CN1312238A - Amino acid chelate fertilizer producing process - Google Patents
Amino acid chelate fertilizer producing process Download PDFInfo
- Publication number
- CN1312238A CN1312238A CN00104213A CN00104213A CN1312238A CN 1312238 A CN1312238 A CN 1312238A CN 00104213 A CN00104213 A CN 00104213A CN 00104213 A CN00104213 A CN 00104213A CN 1312238 A CN1312238 A CN 1312238A
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- CN
- China
- Prior art keywords
- amino acid
- acid chelate
- chelate fertilizer
- hydrolysis
- fertilizer
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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- Fertilizers (AREA)
Abstract
The production process of amino acid chelate fertilizer is characterized by that the chelate fertilizer is prepared by using the sludge from production of brewing beer as raw material, and the combination of yeast autolysis with compound enzyme hydrolysis to prepare amino acid liquor, then chelating the amino acid liquor with trace elements, and its process flow is as follows: enzyme mother sludge, press filtering, autolysis, hydrolysis by adding enzyme, filtering, batching, chelating, cooling, filtering, compounding and packaging finished product. It contains 18 amino acids and several trace elements necessary for growth of plant, can be used as high-efficiency foliage fertilizer, and can raise the yield of crops.
Description
The present invention relates to a kind of production method of amino acid chelate fertilizer, it belongs to the mixture class and the production method thereof of organic fertilizer and various trace elements.
The production of amino acids fertilizer normally adopts the protein raw material hydrolysis to make the mixed amino acid solution, makes through composite again.The preparation of aminoacids solution has acid hydrolyzation and enzymolysis process, and the amino acid fertilizer of domestic production at present all is to adopt acid hydrolyzation production.Though the acid hydrolyzation cost is low, this method needs strong acid, high temperature, and essential amino acids tryptophan is destroyed.And the enzymolysis process mild condition, amino acid is not destroyed, and configuration does not change.But enzymolysis process production generally exists hydrolysis thorough inadequately, the problem that percent hydrolysis is not high.
In order to improve the deficiency of enzymolysis process, purpose of the present invention is the enzymolysis novel process that provides a kind of percent hydrolysis high, is raw material with beer mud, adopts yeast autolysis to combine with combinative enzyme hydrolysis, again with the trace element chelated amino acid chelate fertilizer that makes.
Raw material and weight percent content thereof that amino acid chelate fertilizer of the present invention is required are respectively: yeast slurry (in butt) 50-60%, and proteinase-10 .1-0.2%, mineral element 1-3%, water 30-40%, mineral element can adopt Cu, Fe, Mn, Zn, B, Mo etc.
The producing and manufacturing technique of amino acid chelate fertilizer of the present invention is:
Yeast slurry → press filtration → self-dissolving → add enzymic hydrolysis → filtration → batching → chelating → cooling → filtration → composite → finished product packing.Now processing method is specified as follows:
1. yeast slurry press filtration: beer fermentation finishes, and discharges yeast slurry through the plate-and-frame filter press press filtration from pot bottom, gets filter cake and is used for hydrolysis.
2. self-dissolving is handled: will filter the yeast slurry of doing and add in the biochemical reaction pot, 1: 0.8 water is added in metering, adds 5% MgCL
2Make autolysis promoter, start agitator, and feed steam and slowly heat up, be raised to 48 ℃, be incubated 6 hours through 2 hours.
3. enzymolysis processing: transfer PH=7 with phosphoric acid, slowly be warmed up to 50-60 ℃, the compound protease that adds distiller's yeast mud amount (in butt) 0.1%-0.2%, in initial 6 hours, stirred 5 minutes every 2 hours, static then, allow it clarify naturally, the reaction times is 20 hours altogether, filter, get filtrate for later use.Above-mentioned used compound protease is to be cooperated in 1: 1 ratio by inscribe peptase and circumscribed peptase to form.
