CN1660191A - Oral preparation of Chinese traditional medicine for treating vascular headache and hemicrania, and preparation method - Google Patents
Oral preparation of Chinese traditional medicine for treating vascular headache and hemicrania, and preparation method Download PDFInfo
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- CN1660191A CN1660191A CN 200410047135 CN200410047135A CN1660191A CN 1660191 A CN1660191 A CN 1660191A CN 200410047135 CN200410047135 CN 200410047135 CN 200410047135 A CN200410047135 A CN 200410047135A CN 1660191 A CN1660191 A CN 1660191A
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Abstract
A Chinese medicine in the form of capsule, tablet, or effervescent tablet for treating vascular headache and hemicrania is prepared from 8 Chinese-medicinal materials including Chuan-xiong rhizome, bupleurum root, white peony root, liquorice root, etc. Its preparing process is also disclosed.
Description
Technical field:
The present invention relates to oral formulations of a kind of Chinese medicine and preparation method thereof, relate in particular to a kind of treatment vascular headache and migrainous oral Chinese medicine preparation and preparation method thereof.
Background technology:
Capsule in the oral Pharmaceutical dosage forms or enteric coated capsule or Film coated tablets or enteric coated tablet or effervescent tablet, change dosage form and manage as new drug research according to the relevant laws and regulations of China's drug control as a kind of pharmaceutical dosage form.The original dosage form of this product is a granule, and oneself lists the national drug ministry standard in.
The preparation characteristic of existing treatment vascular headache and migrainous granule is a part medical material ethanol percolation, after percolate reclaims ethanol, is condensed into the gold height, and is standby; Medicinal residues and other medical materials decoct with water, and are condensed into thick paste, precipitate with ethanol, and supernatant reclaims ethanol, and concentrating under reduced pressure becomes extractum; Merge above-mentioned two kinds of extractum,, make granule with adjuvants such as sucrose.
Existing treatment vascular headache and migrainous granule exist takes that volume is big, sugar content is high, the patient takes shortcomings such as inconvenience.
Summary of the invention:
The purpose of this invention is to provide a kind of treatment vascular headache and migrainous oral Chinese medicine preparation and preparation method thereof, overcome the above-mentioned drawback of prior art, improve the quality and the curative effect of product, satisfy the needs of medical treatment better.
Technical solution of the present invention is a kind of treatment vascular headache and migrainous oral Chinese medicine preparation, comprise capsule, enteric coated capsule, tablet (plain sheet, Film coated tablets, enteric coated tablet) and effervescent tablet, its main component is Rhizoma Chuanxiong, Radix Bupleuri, the Radix Angelicae Dahuricae, Rhizoma Cyperi, the Radix Paeoniae Alba, Semen Pruni, Semen Sinapis Albae, Radix Glycyrrhizae.
A kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation is:
(1) medicine constituent and percentage by weight consumption thereof are got the raw materials ready as follows:
Rhizoma Chuanxiong 30-50%, Radix Bupleuri 2-10%, Radix Angelicae Dahuricae 1-5%, Rhizoma Cyperi 6-10%, Radix Paeoniae Alba 15-30%, Semen Pruni 2-10% Semen Sinapis Albae 8-20%, Radix Glycyrrhizae 2-10%;
(2) get Rhizoma Chuanxiong, Rhizoma Cyperi, Radix Bupleuri, Semen Pruni, the Radix Angelicae Dahuricae and be ground into coarse powder, use ethanol percolation, reclaim ethanol after, concentrating under reduced pressure, extractum is standby;
(3) medicinal residues decoct with water 2 times with three flavors such as the Radix Paeoniae Alba, Semen Sinapis Albae, Radix Glycyrrhizae behind Rhizoma Chuanxiong, Rhizoma Cyperi, Radix Bupleuri, Semen Pruni, the Radix Angelicae Dahuricae percolation, each 2 hours, collecting decoction, be condensed into thick paste, add ethanol and reach 75%, precipitate 48 hours to containing the alcohol amount, get supernatant, reclaim ethanol, concentrating under reduced pressure, extractum is standby;
(4) (2) extractum with (3) gained is merged, be condensed into thick paste, standby; Or, be ground into dried cream powder with the thick paste drying, standby;
(5) with (4) gained thick paste or dried cream powder, add suitable adjuvant after, mixing is granulated, drying is made into capsule or enteric coated capsule or Film coated tablets or enteric coated tablet or effervescent tablet again;
The preparation method of treatment vascular headache and migrainous capsule or enteric coated capsule, get (4) gained thick paste or dried cream powder, the adding adjuvant is a lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid, sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, the combination of one or more different proportions in the Polyethylene Glycol, the weight that adds adjuvant is the 0.0-99.9% of drug weight; Adjuvant and medicament mixed are even, granulate dry, granulate; Granule promptly gets capsule with common Capsules fill; Granule enteric hollow capsule fill promptly gets enteric coated capsule;
