CN1582797A - Detoxifying additive for filtering tips - Google Patents
Detoxifying additive for filtering tips Download PDFInfo
- Publication number
- CN1582797A CN1582797A CN 200410044987 CN200410044987A CN1582797A CN 1582797 A CN1582797 A CN 1582797A CN 200410044987 CN200410044987 CN 200410044987 CN 200410044987 A CN200410044987 A CN 200410044987A CN 1582797 A CN1582797 A CN 1582797A
- Authority
- CN
- China
- Prior art keywords
- additive
- chewing
- rod
- extract
- cigarette
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000654 additive Substances 0.000 title claims abstract description 15
- 230000000996 additive effect Effects 0.000 title claims abstract description 15
- 238000001914 filtration Methods 0.000 title description 5
- 235000015489 Emblica officinalis Nutrition 0.000 claims abstract description 11
- 239000002245 particle Substances 0.000 claims abstract description 10
- 235000011517 Terminalia chebula Nutrition 0.000 claims abstract description 6
- 150000001875 compounds Chemical class 0.000 claims description 16
- 230000001055 chewing effect Effects 0.000 claims description 15
- 244000119298 Emblica officinalis Species 0.000 claims description 10
- 239000000284 extract Substances 0.000 claims description 9
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 5
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims description 5
- 235000009685 Crataegus X maligna Nutrition 0.000 claims description 5
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 5
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 5
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 5
- 235000009682 Crataegus limnophila Nutrition 0.000 claims description 5
- 235000004423 Crataegus monogyna Nutrition 0.000 claims description 5
- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 5
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- 240000000171 Crataegus monogyna Species 0.000 claims 2
- 235000019504 cigarettes Nutrition 0.000 abstract description 10
- 239000000779 smoke Substances 0.000 abstract description 3
- XKLJHFLUAHKGGU-UHFFFAOYSA-N nitrous amide Chemical compound ON=N XKLJHFLUAHKGGU-UHFFFAOYSA-N 0.000 abstract description 2
- 241001130943 Phyllanthus <Aves> Species 0.000 abstract 1
- 244000277583 Terminalia catappa Species 0.000 abstract 1
- 244000269722 Thea sinensis Species 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
- 238000000605 extraction Methods 0.000 description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 241000208125 Nicotiana Species 0.000 description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 239000011269 tar Substances 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 241001092040 Crataegus Species 0.000 description 3
- 239000006286 aqueous extract Substances 0.000 description 3
- 230000006837 decompression Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 241000411851 herbal medicine Species 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- 239000000469 ethanolic extract Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 239000004113 Sepiolite Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 241001422033 Thestylus Species 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000015111 chews Nutrition 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000004868 gas analysis Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000019355 sepiolite Nutrition 0.000 description 1
- 229910052624 sepiolite Inorganic materials 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Landscapes
- Medicinal Preparation (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Confectionery (AREA)
Abstract
A detoxicating additive for the tip filter of cigaretter in order to decrease the contents of tar, Co and nitrosamine in cigarette's smoke is prepared from tea leaf, haw, phyllanthus, embolica and myrobalan through extracting their active components in the form of liquid, concentrating and drying to obtain particles.
Description
One, technical field
The present invention relates to a kind of composition that reduces the cigarette harmful components, particularly cigarette and chew rod and use additive, exactly be chew excellent with novel attenuation additive.
Two, background technology
Chew rod effect of harmful components in landing Jiao, the minimizing flue gas in cigarette.Monobasic is chewed excellent being rolled through forming paper by fibre bundle and is formed.The compound rod of chewing promptly adds materials such as silica gel, sepiolite, activated carbon, the filtration of chewing rod with increase at fibre bundle.Facts have proved and use adding technique can significantly reduce tar and CO content in the cigarette smoke, wherein active carbon is chewed the highest tar content that makes of rod and is descended 12%, and the CO burst size reduces 15.68%.Above-mentioned additive mostly is the bigger adsorbent of specific area, therefore also can hold back some aroma components in the flue gas in reducing tar and reducing harm, influence the fragrance style and the flue gas feature of cigarette, and particle diameter is too small, is easily sucked the oral cavity by the consumer.
