841A (en) * | 2013-12-06 | 2015-06-10 | 天津中新药业集团股份有限公司第六中药厂 | Preparation method of Suxiaoxintong granules |
| CN104688838A (en) * | 2013-12-06 | 2015-06-10 | 天津中新药业集团股份有限公司第六中药厂 | Preparation method of Suxiaoxintong oral liquid |
| CN104198614A (en) * | 2014-09-17 | 2014-12-10 | 上海海虹实业(集团)巢湖今辰药业有限公司 | Identification method for quick-acting cardiodynia dropping pill |
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