Treatment vascular headache and migrainous tablet (plain sheet, Film coated tablets or enteric coated tablet) preparation method, get (4) gained thick paste or dried cream powder, the adding adjuvant is a lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid, sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, the combination of one or more different proportions in the Polyethylene Glycol, adding adjuvant weight is the 0.1-99.9% of drug weight; Medicine and adjuvant mix homogeneously, the starch slurry (concentration is 1-20%) or distilled water or ethanol or the polyvinylpyrrolidone rubber cement (concentration is 0.1-20% (g/ml)) that add the 0.1-99.9% of drug weight, granulate, dry, granulate, the mixture that adds one or more different proportions in the magnesium stearate lubricant, Pulvis Talci, micropowder silica gel, polyvinylpyrrolidone class material of drug weight 0.1-50% again, tabletting behind the mix homogeneously, plain sheet; Plain sheet promptly gets Film coated tablets with film-coat material coating; Plain sheet enteric material coating promptly gets enteric coated tablet;
The preparation method of treatment vascular headache and migrainous effervescent tablet, get (4) gained thick paste or dried cream powder, the adding adjuvant is a lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid, sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, the combination of one or more different proportions in the Polyethylene Glycol, adding adjuvant weight is the 0.1-99.9% of drug weight; Medicine is divided into two equal portions, respectively with the adjuvant mix homogeneously after, the mixture of one or more different proportions in a citric acid that adds drug weight 0.1-99.9%, the fumaric acid; The mixture of one or more different proportions in the sodium carbonate of a adding drug weight 0.1-99.9%, the sodium bicarbonate; The starch slurry (concentration is 1-20%) or distilled water or ethanol or the polyvinylpyrrolidone rubber cement (concentration is 0.1-20% (g/ml)) that add drug weight 0.1-99.9% respectively, behind granulation, drying, the granulate, granule is standby; Behind two kinds of granule equal portions mix homogeneously, the mixture that adds one or more different proportions in the magnesium stearate lubricant, Pulvis Talci, micropowder silica gel, polyvinylpyrrolidone class material of the 0.1-50% of particle weight again, tabletting behind the mix homogeneously promptly gets effervescent tablet;
Specific embodiments:
The present invention further specifies as follows in conjunction with specific embodiments:
A kind of treatment vascular headache and migrainous oral Chinese medicine preparation, comprise capsule, enteric coated capsule, tablet (plain sheet, Film coated tablets, enteric coated tablet) and effervescent tablet, it contains main component and is: Rhizoma Chuanxiong, Radix Bupleuri, the Radix Angelicae Dahuricae, Rhizoma Cyperi, the Radix Paeoniae Alba, Semen Pruni, Semen Sinapis Albae, Radix Glycyrrhizae.
A kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation is:
(1) medicine constituent and percentage by weight consumption thereof are got the raw materials ready as follows:
Rhizoma Chuanxiong 3000g, Radix Bupleuri 300g, Radix Angelicae Dahuricae 150g, Rhizoma Cyperi 600g, Radix Paeoniae Alba 1500g, Semen Pruni 300g, Semen Sinapis Albae 900g, Radix Glycyrrhizae 300g.
(2) get Rhizoma Chuanxiong, Rhizoma Cyperi, Radix Bupleuri, Semen Pruni, the Radix Angelicae Dahuricae and be ground into coarse powder,, use ethanol percolation according to the percolation under fluid extract and the extractum item, behind the recovery ethanol, concentrating under reduced pressure, extractum is standby;
(3) medicinal residues decoct with water 2 times with three flavors such as the Radix Paeoniae Alba, Semen Sinapis Albae, Radix Glycyrrhizae behind Rhizoma Chuanxiong, Rhizoma Cyperi, Radix Bupleuri, Semen Pruni, the Radix Angelicae Dahuricae percolation, each 2 hours, collecting decoction, be condensed into thick paste, add ethanol and reach 75%, precipitate 48 hours to containing the alcohol amount, get supernatant, reclaim ethanol, concentrating under reduced pressure, extractum is standby;
(4) (2) extractum with (3) gained is merged, be condensed into thick paste, standby; Or, be ground into dried cream powder with the thick paste drying, standby;
(5) preparation method of treatment vascular headache and migrainous capsule or enteric coated capsule:
Get (4) gained medicine thick paste or dried cream powder, add starch, micropowder silica gel an amount of (the about 120g of mixture), mix homogeneously, granulation, dry, granulate are made 1200 altogether, every heavy 0.5g; With common Capsules fill, promptly get capsule; Use the enteric hollow capsule fill, promptly get enteric coated capsule.