Three, summary of the invention
The present invention overcomes a kind of new additive agent that the defective of above-mentioned additive is developed, and is raw material with the vegetable Chinese herbal medicine, obtains extract through extraction, and extract is made certain size particles through precipitation after concentrating, and this is the attenuation additive.
Described Chinese herbal medicine has following component and percentage by weight:
Tealeaves 20～55%
Hawthorn 12～45%
Emblic 10～35%
The myrobalan 5～15%.
Preferred following percentage by weight:
Tealeaves 30～45%
Hawthorn 20～35%
Emblic 15～25%
The myrobalan 6～10%.
With boiling or refluxing extraction behind the said herbal medicine prescription, perhaps add alcohol reflux and extract, perhaps successively extract, obtain aqueous extract or ethanol extract through separation, extract is through precipitation, the concentrated particle diameter 40-80 order particle of making.
Use the compound rod forming machine of chewing, before the acetate tow moulding, this additive is made the compound rod of chewing by the dosage that 1.75mg/mm chews rod among evenly being mixed in tow.
This compound rod of chewing is positioned at preceding half section with filter tip, can make coke tar in cigarette descend 7.7% more on year-on-year basis, and the CO burst size reduces 17.8%, and energy part blocking nitrosamine formation is synthetic, reduce relevant harmful substance in the cigarette smoke, particularly free stem and TNSA effectively reduce harm of smoking.
This compound rod of chewing is chewed excellent cigarette product flue gas analysis result such as following table with monobasic:
Sample TPM moisture TAR nicotine CO mouth is counted the resistance to suction average weight
Monobasic is chewed rod 16.95 1.25 14.30 1.45 21.25 7.20 1,030 0.91
This compound rod 15.88 1.26 13.20 1.39 17.46 7.30 1,030 0.93 of chewing
Remarks: pipe tobacco is that same experiment product is with a collection of pipe tobacco in the project, and other auxilliary material design is identical.(unit is: mouthful number: mouthful/; Resistance to suction: Pa; Average weight: g/ props up, and other project is: mg/ props up)
This compound rod of chewing is chewed excellent cigarette product aesthetic quality such as following table with monobasic:
The assorted gas excitant pleasant impression of sample fragrance harmony adds up to
Monobasic is chewed rod 32.08 5.13 14.00 13.57 16.58 81.36
This compound rod 32.00 5.07 13.87 13.87 16.73 81.54 of chewing
Remarks: pipe tobacco is that same experiment product is with a collection of pipe tobacco in the project, and other auxilliary material design is identical.
Evil effect falls in the compound rod of chewing of this additive preparation, existing attenuation, does not influence sensory evaluating smoking's quality again, effect such as wet one's whistle, relieving cough and reducing sputum that having again simultaneously promotes the production of body fluid.
Four, the specific embodiment
1, gets 20 parts of tealeaves (calling A in the following text), 45 parts of hawthorn (calling B in the following text), 30 parts of emblics (calling C in the following text), 5 parts of myrobalan'ss (calling D in the following text).Add decocting that 2-5 doubly measures and boil or refluxed 0.5～2 hour, isolated by filtration obtains aqueous extract, and aqueous extract is made particle diameter 40-80 purpose particle through decompression dehydration, after concentrating.
2, get A55 part, B12 part, C18 part, D15 part.Extraction is with embodiment 1.
3, get A25 part, B30 part, C35 part, D10 part.Extraction is with embodiment 1.
4, get A30 part, B35 part, C25 part, D10 part.The alcohol reflux that adds 5～10 times of amounts extracted 1～2 hour, and isolated by filtration obtains ethanol extract, made 40～80 purpose particles after the decompression precipitation reclaims ethanol, concentrates.
5, get A45 part, B20 part, C25 part, D10 part.Extraction is with embodiment 4.
6, get A40 part, B32 part, C20 part, D8 part.Extraction is with embodiment 4.