4. prepare burden: hydrolyzed solution is put in the ingredients pot, be warming up to 50 ℃-60 ℃, add trace element fertilizer, carried out chelatropic reaction 30 minutes, cooled and filtered, the alkylphenol polyoxyethylene that adds gross weight 1% is re-dubbed emulsion, and metering filling gets product.Adopt this technology, protein degree is more than 90%, and protein recovery is more than 85%.
Amino acid chelate fertilizer of the present invention can be used as efficient foliage spray.It contains needed 18 seed amino acids of plant-growth and various trace elements.Amino acid whose total content is about 15%, is about 10% with trace element chelated amino acid wherein.Crop sprays amino acid chelate fertilizer and can enhance metabolism, and improves the photosynthesis ability of farm crop, strengthens growth potential, improves output, improves quality.
Amino acid chelate fertilizer of the present invention has carried out the multiple spot field test on vegetables, tealeaves, tobacco, all obtain good effect, vegetables volume increase 20-30%; Tealeaves volume increase 15-20% improves tea leaf quality; Tobacco leaf volume increase 15-25%, and the grade of raising tobacco leaf.
Claims (4)
1. the production method of an amino acid chelate fertilizer is characterized in that, production process is: yeast slurry → press filtration → self-dissolving → add enzymic hydrolysis → filtration → batching → chelating → cooling → filtration → composite → finished product packing.
2. the production method of amino acid chelate fertilizer as claimed in claim 1 is characterized in that, when hydrolysis treatment, adds 5% MgCL
2Make autolysis promoter, and under 48 ℃ of conditions, be incubated 6 hours.
3. the production method of amino acid chelate fertilizer as claimed in claim 1 is characterized in that, during enzymolysis processing, transfers PH=7 with phosphoric acid, adds 0.1%～0.2% compound protease of mashed yeast butt amount, and hydrolysis is 20 hours under 50-60 ℃ of condition.
4. the production method of amino acid chelate fertilizer as claimed in claim 3 is characterized in that used compound protease is to be cooperated in 1: 1 ratio by inscribe peptase and circumscribed peptase to form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00104213A CN1312238A (en) | 2000-03-08 | 2000-03-08 | Amino acid chelate fertilizer producing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00104213A CN1312238A (en) | 2000-03-08 | 2000-03-08 | Amino acid chelate fertilizer producing process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1312238A true CN1312238A (en) | 2001-09-12 |
Family
ID=4577217
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN00104213A Pending CN1312238A (en) | 2000-03-08 | 2000-03-08 | Amino acid chelate fertilizer producing process |
Country Status (1)
| Country | Link |
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| CN (1) | CN1312238A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100369867C (en) * | 2006-09-01 | 2008-02-20 | 陈景华 | Highly effective ecology animal and plant nutriment, preparation method and application thereof |
| WO2010063195A1 (en) * | 2008-12-02 | 2010-06-10 | 安琪酵母股份有限公司 | Feed premix containing multiple trace elements and preparing method thereof |
| EP2128114A3 (en) * | 2008-05-28 | 2011-12-28 | Heineken España, S.A. | Procedure for obtaining a fertilizing product from beer production waste |
| EP2719289A1 (en) * | 2012-10-12 | 2014-04-16 | SC Medisan 2010 SRL | Process for obtainment of amino acids chelates with micro-elements |
| CN105198665A (en) * | 2014-06-06 | 2015-12-30 | 江苏植丰生物科技有限公司 | Amino acid water-soluble fertilizer and preparation method thereof |