(6) preparation method of treatment vascular headache and migrainous tablet (plain sheet, Film coated tablets or enteric coated tablet):
Get (4) gained medicine thick paste or dried cream powder, add starch, low-substituted hydroxypropyl cellulose, micropowder silica gel (the about 200g of mixture) in right amount, mix homogeneously, granulation, dry, granulate, the magnesium stearate of adding granule total amount 2%, tabletting is made 1500 altogether; Plain sheet promptly gets Film coated tablets with film-coat material coating; Plain sheet enteric coating material coating promptly gets enteric coated tablet.
(7) preparation method of treatment vascular headache and migrainous effervescent tablet:
Get (4) gained medicine thick paste or dried cream powder, be divided into two equal portions, add sucrose, starch, dextrin an amount of (the about 100g of mixture) respectively, a citric acid 50g that adds; Another part adds sodium bicarbonate 80g; The difference mix homogeneously, granulation, dry, granulate with two kinds of granule mix homogeneously, add the magnesium stearate of granule total amount 2%, and tabletting promptly gets effervescent tablet.
Advantage of the present invention is:
Carry, taking convenience, be conducive to improve curative effect.
Claims (6)
1, a kind of treatment vascular headache and migrainous oral Chinese medicine preparation, it is characterized in that comprising capsule, enteric coated capsule, tablet (plain sheet, Film coated tablets, enteric coated tablet) and effervescent tablet, its main component is Rhizoma Chuanxiong, Radix Bupleuri, the Radix Angelicae Dahuricae, Rhizoma Cyperi, the Radix Paeoniae Alba, Semen Pruni, Semen Sinapis Albae, Radix Glycyrrhizae.
2, a kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation is characterized in that:
(1) medicine constituent and percentage by weight consumption thereof are got the raw materials ready as follows:
Rhizoma Chuanxiong 30-50%, Radix Bupleuri 2-10%, Radix Angelicae Dahuricae 1-5%, Rhizoma Cyperi 6-10%, Radix Paeoniae Alba 15-30%, Semen Pruni 2-10% Semen Sinapis Albae 8-20%, Radix Glycyrrhizae 2-10%;
(2) get Rhizoma Chuanxiong, Rhizoma Cyperi, Radix Bupleuri, Semen Pruni, the Radix Angelicae Dahuricae and be ground into coarse powder, use ethanol percolation, reclaim ethanol after, concentrating under reduced pressure, extractum is standby;
(3) medicinal residues decoct with water 2 times with three flavors such as the Radix Paeoniae Alba, Semen Sinapis Albae, Radix Glycyrrhizae behind Rhizoma Chuanxiong, Rhizoma Cyperi, Radix Bupleuri, Semen Pruni, the Radix Angelicae Dahuricae percolation, each 2 hours, collecting decoction, be condensed into thick paste, add ethanol and reach 75%, precipitate 48 hours to containing the alcohol amount, get supernatant, reclaim ethanol, concentrating under reduced pressure, extractum is standby;
(4) (2) extractum with (3) gained is merged, be condensed into thick paste, standby; Or, be ground into dried cream powder with the thick paste drying, standby;
(5) with (4) gained thick paste or dried cream powder, add suitable adjuvant after, mixing is granulated, drying is made into capsule or enteric coated capsule or tablet or effervescent tablet again.
3, a kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation according to claim 2, the preparation method that it is characterized in that capsule or enteric coated capsule is: get the thick paste or the dried cream powder that make, the adding adjuvant is a lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid, sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, the combination of one or more different proportions in the Polyethylene Glycol, the weight of adjuvant are the 0.0-99.9% of drug weight; Adjuvant and medicament mixed are even, granulate dry, granulate; Granule promptly gets capsule with common Capsules fill; Granule enteric hollow capsule fill promptly gets enteric coated capsule.
4, a kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation according to claim 2, it is characterized in that tablet (plain sheet, Film coated tablets or enteric coated tablet) preparation method be: get the thick paste or the dried cream powder that make, the adding adjuvant is a lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid, sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, the combination of one or more different proportions in the Polyethylene Glycol, adjuvant weight are the 0.1-99.9% of drug weight; Medicine and adjuvant mix homogeneously, the starch slurry (concentration is 1-20%) or distilled water or ethanol or the polyvinylpyrrolidone rubber cement (concentration is 0.1-20% (g/ml)) that add the 0.1-99.9% of drug weight, granulate, dry, granulate, the mixture that adds one or more different proportions in the magnesium stearate lubricant, Pulvis Talci, micropowder silica gel, polyvinylpyrrolidone class material of drug weight 0.1-50% again, tabletting behind the mix homogeneously, plain sheet; Plain sheet promptly gets Film coated tablets with film-coat material coating; Plain sheet enteric material coating promptly gets enteric coated tablet.
