CN1299614A - Superfine fresh bone powder and its production process and use - Google Patents
Superfine fresh bone powder and its production process and use Download PDFInfo
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Abstract
The present invention relates to a superfine fresh bone powder and its production method, special-used in the field of food additive and health-care food processing technology. Said superfine fresh bone powder contains organic nutrients of protein, etc. and its water content is less than 8%. Its production process includes the following steps: cleaning shoulder bone, removing impurity, dewatering, coarse grinding, secondary crushing, fine grinding and superfine grinding which are continuously implemented at 75-85 deg.C. Said invention provides a new health-care food additive, and its production process is simple.
Description
Superfine fresh bone meal of the present invention and production method thereof and usage are exclusively used in food additives and health food processing and fabricating field.
Animal skeleton accounts for trunk 10～15%, and it enriches the bone source electrode.Bright poultry bone has multivalence nutrition, and mammal is for its own existence and produce offspring, and nutrition in a large number are stored in the bone.According to japanese food analysis center data, contain 18 seed amino acids such as glutamic acid, aspartic acid in the Fresh Os Sus domestica, 27 kinds of trace elements such as calcium, phosphorus, iron, necessary or the useful factor of human bodies such as rich in protein, lecithin, vitamin, unrighted acid, only compare with the contained micro-parameter of Fresh Os Sus domestica and pork, the calcium in the pig bone is that (3.1: 0.005) iron, the zinc etc. more than 600 times of its meat also all are more than 3 times of its meat.The output of the annual fresh pig bone of China reaches more than 400 ten thousand tons, has only wherein seldom that a part is used to make ossified oil, feed bone powder etc., and major part has gone out of use.If can utilize half processing and eating wherein, this just has been equivalent to increase by 2,000,000,000 kilograms meat, also just equals to have supported more than 4,000 ten thousand pigs more, can save the tens billion of kilograms of feed grain every year.Contain abundant calcium, phosphorus, iron, zinc, magnesium and multiple organic nutrition composition in the animal skeleton, the international market has become focus to the development and use of bone ware in recent years.Bone meal is the first-selected calcium tonic of generally acknowledging in the world, but technical barriers such as processing technology, fine granularity, content of beary metal, security have hindered the development of bone meal as best calcium tonic all the time in actual applications.
Utilize that nutritional resource all has the guide both at home and abroad in the bright bone, the international market develops bright bone ware already.Japan and American-European countries researched and developed bright bone product and obtained gratifying results the beginning of the eighties.As the bright bone of the animal fresh bone senior nutrition of exploitations such as the company like a chain of pearls or a string of beads of the U.S., Britain Lensfield company stick with paste, the fresh bone paste series products is in great demand so far.The very farsighted nutrition expert of China eats the custom that meat is abandoned bone in view of people, is devoted to the development and use of nutritional resource in the bright bone already.But owing to domestic process equipment of past does not reach the reasons such as control problem of certain fineness and sanitary index, this processing industry development is slower, also rests on the dried bone process segment.The home and abroad is generally adopted steaming, is boiled or method of calcination the preparation of bone meal according to reports, most of nutrition is run off or destroy, and fineness does not pass a test, and heavy metal is especially plumbous, arsenic content height.Bright bone is stuck with paste, because moisture too high, store, transport and guarantee the quality especially by inconvenience for the fresh bone paste series products.
The object of the present invention is to provide superfine fresh bone meal and production method thereof and usage, overcome in the prior art and to steam, to boil or defective that nutrition that calcining, grinding technics bring is destroyed, make product have characteristics such as ultrafine, safety and sanitation, the bright bone organic nutrition of maintenance composition, and the difficult problem in the solution machining process, dry superfine fresh bone meal is provided, make its product water content below 8%, use it for the reinforcement calcium source that makes varieties of food items.
Superfine fresh bone meal provided by the present invention, its composition is as follows:
Protein, 10～31% (M/M, Hereinafter the same); Fat, 5～15%; Moisture content, 1.0～8%; Calcium (in Ca), 5～17.0%; Phosphorus (in P), 2.5～8.5%; Peroxide value≤40meq/kg, lead (in Pb)≤0.5mg/kg, arsenic (in As)≤0.5mg/kg, all the other are bone nutrition.
Above-mentioned superfine fresh bone meal also contains: zinc (in Zn) 〉=0.08%; Iron (in Fe) 〉=0.03%.Be little bloom powder, no gritty sense, free from extraneous odour, free from admixture, special bone fragrance flavor arranged, particle≤100 μ m.