7, get A42 part, B28 part, C23 part, D7 part, first water extraction, alcohol extract is used in filtering again, merges water and two kinds of extracts of ethanol, and the decompression precipitation reclaims ethanol, makes grain through 40～80 purpose particles after continuing to dewater, concentrating.
8, process the compound rod of chewing with the novel attenuation additive of embodiment 1～7 preparation.Use the compound rod forming machine of chewing, before the acetate tow moulding, chew the stylus amount by 1.75mg/mm and make the compound rod of chewing among this additive is evenly added tow, this compound rod of chewing is positioned at preceding half section with filter tip.
Claims (2)
1, a kind of rod of chewing is with novel attenuation additive, and through the particle that extracts, extract is made through precipitation, after concentrated, it is characterized in that: described compound Chinese herb has following component and percentage by weight by compound Chinese herb
Tealeaves 20～55%
Hawthorn 12～45%
Emblic 10～35%
The myrobalan 5～15%.
2, attenuation additive according to claim 1 is characterized in that the preferred following percentage by weight of compound Chinese herb:
Tealeaves 30～45%
Hawthorn 20～35%
Emblic 15～25%
The myrobalan 6～10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410044987 CN1253112C (en) | 2004-06-05 | 2004-06-05 | Detoxifying additive for filtering tips |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410044987 CN1253112C (en) | 2004-06-05 | 2004-06-05 | Detoxifying additive for filtering tips |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1582797A true CN1582797A (en) | 2005-02-23 |
| CN1253112C CN1253112C (en) | 2006-04-26 |
Family
ID=34601860
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410044987 Expired - Lifetime CN1253112C (en) | 2004-06-05 | 2004-06-05 | Detoxifying additive for filtering tips |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1253112C (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1935179B (en) * | 2005-09-23 | 2010-06-09 | 南京星银药业有限公司 | Fat-regulating medicinal composition from Tibetanmedicine and its preparing method |
| CN101787329A (en) * | 2010-03-10 | 2010-07-28 | 广东中烟工业有限责任公司 | Tobacco flavor as well as preparation method and application thereof |
| CN102742933A (en) * | 2012-07-26 | 2012-10-24 | 红云红河烟草(集团)有限责任公司 | Application of hawthorn in cigarette |
| CN105011362A (en) * | 2015-06-17 | 2015-11-04 | 云南中烟工业有限责任公司 | Glyceryl triacetate extract of Chinese hawthorn fruit and application thereof to cigarette |
| CN110613131A (en) * | 2019-06-20 | 2019-12-27 | 中国林业科学研究院资源昆虫研究所 | Application of emblic leafflower fruit extract in preparing health attenuated food |
| CN115369695A (en) * | 2022-09-14 | 2022-11-22 | 云南中烟工业有限责任公司 | Natural sweetener, coating liquid containing natural sweetener and application of coating liquid to tipping paper for cigarettes |
-
2004
- 2004-06-05 CN CN 200410044987 patent/CN1253112C/en not_active Expired - Lifetime
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1935179B (en) * | 2005-09-23 | 2010-06-09 | 南京星银药业有限公司 | Fat-regulating medicinal composition from Tibetanmedicine and its preparing method |
| CN101787329A (en) * | 2010-03-10 | 2010-07-28 | 广东中烟工业有限责任公司 | Tobacco flavor as well as preparation method and application thereof |
| CN102742933A (en) * | 2012-07-26 | 2012-10-24 | 红云红河烟草(集团)有限责任公司 | Application of hawthorn in cigarette |
| CN105011362A (en) * | 2015-06-17 | 2015-11-04 | 云南中烟工业有限责任公司 | Glyceryl triacetate extract of Chinese hawthorn fruit and application thereof to cigarette |
| CN110613131A (en) * | 2019-06-20 | 2019-12-27 | 中国林业科学研究院资源昆虫研究所 | Application of emblic leafflower fruit extract in preparing health attenuated food |
| CN115369695A (en) * | 2022-09-14 | 2022-11-22 | 云南中烟工业有限责任公司 | Natural sweetener, coating liquid containing natural sweetener and application of coating liquid to tipping paper for cigarettes |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1253112C (en) | 2006-04-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101199363B (en) | Additive agent for reducing harmful constituents in flue gas and method for preparing same | |