5, a kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation according to claim 2, the preparation method that it is characterized in that effervescent tablet is: get the thick paste or the dried cream powder that make, the adding adjuvant is a lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid, sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, the combination of one or more different proportions in the Polyethylene Glycol, adjuvant weight are the 0.1-99.9% of drug weight; Medicine is divided into two equal portions, respectively with the adjuvant mix homogeneously after, the mixture of one or more different proportions in a citric acid that adds drug weight 0.1-99.9%, the fumaric acid; The mixture of one or more different proportions in the sodium carbonate of a adding drug weight 0.1-99.9%, the sodium bicarbonate; The starch slurry (concentration is 1-20%) or distilled water or ethanol or the polyvinylpyrrolidone rubber cement (concentration is 0.1-20% (g/ml)) that add drug weight 0.1-99.9% respectively, behind granulation, drying, the granulate, granule is standby; Behind two kinds of granule equal portions mix homogeneously, the mixture that adds one or more different proportions in the magnesium stearate lubricant, Pulvis Talci, micropowder silica gel, polyvinylpyrrolidone class material of the 0.1-50% of particle weight again, tabletting behind the mix homogeneously promptly gets effervescent tablet.
6, a kind of preparation method for the treatment of vascular headache and migrainous oral Chinese medicine preparation according to claim 2 is characterized in that the optimum weight percentage ratio of its main constituent is:
Rhizoma Chuanxiong 42.5%, Radix Bupleuri 4.3%, the Radix Angelicae Dahuricae 2.1%, Rhizoma Cyperi 8.5%, the Radix Paeoniae Alba 21.3%, Semen Pruni 4.3%, Semen Sinapis Albae 12.7%, Radix Glycyrrhizae 4.3%.
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| CN 200410047135 CN1660191A (en) | 2004-12-31 | 2004-12-31 | Oral preparation of Chinese traditional medicine for treating vascular headache and hemicrania, and preparation method |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100475249C (en) * | 2008-05-20 | 2009-04-08 | 常立国 | Chinese medicinal composition for curing migraine |
| CN104189351A (en) * | 2014-09-29 | 2014-12-10 | 洛阳御平国生物科技有限公司 | Traditional Chinese medicine for treating migraine |
| CN105535346A (en) * | 2016-01-05 | 2016-05-04 | 成都市飞龙水处理技术研究所青白江第一分所 | Decoction for treating vascular neuralgia headaches and migraine and preparation method |
| CN106389886A (en) * | 2016-10-27 | 2017-02-15 | 吴安相 | Traditional Chinese medicine recipe for treating migraine |
| CN106963886A (en) * | 2017-04-14 | 2017-07-21 | 崔应麟 | Plus taste dissipates inclined soup |
| CN110559379A (en) * | 2019-09-27 | 2019-12-13 | 湖北神农汉方生物科技有限公司 | Preparation method of pure traditional Chinese medicine powder decoction granules |
| CN116077554A (en) * | 2022-11-29 | 2023-05-09 | 神威药业集团有限公司 | Preparation method of Guanxinning composition |
-
2004
- 2004-12-31 CN CN 200410047135 patent/CN1660191A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100475249C (en) * | 2008-05-20 | 2009-04-08 | 常立国 | Chinese medicinal composition for curing migraine |
| CN104189351A (en) * | 2014-09-29 | 2014-12-10 | 洛阳御平国生物科技有限公司 | Traditional Chinese medicine for treating migraine |
| CN105535346A (en) * | 2016-01-05 | 2016-05-04 | 成都市飞龙水处理技术研究所青白江第一分所 | Decoction for treating vascular neuralgia headaches and migraine and preparation method |
| CN106389886A (en) * | 2016-10-27 | 2017-02-15 | 吴安相 | Traditional Chinese medicine recipe for treating migraine |
| CN106963886A (en) * | 2017-04-14 | 2017-07-21 | 崔应麟 | Plus taste dissipates inclined soup |
| CN110559379A (en) * | 2019-09-27 | 2019-12-13 | 湖北神农汉方生物科技有限公司 | Preparation method of pure traditional Chinese medicine powder decoction granules |
| CN116077554A (en) * | 2022-11-29 | 2023-05-09 | 神威药业集团有限公司 | Preparation method of Guanxinning composition |
| CN116077554B (en) * | 2022-11-29 | 2023-12-26 | 神威药业集团有限公司 | Preparation method of Guanxinning composition |
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