The production method of superfine fresh bone meal provided by the present invention comprises: 1) clean: select for use fresh bone of fowls and animals to make raw material, raw material is cleaned, to meet hygienic requirements; 2) dehydration: the moisture content that adopts dewaterer will adhere to bone surface is sloughed; 3) coarse crushing: the raw material of dehydration is slowly put into Roughpulverizer with every crowd of 10～15kg, carry out coarse crushing with load rate; 4) secondary is pulverized: the skeletal grain through coarse crushing changes one-level roller-type pulverizer extruding pulverizing over to every crowd of 10～15kg, pushes pulverizing repeatedly, makes particle reach 0.3～0.5mm; 5) in small, broken bits: material changes the extruding of secondary roller-type pulverizer over to every crowd of 10～15kg and pulverizes, in the extruding drum temperature is under 75～85 ℃ of states, the progressive rotating shaft spacing of turning down, the repetitiousness extruding, the terminal composition granule is 180～150 μ m, carry out simultaneously and connect oil work, material is put into all rotating disks and is entered next procedure, and empty machine moves to cooling; 6) ultra-fine: material changes three grades of roller-type pulverizers over to every crowd of 10～15kg, is under 75～85 ℃ of states in the extruding drum temperature, the progressive rotating shaft spacing of turning down, extruding is pulverized repeatedly, terminal material particles≤100 μ m, mechanical empty machine moves to cooling, and material is put into all rotating disks and is changed next procedure over to; 7) cooling, the packing: cool to room temperature, change over to bulk machine bulk after, the product vacuum packaging.
Can also add air-flow in above-mentioned cooling, packet assembler pulverizes or freezing pulverizing process: promptly at cool to room temperature, change the bulk back of bulk machine over to:
Material is added the airslide disintegrating mill spout, and pulverizing the processing cavity input pressure to air-flow is that 1-1.5 MPa (MPa), temperature are 0-5 ℃, the aseptic cold air that dries, and in air-flow is pulverized processing cavity material is carried out air-flow and collides processing;
Perhaps material is added the freezing crusher spout, in freezing crusher, material is reduced the temperature to-150--200 ℃ and carry out freezing pulverization process, product vacuum packaging with liquid nitrogen.
Used bright collagen material is preferably bright pork shoulder bone.
The usage of above-mentioned superfine fresh bone meal comprises: as calcium tonic, use according to national dietary reference intake standard (DRIS, in October, 2000 Ministry of Public Health's promulgation); Add superfine fresh bone meal and strengthen as high-quality calcium source in varieties of food items goods such as biscuit, instant noodles, bowel lavage, meat pulp, dried meat floss, addition is 10-20% (M/M is in dry), in calcic 15%.
Superfine fresh bone meal provided by the present invention is the comprehensive development and utilization animal fresh bone to improve the national general calcium deficiency nutrition condition of China, and a high-quality calcium source and nutritional health food are provided.Owing to superfine fresh bone meal gets with the physics mode processing, nutrition all exists with original form of natural biological structure.And animal skeleton composition and physiognomy are like (contained composition and ratio are also close, all are 2: 1 as calcium-phosphorus ratio).Human tissue cell's material has stronger affinity (being tissue specificity) for homologue's cell.The polypeptide huge legendary turtle compound of natural formation in the animal fresh bone, acid mucopolysaccharide macromolecular compound be the peculiar composition that constitutes animal connective tissue, thereby the absorption rate of superfine fresh bone meal are higher.Calcium biological function research in the superfine fresh bone meal goods that Nanjing Railway College of Medicine of national appointment does, other calcium activated of superfine fresh bone meal comparison, chemical synthesis class calcium preparation both be beneficial to absorption of human body, were beneficial in the skeleton again to retain, and increased bone density.And can not cause calcium and other trace element out of proportion.Superfine fresh bone meal can provide multivalence nutrition to human body.Show that after deliberation superfine fresh bone meal has following characteristic: (1) pure natural property; (2) calcium absorptivity and retain the rate height; (3) safe; (4) nutritious; (5) calcium, phosphorus ratio are reasonable.Can be added in the numerous food as the nourishing additive agent that improves the food class.
Processing technology provided by the invention has overcome in the prior art the defective of its nutritions of mode heavy damage such as bright bone thermophilic digestion, calcination, electric mill, grinding, employing is through fixed point meat processing combine, locality veterinary hygiene department quarantines, and (the pig bone is low than the ox bone content of beary metal for the Fresh Os Sus domestica of providing no infecting both domestic animals and human eqpidemic disease document, test shows that wherein pork shoulder bone content of beary metal is minimum), the ultra-fine degreasing of attrition crushing is pulverized under 75～85 ℃ of temperature controls, and heavy metal free mechanicalness band dyes.Product fineness evenly reaches the human body following particles of easy degree of absorption 100 μ m (solvable under identical pH value with human gastric juice), through air-flow collision or the freezing average diameter of pulverizing back bone meal particle is: 3-20 μ m.Moisture all is lower than country or international food standard.Through experiment, raw material produces under the state of powerful attrition crushing and discharges the moment heat in this technology, and harmful microorganism can not be survived, and product reaches hygienic index.The bone calcium absorptivity is up to 59.6%, and the rate of retaining reaches 49%, rich protein and 17 seed amino acid several mineral materials, vitamin, a kind of really polyauxotrophic high-quality calcium source.Its technology has solved technical barriers such as the fine granularity that do not have nearly half a century to solve, content of beary metal, security, and extensive use in industries such as Flour product, biscuit, meat, milk products now obtained remarkable social benefit and economic benefit.