| CN103445295A (en) | Ternary tobacco fiber paper filter rod made from composite aroma-enhancing plants and preparation method of filter rod | |
| CN101928352B (en) | Extraction for active ingredients of cordyceps sinensis and application thereof in cigarette filter | |
| CN101912161B (en) | Mint tobacco filter stick and preparation method thereof | |
| CN102669816B (en) | Filter tip and filter stick pre-filled with large-particle materials | |
| CN106360805B (en) | Novel recombined cigarette filter stick prepared from functional powder material | |
| CN101623126A (en) | Preparation technology of traditional Chinese medicine detoxification smoke-quit perfuming annex solution for cigarette | |
| CN101199364A (en) | Chinese herbal medicine cigarette filter tip rod for relieving cough and reducing sputum | |
| CN1253112C (en) | Detoxifying additive for filtering tips | |
| CN104256900A (en) | Novel electronic cigarette cotton | |
| CN101044918A (en) | Frangipani shaped Cigarette with egg extraction for reducing | |
| CN1473519A (en) | Toxin reduced body building type cigarette and its producing method | |
| CN101897478B (en) | Filter stick for cigarettes and preparation method thereof | |
| CN201919648U (en) | Artificial fiber filter tip with capsule | |
| CN101049186A (en) | Cigarette holder stick of adsorbing and reducing tar in high efficiency | |
| CN107874318B (en) | Herbal carbon composite particles, preparation method and application thereof in cigarettes | |
| CN106666825B (en) | A kind of cigarette filter rod preparation method for adding yew plants particle | |
| CN103622157B (en) | Ternary tobacco fiber paper filter stick containing herbaceous plants and manufacturing method thereof | |
| CN207355461U (en) | A kind of graphene health-care cigarette holder | |
| CN101912160B (en) | Harm reduction filter stick for cigarette and preparation method thereof | |
| CN202514579U (en) | Cigarette filter | |
| CN202603595U (en) | Filter tip containing large-particle material and filter rod | |
| CN1202760C (en) | Tobacco with low nicotine content and its producing method | |
| CN103110185A (en) | Ternary tobacco fiber paper filter stick for compositing tobacco shreds and preparation method thereof | |
| CN1579261A (en) | Tabacco additive of coke-reducing toxicant-reducing and cough-relieving lung-nourishing and preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: ANHUI TOBACCO INDUSTRY CO., LTD. Free format text: FORMER NAME OR ADDRESS: WUHU CIGARETTE FACTORY |
|
| CP03 | Change of name, title or address |
Address after: No. 9, Tianda Road, hi tech Development Zone, Anhui, Hefei Patentee after: China Tobacco Anhui Industrial Corp. Address before: No. 135, Wuhu Road, Wuhu, Anhui Patentee before: Wuhu Cigarette Factory |
|
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Wuhu Cigarette Materials Factory Assignor: China Tobacco Anhui Industrial Corp. Contract fulfillment period: 2009.8.25 to 2014.8.24 Contract record no.: 2009340000227 Denomination of invention: Detoxifying additive for filtering tips Granted publication date: 20060426 License type: Exclusive license Record date: 20090828 |
|
| LIC | Patent licence contract for exploitation submitted for record |
Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2009.8.25 TO 2014.8.24; CHANGE OF CONTRACT Name of requester: WUHU CIGARETTE MATERIAL FACTORY Effective date: 20090828 |
|
| CP03 | Change of name, title or address |
Address after: 230088 No. 606 Huangshan Road, Hefei High-tech Zone, Anhui Province Patentee after: CHINA TOBACCO ANHUI INDUSTRIAL Co.,Ltd. Address before: 230088 No. 9, Tianda Road, hi tech Development Zone, Anhui, Hefei Patentee before: China Tobacco Anhui Industrial Corp. |
|
| CP03 | Change of name, title or address | ||
| CX01 | Expiry of patent term |
Granted publication date: 20060426 |
|
| CX01 | Expiry of patent term |