CN1326961C - 一种高强防腐涂料及其制备方法 - Google Patents
一种高强防腐涂料及其制备方法 Download PDFInfo
- Publication number
- CN1326961C CN1326961C CNB2004100214219A CN200410021421A CN1326961C CN 1326961 C CN1326961 C CN 1326961C CN B2004100214219 A CNB2004100214219 A CN B2004100214219A CN 200410021421 A CN200410021421 A CN 200410021421A CN 1326961 C CN1326961 C CN 1326961C
- Authority
- CN
- China
- Prior art keywords
- polyisocyanates
- performed polymer
- diisocyanate
- coating
- viscotrol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000576 coating method Methods 0.000 title claims abstract description 42
- 239000011248 coating agent Substances 0.000 title claims abstract description 41
- 239000000463 material Substances 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 11
- 239000005056 polyisocyanate Substances 0.000 claims abstract description 32
- 229920001228 polyisocyanate Polymers 0.000 claims abstract description 32
- 230000007797 corrosion Effects 0.000 claims abstract description 18
- 238000005260 corrosion Methods 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 4
- DKPFZGUDAPQIHT-UHFFFAOYSA-N butyl acetate Chemical compound CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims description 22
- 229920000642 polymer Polymers 0.000 claims description 21
- ZEMPKEQAKRGZGQ-AAKVHIHISA-N 2,3-bis[[(z)-12-hydroxyoctadec-9-enoyl]oxy]propyl (z)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCCC(O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(O)CCCCCC)COC(=O)CCCCCCC\C=C/CC(O)CCCCCC ZEMPKEQAKRGZGQ-AAKVHIHISA-N 0.000 claims description 18
- 229920005862 polyol Polymers 0.000 claims description 18
- 150000003077 polyols Chemical class 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 15
- 239000005057 Hexamethylene diisocyanate Substances 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 11
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims description 11
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 229920006389 polyphenyl polymer Polymers 0.000 claims description 9
- -1 hydroxy group hydrocarbon compound Chemical group 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 230000032683 aging Effects 0.000 claims description 7
- 150000002148 esters Chemical class 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 7
- YYROPELSRYBVMQ-UHFFFAOYSA-N 4-toluenesulfonyl chloride Chemical compound CC1=CC=C(S(Cl)(=O)=O)C=C1 YYROPELSRYBVMQ-UHFFFAOYSA-N 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000003063 flame retardant Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 5
- DQFBYFPFKXHELB-UHFFFAOYSA-N Chalcone Natural products C=1C=CC=CC=1C(=O)C=CC1=CC=CC=C1 DQFBYFPFKXHELB-UHFFFAOYSA-N 0.000 claims description 4
- 235000005513 chalcones Nutrition 0.000 claims description 4
- 229960002725 isoflurane Drugs 0.000 claims description 4
- 239000011877 solvent mixture Substances 0.000 claims description 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims description 3
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 3
- 239000006096 absorbing agent Substances 0.000 claims description 3
- 238000007259 addition reaction Methods 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- WHHGLZMJPXIBIX-UHFFFAOYSA-N decabromodiphenyl ether Chemical compound BrC1=C(Br)C(Br)=C(Br)C(Br)=C1OC1=C(Br)C(Br)=C(Br)C(Br)=C1Br WHHGLZMJPXIBIX-UHFFFAOYSA-N 0.000 claims description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 229940059574 pentaerithrityl Drugs 0.000 claims description 3
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 3
- 150000004986 phenylenediamines Chemical group 0.000 claims description 3
- 229920006149 polyester-amide block copolymer Polymers 0.000 claims description 3
- 229940095064 tartrate Drugs 0.000 claims description 3
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 claims description 3
- AUSHDWFFQTZGHL-UHFFFAOYSA-N C(C)C1NC(OC1)C(CCC)C Chemical class C(C)C1NC(OC1)C(CCC)C AUSHDWFFQTZGHL-UHFFFAOYSA-N 0.000 claims description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- 239000005058 Isophorone diisocyanate Substances 0.000 claims description 2
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 238000010790 dilution Methods 0.000 claims description 2
- 239000012895 dilution Substances 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 claims description 2
- 239000003973 paint Substances 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000002253 acid Substances 0.000 abstract description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract description 3
- 239000004814 polyurethane Substances 0.000 abstract description 3
- 229920002635 polyurethane Polymers 0.000 abstract description 3
- 238000005507 spraying Methods 0.000 abstract description 3
- 239000003513 alkali Substances 0.000 abstract description 2
- 229910021529 ammonia Inorganic materials 0.000 abstract description 2
- 239000004202 carbamide Substances 0.000 abstract description 2
- 238000004132 cross linking Methods 0.000 abstract description 2
- 238000010292 electrical insulation Methods 0.000 abstract description 2
- 150000005846 sugar alcohols Polymers 0.000 abstract 3
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000007711 solidification Methods 0.000 abstract 1
- 230000008023 solidification Effects 0.000 abstract 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 239000002585 base Substances 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 230000001681 protective effect Effects 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000012948 isocyanate Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 230000002421 anti-septic effect Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 150000002513 isocyanates Chemical class 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 230000037452 priming Effects 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- GLGSZERYOLHNML-UHFFFAOYSA-N $l^{1}-oxidanyl(phenyl)methanone Chemical compound [O]C(=O)C1=CC=CC=C1 GLGSZERYOLHNML-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241001112258 Moca Species 0.000 description 1
- WYNCHZVNFNFDNH-UHFFFAOYSA-N Oxazolidine Chemical compound C1COCN1 WYNCHZVNFNFDNH-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 238000003916 acid precipitation Methods 0.000 description 1
- 239000003619 algicide Substances 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000003373 anti-fouling effect Effects 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical compound C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- HKKDKUMUWRTAIA-UHFFFAOYSA-N nitridooxidocarbon(.) Chemical compound [O]C#N HKKDKUMUWRTAIA-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 150000002917 oxazolidines Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000007348 radical reaction Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
Abstract
Description
序号 | 项目 | 技术指标 | 检测依据 | 备注 |
1 | 固定含量(%) | ≥50 | GB1725-79 | |
2 | 附着力(级) | 1 | GB1720-79 | |
3 | 表干时间(h) | 0.5~3 | GB1728-79 | 根据不同用途可调整 |
4 | 实干时间(h) | ≤14 | GB1728-79 | |
5 | 耐冲击性(kg/cm2) | 50 | GB/T1732-93 | |
6 | 耐磨性(mg) | 36 | ||
6 | 柔韧性(mm) | 1 | GB/T1731-93 | |
7 | 硬度 | 0.65 | GB/T1730-93 | |
8 | 耐酸性浸入10%HCL溶液中(480h) | 无变化 | GB9274-88 | |
9 | 耐碱性浸入10%NaOH溶液中(480h) | 无变化 | GB9274-88 | |
10 | 耐盐雾试验1000h | 无变化 | GB/T1771-91 | |
11 | 耐电压(2000v,1min) | 无击穿,无闪络 | ||
12 | 苯(%) | 未检出 | GB18581-2001 | |
13 | 甲苯(%) | 未检出 | GB18581-2001 | |
14 | 甲苯二异氰酸脂(%) | 0.6 | GB/T18446-2001 | 限量值≤0.7 |
15 | 总挥发性有机物(g/l) | 436 | GB/T6751-1986 | 限量值≤600 |
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100214219A CN1326961C (zh) | 2004-03-19 | 2004-03-19 | 一种高强防腐涂料及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100214219A CN1326961C (zh) | 2004-03-19 | 2004-03-19 | 一种高强防腐涂料及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1563232A CN1563232A (zh) | 2005-01-12 |
CN1326961C true CN1326961C (zh) | 2007-07-18 |
Family
ID=34479811
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2004100214219A Expired - Fee Related CN1326961C (zh) | 2004-03-19 | 2004-03-19 | 一种高强防腐涂料及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1326961C (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102863606A (zh) * | 2011-07-08 | 2013-01-09 | 贺孝敏 | 一种环境友好型单组分潮气固化的预聚体树脂及其制备方法和应用 |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100500777C (zh) * | 2006-06-13 | 2009-06-17 | 大连科盾防腐新材料有限公司 | 一种聚氨酯导静电防腐涂料 |
CN102786870B (zh) * | 2012-08-28 | 2014-07-09 | 山东大学 | 一种聚脲防腐涂层制备方法 |
CN107606013B (zh) * | 2017-07-25 | 2020-02-18 | 浦江县顺光科技有限公司 | 一种通过弹簧控制的档位机构 |
CN111187563B (zh) * | 2020-03-10 | 2022-07-15 | 顺缔高新材料江苏有限公司 | 一种高粘结力耐水解聚脲专用底涂料及其制备方法 |
CN114456694A (zh) * | 2022-01-07 | 2022-05-10 | 湖南航天三丰科工有限公司 | 一种聚氨酯底漆及面漆组合涂料 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4304706A (en) * | 1979-10-24 | 1981-12-08 | Urs Bhaskar R | Method for preparing a color pigmented moisture curing polyurethane coating |
CN85104738A (zh) * | 1984-05-29 | 1986-12-24 | 吴·勒·戈尔合作有限公司 | 聚氨酯类预聚物与高弹体 |
CN1089965A (zh) * | 1992-12-17 | 1994-07-27 | 格雷斯公司 | 具有增强的防腐性能的新型聚氨酯组合物 |
US5925781A (en) * | 1997-11-03 | 1999-07-20 | Bayer Corporation | Prepolymers with low monomeric TDI content |
JPH11322879A (ja) * | 1998-05-21 | 1999-11-26 | Asahi Chem Ind Co Ltd | 一液湿気硬化型ポリイソシアネート組成物 |
CN1471548A (zh) * | 2000-10-23 | 2004-01-28 | 亨茨曼国际有限公司 | 基于mdi预聚物的高性能密封胶配方 |
-
2004
- 2004-03-19 CN CNB2004100214219A patent/CN1326961C/zh not_active Expired - Fee Related
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4304706A (en) * | 1979-10-24 | 1981-12-08 | Urs Bhaskar R | Method for preparing a color pigmented moisture curing polyurethane coating |
CN85104738A (zh) * | 1984-05-29 | 1986-12-24 | 吴·勒·戈尔合作有限公司 | 聚氨酯类预聚物与高弹体 |
CN1089965A (zh) * | 1992-12-17 | 1994-07-27 | 格雷斯公司 | 具有增强的防腐性能的新型聚氨酯组合物 |
US5925781A (en) * | 1997-11-03 | 1999-07-20 | Bayer Corporation | Prepolymers with low monomeric TDI content |
JPH11322879A (ja) * | 1998-05-21 | 1999-11-26 | Asahi Chem Ind Co Ltd | 一液湿気硬化型ポリイソシアネート組成物 |
CN1471548A (zh) * | 2000-10-23 | 2004-01-28 | 亨茨曼国际有限公司 | 基于mdi预聚物的高性能密封胶配方 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102863606A (zh) * | 2011-07-08 | 2013-01-09 | 贺孝敏 | 一种环境友好型单组分潮气固化的预聚体树脂及其制备方法和应用 |
Also Published As
Publication number | Publication date |
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CN1563232A (zh) | 2005-01-12 |
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