The electromicroscopic photograph of Fig. 1 bone meal
Fig. 2 hangs down calcium model group (♀) * 100
Fig. 3 low dose group (♀) * 100
Dosage among Fig. 4 (♀) * 100
Fig. 5 high dose group (♀) * 100
Embodiment:
One. materials and methods
1. bright collagen material: from Pest-or disease-free area animal-slaughtering in fixed place field, slaughter back pork and cut apart the bright shoulder blade of rejecting the muscle tendon and adhering to muscle, it is freezing standby to go into storehouse below-15 ℃.
2. key instrument equipment:
Instrument: S-450 ESEM, UV-754 spectrophotometer, micrometer, microscope etc.
Equipment: disintegrating machine, vacuum roller press, vacuum mixing filling machine, vacuum-packed sealing machine, DRG series pulverizer, micro-wave oven, drying box, centrifuge etc.
3. the method for inspection: the various physics and chemistry of product (comprising nutrition) index all adopts existing national standard method, tests as GB12398, GB5009 etc. and radioimmunology etc.
4. biological test: carry out with reference to China's health food functional experiment method.
Experimental animal is about big white mouse SD strain body weight 50g, male and female half and half totally 60 provide by Nanjing Medical University, experimental period is 135 days.Experiment grouping and main feed composition see Table 1.
5. statistical analysis technique: experimental data all adopts epidemiology statistics software (EP15) to handle.Respectively organize the average and the standard deviation of data with variance analysis, X ± SD represents; The T check is carried out the significance of difference and is judged.
Two. the result
(1) superfine fresh bone meal production technology
(1) cleans: select for use the bright bone of pig to make raw material, raw material is carried out strictness clean, to meet hygienic requirements.
(2) dehydration: the moisture content that adopts dewaterer will adhere to bone surface is sloughed.
(3) coarse crushing: the raw material of dehydration is evenly slowly put into Roughpulverizer, carry out coarse crushing with load rate.
(4) secondary is pulverized: the skeletal grain through coarse crushing changes one-level DRG series pulverizer over to every crowd of 10～15kg, pushes pulverizing repeatedly, makes particle reach 0.3～0.5mm.This process is approximately carried out 10～15min.
(5) in small, broken bits: material changes secondary DRG series pulverizer over to every crowd of 10～15kg.Regulate the rotating shaft spacing in advance, material is slowly poured in zero load start preheating down into when temperature reaches 75～85 ℃, and repetitiousness pushes about 25min, about 180～150 μ m of terminal composition granule.This process flows out through being extruded with oil because of material, just must carry out the oil work that connects.Material is put into all rotating disks and is entered next procedure, and empty machine moves to cooling.
(6) ultra-fine: material changes three grades of DRG series pulverizers over to every crowd of 10～15kg.Regulate the rotating shaft spacing in advance, material is slowly poured in zero load start preheating down into when temperature reaches 75～85 ℃, the progressive rotating shaft spacing of turning down, and 25min is approximately carried out in extruding repeatedly, terminal material particles≤100 μ m, mechanical empty machine moves to cooling.Material is put into all rotating disks and is changed next procedure over to.
(7) cooling, packing: cool to room temperature, change over to bulk machine bulk after, product can be vacuum-packed, also can increase with next process:
Material is added the airslide disintegrating mill spout, and pulverizing the processing cavity input pressure to air-flow is that 1-1.5 MPa (MPa), temperature are 0-5 ℃, the aseptic cold air that dries, and carries out air-flow and collide processing in air-flow is pulverized processing cavity;
Perhaps material is added the freezing crusher spout, in freezing crusher, material is reduced the temperature to-150--200 ℃ and carry out freezing pulverization process, product vacuum packaging with liquid nitrogen.
(2) main nutrition, harmful element (see Table 2, table 3) and microorganism
Micro biological Tests result through 6 batch samples all is lower than company standard.Total plate count＜800cf μ/g, coliform＜30MPN/100g, pathogenic bacteria (comprising pathogenic entero becteria and pathogenic coccus) all do not detect.
(3) granularity of superfine fresh bone meal
The electromicroscopic photograph of superfine fresh bone meal such as Fig. 1.Can find out from electromicroscopic photograph Fig. 1, the bone meal out-of-shape, not of uniform size, by measuring, the average diameter of bone meal particle is after the ultra-fine operation of process: 96.4 ± 38.48 μ m.Through air-flow pulverizing or the freezing average diameter of pulverizing back bone meal particle be: 3-20 μ m.
(4) biological experiment of superfine fresh bone meal calcium
1. calcium metabolism result of the test (table 4)
(1) calcium intake, excrement calcium discharge rate and urine calcium discharge rate:
Each metabilic stage each treated animal calcium intake difference is arranged, this is in the feed due to the calcium content difference, excrement calcium discharge rate, urine calcium discharge rate conform to calcium intake, promptly take in to discharge manyly more, take in few the discharge and lack.
(2) calcium uptake and absorptivity
By table 4 as seen, the calcium uptake conforms to intake.It is the highest at first metabilic stage that each organizes calcium absorptivity, descends gradually with experiment, minimum until the 4th metabilic stage, and this calcium absorptivity descends and belongs to normal phenomenon.In the metabolism experiment in earlier stage, the serious calcium deficiency of all animals, body needs a large amount of calcium thereby calcium absorptivity height.Replenish the calcium gradually with experiment, be general calcium deficiency to the 4th metabilic stage, body needs the calcium amount to present the phenomenon that calcium absorptivity reduces early stage less.Can think the serious calcium deficiency phase of body first, second metabilic stage, for vitamin D and normal 3 groups of calcium intake (middle dosage group) and 5 groups (calcium activated group), calcium absorptivity all reaches more than 70%.Can think the general calcium deficiency of body the 4th metabilic stage, 3 groups and 5 groups of calcium absorptivities are about 40%, and 5 groups are low slightly, but difference not significantly (P＞0.05), the visible high calcium absorptivity of superfine fresh bone meal is better than calcium activated; Low but the absorptivity height of 1 group of calcium uptake, the absorbing better of calcium, be because the activity in vivo vitamin D [1,25-(OH)
2D
3] under low calcium state, increase, promote intestines calcium to absorb.As for 4 groups (high dose group), the calcium uptake is apparently higher than 2,3 groups, and especially first, second and third metabilic stage is more obvious.
(3) calcium amount retained and retain rate
Calcium amount retained and the calcium utilization situation that retains rate reflection body.It is similar to absorptivity that calcium retains rate, also is that first metabilic stage is the highest, reduces gradually with experiment, minimum until the 4th metabilic stage.It is similar that 3 groups of serious calcium deficiency phases and 5 groups of calcium retain rate, is 70～80%.The 4th low thanks to 3 groups of phases and 5 groups of calcium rates of retaining are that 40～50%, 3 groups of calcium retain rate a little more than 5 groups, but difference not significantly (P＞0.05); And 4 groups had only 20～30%, compares difference extremely significantly (P＜0.01) with other each group.2,3,4 groups situation of change is consistent with calcium uptake and absorptivity, and the utilization rate of high calcium group is better than calcium activated in this experiment.
2. the measurement result of bone length, weight and bone density (see Table 5, table 6)
As shown in Table 5, difference (P＜0.05) that there are no significant between five groups of the femur lengths illustrates that long-term calcium deficiency do not have obvious influence to femur length.
1 group of femur weight is compared significant difference (P＜0.05) with 3 groups, compare difference extremely significantly (P＜0.01) with 4 groups for 1 group; Compare significant difference (P＜0.05) with 5 groups for 3 groups, compare difference extremely significantly (P＜0.01) with 5 groups for 4 groups.Difference (P＜0.05) that there are no significant between all the other each groups.The content difference of calcium in the feed is described, the femur weight of rat is had in various degree influence.Calcium content is high more in the feed, and then the femur of rat is heavy more.But 5 groups of height of 3 groups of femur weight ratios (P＜0.05) of same dose illustrate that the effect of supplemented calcium of high calcium group specific activity calcium will be got well.
1 group of femoral bmd is compared significant difference (P＜0.05) with 2 groups, compare difference extremely significantly (P＜0.01) with 3,4 groups for 1 group; Compare significant difference (P＜0.05) with 5 groups for 3 groups, compare difference extremely significantly (P＜0.01) with 5 groups for 4 groups.Difference (P＞0.05) that there are no significant between all the other each groups.The content difference of calcium in the feed is described, the femoral bmd of rat is had in various degree influence.Calcium content is high more in the feed, and then the femoral bmd of rat is big more; But 3 groups of femoral bmds of same dose are than 5 groups of height (P＜0.05), and the effect of supplemented calcium that further specifies the high calcium group is better than calcium activated.
As seen, focile weight and shin bone weight significance test of difference between each group shows that significant difference between 1 group and 3 groups, 4 groups (P＜0.05) is compared all not remarkable (P＞0.05) between all the other each groups.Illustrate that the low calcium feed of feeding for a long time can influence the growth of rat focile and shin bone.
Tibial metaphysis bone tissue section micro-shown in (seeing Fig. 2～5).
Because calcium deficiency makes the bone tissue can not calcification, rests on the osteoid tissue stage, causes osteoblast hyperplasia and increased functionality, the osteoclast number reduces simultaneously, the cortex of bone attenuation, and bone trabecula reduces, and attenuates, and branch disappears.Be that the speed that bone formation is slowed down absorbs the speed that slows down less than bone, cause osteoporosis.Because the pathology of cancellous bone is attached most importance to than cortex bone, thereby cortex of bone is changed significantly not as bone trabecula in this experiment.
By Fig. 4 Fig. 5 as seen, the shin bone microphoto shows that bone trabecula is thinning, attenuates, and the medullary substance chamber broadens, and inner red marrow is replaced by a large amount of adipocytes, show that osteoporosis has taken place to hang down calcium model group rat (the 135th day), its bone absorbs and bone forms the extremely active state that is in.
(5) application result
Beginning in 1997 in one class kindergarten, Nanjing to children surplus 70,000 as calcium tonic, every day, everyone 1g took, and went through 3 years, the result generally reacts appetite to be increased, resistance improves, cold reduces, nutrition condition is improved.According to 150 3-6 year children are tested observation, the result shows: the activity of bone alkaline phosphatase (BALP) test group has significant difference apparently higher than control group.By table 7 visible＜200 48 examples are than nearly 60% (P＜0.05) of control group 29 routine increase numbers, illustrates that to take the synthetic Gegenbaur's cell of superfine fresh bone meal more and can be converted into osteocyte, so the active decline of BALP.
The continent, Taiwan is unified food enterprise and was strengthened as the calcium nutritious supplementary pharmaceutical in instant noodles in 1999, is supervised by Chinese Soclety of Nutrition, sells in the whole nation, and annual sales reaches more than 350,000 tons.Not only satisfy the needs of the general calcium deficiency of numerous residents, improved social benefit, and before not strengthening, improved sales volume 15%.
Nanjing Yurun food Co., Ltd, the moderately well-off Food Co., Ltd in Xuzhou, Nanjing three great Food Co., Ltd are just adding superfine fresh bone meal and are strengthening as high-quality calcium source in goods such as bowel lavage, meat pulp, dried meat floss, Food Additives Used in China technical committee for standardization (TCST) passes above-mentioned reinforcement scope through discussion, and has listed China's food enrichment in by Ministry of Public Health's approval and used sanitary standard list (GB14880).
Produced ultra-fine bright bone calcium biscuit since 2000, addition is 10-20%, in calcic 15%, the heavy 6g of each piece biscuit, calcium content is 100mg, and children take 1/4 to 1/3 the amount of reinforcement that the 2-3 piece can obtain Ca-DRIS every day, and Jiangsu Province Department of Public Health approval is food of special nutrients, in Nanjing, ground nurseries and kindergartens mechanisms such as Suzhou, Wuxi, Nantong, Yangzhou, Zhenjiang, Shenzhen, Hefei, the Hangzhou snack food of replenishing the calcium as children, and will promote in other areas in the whole nation.
(6) standardization
As calcium-nutrition intensifying agent, the Department of Public Health of Shanxi Province's approval of bone meal biscuit is food of special nutrients to the approval of the national food additives of product technical committee for standardization (TCST) in meat products.
Superfine fresh bone meal has now formed company standard and has put on record through Jiangsu Province Bureau of Technical Supervision.The key technical indexes is as follows:
(1) sense organ: be little bloom powder, no gritty sense, free from extraneous odour, free from admixture, special bone fragrance flavor is arranged.
(2) physics and chemistry: protein 20～30%, calcium 〉=12%, phosphorus 7.8%, lipase 37～12%, moisture content≤8%, iron 〉=0.03%, zinc 〉=0.08%, peroxide value≤30meq/kg, lead (in Pb)≤0.5mg/kg, arsenic (in As)≤0.5mg/kg, particle≤100 μ m.
(3) microorganism: total plate count≤10000cfu/g, coliform≤90MPN/100g, pathogenic bacteria (duodenum 12 road pathogenic bacteria and pathogenic coccus) must not detect.
Three. discuss
Superfine fresh bone meal is the high-quality calcium source of solution crowd calcium deficiency.From experimental studies results, superfine fresh bone meal should be as first-elected high-quality calcium source, because superfine fresh bone meal calcium has following characteristic at least: 1) pure natural property.Be the utilization of a kind of bio-absorbable, do not have the pure natural calcium source of any intermediate and additive; 2) calcium absorptivity height.As seen thank to the phase animal at the third generation of general calcium deficiency by table 4, the absorptivity of middle calcium group can reach 56.9%, serious calcium deficiency second metabilic stage animal middle calcium group absorptivity can reach 68.9%, be higher than the calcium in other calcium sources at present commonly used and the milk; 3) calcium retains the rate height.By the visible third generation of the table 4 calcium group calcium rate of retaining in the phase animal of thanking is that the low calcium group at 55.1%, the second metabilic stage reaches 67.4%, illustrates that calcium is very high by the utilization rate of body.Therefore as seen can have by Fig. 3～5 and table 5, table 6, table 7 and improve osteoporotic function effectively; 4) safe.Adopt the minimum pig tabulare (shoulder blade) of Pb, As content as bright collagen material after deliberation, by the visible product P b of table 1, As content all＜below the 0.5mg/kg, microorganism all is lower than company standard; 5) many trophism.By the visible superfine fresh bone meal of table 2 and table 3 not only calcium content be higher than general calcium source, and contain other constants and micro-and the various organic nutrition compositions that constitute bone.6) ultrafine dust.Adopt advanced air-flow physical crushing technology, not only make product particle＜100 μ m, reach the fineness that people's physical efficiency absorbs, and kept all nutritions; 7) calcium, phosphorus ratio are reasonable.Ca by the visible superfine fresh bone meal of table 2: P=1.5: 1, meet the reasonable ratio that human body utilizes.
The main feed composition grouping of table 1 animal experiment
| The experiment grouping | Superfine fresh bone meal Ca counts (mg) | Protein (g) | Heat energy (kcal) |
| 1. (normal diet) | 47.9 | 13.0 | 570 |
| 2. (bone meal hangs down the calcium feed) | 250 | 13.5 | 575 |
| 3. (calcium feed in the bone meal) | 500 | 13.8 | 573 |
| 4. (bone meal high calcium feed) | 1000 | 13.9 | 571 |
| 5. (add the calcium activated feed) | 500 | 13.2 | 577 |
Main nutrition of table 2 superfine fresh bone meal and harmful element
| Project | Measure batch | Scope | Mean value |
| Protein % fat % moisture content % calcium (in Ca), % phosphorus (in P), % iron (in Fe), mg/kg zinc (in Zn), mg/kg magnesium (in Mg), % potassium (in K), % sodium (in Na), % | 6 6 6 6 6 6 6 6 6 6 | 29.6～31 7.54～7.72 2.8～3.2 10.4～17.0 7.85～7.9 31.0～36.0 87.8～88.4 | 30.0 7.6 3.0 7.88 34.0 81.0 0.35 0.10 0.39 |
| Plumbous (in Pb mg/kg), % arsenic (in As mg/kg), % | 6 6 | 0.3～0.34 0.3～0.35 | 0.33 0.30 |
The various amino acid contents of table 3 superfine fresh bone meal
| The amino acid title | Result (ng/100g) |
| Aspartic acid Su An Suan Silk propylhomoserin glutamic acid proline glycine alanine tyrosine methionine isoleucine leucine val phenyl alanine lysine histidine tryptophan arginine | 298.27??(1.91) 11?8.96?(0.76) 163.62??(1.04) 639.26??(4.04) 506.25??(3.25) 916.13??(5.88) 441.00??(2.83) 85.69???(0.55) 96.92???(0.62) 90.34???(0.58) 213.29??(1.37) 195.85??(1.26) 159.82??(1.03) 207.34??(1.33) 53.31???(0.34) 56.53???(0.04) 391.69??(2.51) |
Annotate: in the table bracket is the % that accounts for total amino acid content.
4 ( mg/5d ) ( mg/5d ) ( mg/5d ) ( mg/5d ) ( ％ ) ( mg/5d ) ( ％ ) 1 27.4±3.4 5.4±1.2 2.6±0.6 21.8±2.7 80.1±9.6 19.2±2.2 70.6±10.2 2 120.2±17.5 25.3±7.9 2.6±0.5 94.9±11.4 79.0±4.5 92.3±11.3 76.8±11.3 3 222.7±44.0 65.2±9.3 3.2±0.7 157.5±23.2 70.7±3.6 154.3±10.5 69.3±9.5 4 373.2±54.8 115.7±19.1 5.5±1.6 257.5±24.7 69.0±3.2 252.0±24.3 67.5±9.6 5 213.8±31.1 60.2±12.4 5.8±1.7 153.6±26.1 71.8±8.1 147.8±13.3 69.1±11.8 1 32.9±4.0 5.8±0.6 1.4±0.3 27.1±5.1 82.3±5.1 25.7±7.4 78.1±8.4 2 155.5±16.2 34.6±8.3 2.3±0.4 120.9±15.5 77.7±3.7 118.6±13.5 76.2±8.1 3 274.6±36.0 85.3±11.6 4.2±0.6 189.3±23.4 68.9±8.4 185.1±17.3 67.4±7.5 4 552.2±73.8 273.6±43.7 3.9±0.4 278.6±43.7 50.5±9.2 274.7±31.7 49.7±7.1 5 281.4±41.6 101.3±15.7 6.5±2.3 180.1±27.1 64.0±7.3 173.6±20.8 61.7±6.4 1 43.1±3.7 8.7±1.6 3.7±0.5 34.2±6.1 79.4±9.7 30.7±6.5 71.2±8.2 2 162.1±26.9 44.7±6.1 5.0±1.3 117.4±37.5 72.4±7.3 112.4±13.4 69.3±7.3 3 323.3±36.4 139.4±21.1 5.9±1.2 183.9±51.6 56.9±9.5 178.0±30.5 55.1±6.1 4 682.5±49.6 442.2±36.8 7.3±0.7 240.3±62.7 35.2±6.0 233±26.1 34.1±5.4 5 341.3±31.5 131.6±17.9 11.3±3.4 209.7±47.3 61.4±9.8 198.4±21.7 58.1±9.0 1 44.6±6.0 12.5±1.9 3.7±0.6 32.1±4.0 72.0±7.0 28.4±5.6 63.7±6.5 2 187.7±30.8 76.6±6.9 6.3±1.0 111.1±27.5 59.2±8.5 104.8±12.1 55.8±5.7 3 359.3±39.7 205.8±26.2 6.7±1.6 153.4±21.2 42.7±6.5 146.7±20.2 40.8±3.6 4 732.4±70.7 519.7±51.2 8.1±1.2 212.7±41.0 29.0±3.2 204.6±25.3 27.9±3.2 5 363.8±41.5 212.0±31.6 11.7±3.8 151.8±18.3 41.7±7.0 140.1±18.4 38.5±4.7
Annotate: calcium absorptivity=(calcium intake-excrement calcium discharge rate)/calcium intake * 100.
Calcium retains rate=(calcium intake-excrement calcium discharge rate-urine calcium discharge rate)/calcium intake * 100.
The length of table 5 femur, weight and bone density
Annotate: each organizes routine number average is 10.
*With 1 group of comparing difference remarkable (P＜0.05),
*With 1 group of poor heteropole remarkable (P＜0.01);
△With 5 groups of comparing differences remarkable (P＜0.05),
△ △With 5 groups of poor heteropoles remarkable (P＜0.01).
| Group | Length (cm) | Weight (g) | Bone density (g/cm 2) |
| 1 | 2.993±0.152 | 0.541±0.095 | 0.192±0.036 |
| 2 | 2.997±0.189 | 0.544±0.117 | 0.217±0.020 * |
| 3 | 3.050±0.116 | 0.599±0.086 *△ | 0.229±0.018 **△ |
| 4 | 3.057±0.162 | 0.659±0.109 **△△ | 0.240±0.039 **△△ |
| 5 | 2.904±0.204 | 0.540±0.088 | 0.205±0.047 |
Table 6 focile weight (g) and shin bone weight (g)
| Group | Focile weight (g) | Shin bone weight (g) |
| 1 | 0.283±0.057 | 0.450±0.095 |
| 2 | 0.294±0.041 | 0.453±0.107 |
| 3 | 0.317±0.043 * | 0.500±0.088 * |
| 4 | 0.338±0.052 * | 0.508±0.086 * |
| 5 | 0.305±0.045 | 0.479±0.109 |
Annotate:
*With 1 group of comparing difference remarkable (P＜0.05).
Table 7 test group and control group BALP specific activity are
| The BALP activity | Test group (routine number) | Control group (routine number) | X 2 | P |
| ＜200 | 48 | 29 | 6.31 | ＜0.05 |
| 200-250 | 87 | 104 | 4.16 | ＜0.05 |
| 250-300 | 15 | 17 | 0.14 | ＞0.05 |
Annotate: the result is provided by Nanjing woman health centre in the table.
Claims (7)
1, a kind of superfine fresh bone meal is characterized in that, contains following composition:
Protein, 10～31% (M/M, Hereinafter the same); Fat, 5～15%; Moisture content, 1.0～8%; Calcium (in Ca), 5～17.0%; Phosphorus (in P), 2.5～8.5%; Peroxide value≤40meq/kg, lead (in Pb)≤0.5mg/kg, arsenic (in As)≤0.5mg/kg, all the other are bone nutrition.
2, superfine fresh bone meal according to claim 1 is characterized in that, also contains: zinc (in Zn) 〉=0.08%; Iron (in Fe) 〉=0.03%.
3, superfine fresh bone meal according to claim 1 and 2 is characterized in that: be little bloom powder, no gritty sense, free from extraneous odour, free from admixture, special bone fragrance flavor arranged, particle≤100 μ m.
4, the production method of the described superfine fresh bone meal of one of claim 1-3 comprises:
1) cleans: select for use fresh bone of fowls and animals to make raw material, raw material is cleaned, to meet hygienic requirements;
2) dehydration: the moisture content that adopts dewaterer will adhere to bone surface is sloughed;
3) coarse crushing: the raw material of dehydration is slowly put into Roughpulverizer with every crowd of 10～15kg, carry out coarse crushing with load rate;
4) secondary is pulverized: the skeletal grain through coarse crushing changes one-level roller-type pulverizer extruding pulverizing over to every crowd of 10～15kg, pushes pulverizing repeatedly, makes particle reach 0.3～0.5mm;
5) in small, broken bits: material changes the extruding of secondary roller-type pulverizer over to every crowd of 10～15kg and pulverizes, in the extruding drum temperature is under 75～85 ℃ of states, the progressive rotating shaft spacing of turning down, the repetitiousness extruding, the terminal composition granule is 180～150 μ m, carry out simultaneously and connect oil work, material is put into all rotating disks and is entered next procedure, and empty machine moves to cooling;
6) ultra-fine: material changes three grades of roller-type pulverizers over to every crowd of 10～15kg, is under 75～85 ℃ of states in the extruding drum temperature, the progressive rotating shaft spacing of turning down, extruding is pulverized repeatedly, terminal material particles≤100 μ m, mechanical empty machine moves to cooling, and material is put into all rotating disks and is changed next procedure over to;
7) cooling, the packing: cool to room temperature, change over to bulk machine bulk after, the product vacuum packaging.
5, according to the production method of the described superfine fresh bone meal of claim 4, it is characterized in that: in cooling, the packet assembler,, change the bulk back of bulk machine at the material cool to room temperature:
Material is added the airslide disintegrating mill spout, and pulverizing the processing cavity input pressure to air-flow is that 1-1.5 MPa (MPa), temperature are 0-5 ℃, the aseptic cold air that dries, and in air-flow is pulverized processing cavity material is carried out air-flow and collides processing;
Perhaps material is added the freezing crusher spout, in freezing crusher with liquid nitrogen material is reduced the temperature to-150--200 ℃ carries out freezing pulverization process, product vacuum packaging.
6, according to the production method of claim 4 or 5 described superfine fresh bone meals, it is characterized in that: used bright collagen material is bright pork shoulder bone.
7, the usage of the described superfine fresh bone meal of one of claim 1-3 comprises:
As calcium tonic, use according to national dietary reference intake standard;
Add superfine fresh bone meal and strengthen as high-quality calcium source in varieties of food items goods such as biscuit, instant noodles, bowel lavage, meat pulp, dried meat floss, addition is 10-20% (M/M is in dry), in calcic 15%.
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| CN00135416A CN1109512C (en) | 2000-12-20 | 2000-12-20 | Superfine fresh bone powder and its production process and use |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1297283C (en) * | 2005-07-06 | 2007-01-31 | 薛洪爱 | Superfine fresh bone with marrow high calcium powder capsule |
| CN102160621A (en) * | 2011-03-10 | 2011-08-24 | 湖南农业大学 | Method for processing animal bone paste dried noodles |
| CN103431423A (en) * | 2013-07-23 | 2013-12-11 | 广州市全能鲜骨粉生物食品有限公司 | Fresh bone-meat powder, and preparation method and edible method thereof |
| CN104161273A (en) * | 2014-08-18 | 2014-11-26 | 李春林 | Bone paste food for improving sclerotin of children, pregnant women and old people |
| CN106071922A (en) * | 2016-06-03 | 2016-11-09 | 泰安市海之润食品有限公司 | The preparation method of bone revolution product |
-
2000
- 2000-12-20 CN CN00135416A patent/CN1109512C/en not_active Expired - Lifetime
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1297283C (en) * | 2005-07-06 | 2007-01-31 | 薛洪爱 | Superfine fresh bone with marrow high calcium powder capsule |
| CN102160621A (en) * | 2011-03-10 | 2011-08-24 | 湖南农业大学 | Method for processing animal bone paste dried noodles |
| CN102160621B (en) * | 2011-03-10 | 2012-06-06 | 湖南农业大学 | Method for processing animal bone paste dried noodles |
| CN103431423A (en) * | 2013-07-23 | 2013-12-11 | 广州市全能鲜骨粉生物食品有限公司 | Fresh bone-meat powder, and preparation method and edible method thereof |
| CN104161273A (en) * | 2014-08-18 | 2014-11-26 | 李春林 | Bone paste food for improving sclerotin of children, pregnant women and old people |
| CN106071922A (en) * | 2016-06-03 | 2016-11-09 | 泰安市海之润食品有限公司 | The preparation method of bone revolution product |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1109512C (en) | 2003-05-28 |
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