| CN105272478A (en) * | 2015-11-17 | 2016-01-27 | 烟台泓源生物肥料有限公司 | Water-soluble protein peptide fertilizer |
| CN105819957A (en) * | 2016-03-17 | 2016-08-03 | 陕西先农生物科技有限公司 | Enzyme and amino acid containing aromatic liquid fertilizer prepared by inferior-quality fruit combined enzyme method and preparation method thereof |
| CN105967761A (en) * | 2016-05-26 | 2016-09-28 | 陈可夫 | Method for producing amino acid water-soluble fertilizer by utilizing Drawida Japonica Michelsen |
| CN106478271A (en) * | 2016-11-10 | 2017-03-08 | 云南农业大学 | A kind of water-soluble fertilizer of aminoacid containing enzymatic isolation method and preparation method thereof |
| CN110128213A (en) * | 2019-06-19 | 2019-08-16 | 乐斯福(明光)有限公司 | A method of liquid fertilizer is produced using beer waste yeast |
| CN112209784A (en) * | 2020-11-02 | 2021-01-12 | 中国科学院沈阳应用生态研究所 | Synergistic stable compound fertilizer and preparation method thereof |
| CN112321361A (en) * | 2020-11-02 | 2021-02-05 | 中国科学院沈阳应用生态研究所 | Synergistic stable nitrogenous fertilizer and preparation method thereof |
-
2000
- 2000-03-08 CN CN00104213A patent/CN1312238A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100369867C (en) * | 2006-09-01 | 2008-02-20 | 陈景华 | Highly effective ecology animal and plant nutriment, preparation method and application thereof |
| EP2128114A3 (en) * | 2008-05-28 | 2011-12-28 | Heineken España, S.A. | Procedure for obtaining a fertilizing product from beer production waste |
| WO2010063195A1 (en) * | 2008-12-02 | 2010-06-10 | 安琪酵母股份有限公司 | Feed premix containing multiple trace elements and preparing method thereof |
| EP2719289A1 (en) * | 2012-10-12 | 2014-04-16 | SC Medisan 2010 SRL | Process for obtainment of amino acids chelates with micro-elements |
| CN105198665A (en) * | 2014-06-06 | 2015-12-30 | 江苏植丰生物科技有限公司 | Amino acid water-soluble fertilizer and preparation method thereof |
| CN105272478A (en) * | 2015-11-17 | 2016-01-27 | 烟台泓源生物肥料有限公司 | Water-soluble protein peptide fertilizer |
| CN105819957A (en) * | 2016-03-17 | 2016-08-03 | 陕西先农生物科技有限公司 | Enzyme and amino acid containing aromatic liquid fertilizer prepared by inferior-quality fruit combined enzyme method and preparation method thereof |
| CN105967761A (en) * | 2016-05-26 | 2016-09-28 | 陈可夫 | Method for producing amino acid water-soluble fertilizer by utilizing Drawida Japonica Michelsen |
| CN106478271A (en) * | 2016-11-10 | 2017-03-08 | 云南农业大学 | A kind of water-soluble fertilizer of aminoacid containing enzymatic isolation method and preparation method thereof |
| CN110128213A (en) * | 2019-06-19 | 2019-08-16 | 乐斯福(明光)有限公司 | A method of liquid fertilizer is produced using beer waste yeast |
| CN112209784A (en) * | 2020-11-02 | 2021-01-12 | 中国科学院沈阳应用生态研究所 | Synergistic stable compound fertilizer and preparation method thereof |
| CN112321361A (en) * | 2020-11-02 | 2021-02-05 | 中国科学院沈阳应用生态研究所 | Synergistic stable nitrogenous fertilizer and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| ASS | Succession or assignment of patent right |
Owner name: KUMIN GUOZONG BIOLOGY ENGINEERING CO., LTD. Free format text: FORMER OWNER: AIDI BIOLOGICAL TECHN INST., YUNAN Effective date: 20020705 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20020705 Address after: 650011 Yunnan city of Kunming province Shu Lin Jie Shulin garden 5 Applicant after: Kunming Guozhong Biological Engineering Co. Ltd. Address before: 650021 Yunnan city in Kunming Province, the Provincial Association for science and Technology Road No. 22 Building 5 Applicant before: Aidi Bio-Technology Inst, Yunnan |
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |