CN1293831C - Effervescent solid beverage of amino acid chelated calcium and its prepn - Google Patents

Effervescent solid beverage of amino acid chelated calcium and its prepn Download PDF

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Publication number
CN1293831C
CN1293831C CNB031168132A CN03116813A CN1293831C CN 1293831 C CN1293831 C CN 1293831C CN B031168132 A CNB031168132 A CN B031168132A CN 03116813 A CN03116813 A CN 03116813A CN 1293831 C CN1293831 C CN 1293831C
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calcium
amino acid
aspartame
group
chelating
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CN1547964A (en
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华振珊
华振忠
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Abstract

The present invention discloses an effervescent solid beverage of compound amino acid chelated calcium, which belongs to the technical field of health-care foods. The solid beverage uses chelated amino acid calcium as main component and nutrient substances as auxiliary materials, such as lysine, zinc gluconate, taurine, etc. to have the functions of supplement cooperation and nutrition equalization. Simultaneously, the solid beverage is prepared into effervescent solid granules suitable for drinking and has stable quality. The present invention provides a preparation method of the effervescent solid beverage.

Description

Effervescence type compound amino acid chelate calcium solid drink liquid and preparation method
Technical field
The invention belongs to the health food technology field.Be specifically related to a kind of effervescence type compound amino acid chelate calcium solid drink liquid (how happy high solid drink liquid) and preparation method.
Background technology
Calcium is one of important element that constitutes human body, also is the maximum mineral composition of body burden.The calcium of human body 99% is stored in the bone, is known as " bone calcium storehouse ", and all the other about 1% are distributed in soft tissue and extracellular fluid.With the 60kg normal adult is example: bone calcium total amount is about 1100-1200g, the about 7.0g of soft tissue calcium content, and the about 7.0g extracellular fluid of tooth calcium content calcium content is 1.0g, wherein blood plasma calcium content: 300-500mg.
Calcium and human body healthy closely bound up, calcium deficiency will cause a series of diseases: the people was in positive calcium balance (bone forms, and the bone amount increases) by 20 years old from being born, and was in relative balance state in 20-35 year.If this moment calcium deficiency, bone is from being obstructed, serious formed rickets, bone amount bone hang down in lighter formation, causes of short and small staturely, enters and the bone retrogression pathological changes can take place earlier after growing up, and fractures easily.
Pregnant woman's calcium deficiency: can influence the growth of fetus, cause neonate's calcium deficiency, children's is low, and blood calcium is twitched.Self can cause and have a pain in the back, numb in every limb, jerk, the hypertension of pregnancy, postpartum tooth mobility, arthralgia etc. all the year round.
Entered negative calcium balance (bone loss) in 35 years old later on, after male sex 40-45 year, per 10 years bone loss 3-5%, bone loss quickens after women's menopause, reaches 9% in per 10 years.
Long-term calcium deficiency is the main cause of " calcium is lost ": because self regulating system effect of blood calcium balance in order to satisfy the organism physiology action need, has to employ the calcium in the bone, to remedy the deficiency of blood calcium.The overreaction of this self compensation to calcium deficiency in the course of time, makes blood calcium surpass previous level and is increased to the upper limit of blood calcium.At this moment skeletal calcium constantly " is migrated " to blood and soft tissue, " calcium is lost " phenomenon occurred, and the pathosis of blood and the many calcium of all kinds of soft tissues, old and feeble just typical case's performance.
According to the nutrition viewpoint, for well, so the calcium source can be used as food enrichment to the approach of replenishing the calcium, and adds food, plays invigoration effect in the beverage with tonic.The simultaneously drug of first choice and the adjuvant of all kinds of diseases that also cause because of calcium deficiency as treatment and prevention of calcium source.
Be main calcium source with calcium carbonate abroad at present, only there are calcium gluconae, calcium lactate in the calcium source of domestic pharmacopeia regulation, and calcium carbonate is to be applied to clinical as ending sour agent.Calcium activated is active in calcium market in recent years, but exist to some extent poorly soluble, trap is low, intestines and stomach are had weak points such as stimulation.
For this reason, developing efficient, safe, cheap novel calcium source has its important meaning, also is pressing for of society.
Calcium agent trap in the market is all not high, traces it to its cause nothing more than following several situations: (1) solubility itself is very little, inevitable in enteron aisle calcium ion concentration low; (2) calcium ion that has dissolved by combinations such as the phytic acid in some diet, oxalic acid, makes calcium ion concentration reduction in the enteron aisle in gastric juice; (3) user's renal function goes down and physiologic factor such as sex hormone minimizing.
Summary of the invention
Technical problem to be solved by this invention is to overcome above-mentioned weak point, designs a kind of new calcium preparation.
The invention provides a kind of effervescence type compound amino acid chelate calcium solid drink liquid, this solid drink liquid comprises that following two components are that A group and B group formation 100% are formed; The weight percent content of its each component is an A group+B group:
Chelating type amino acid calcium 5.00g-6.60g
Taurine 0.10g-0.50g
L-lysine hydrochloride 0.30g-0.80g
Zinc gluconate 0.04g-0.07g
Solids-enriched dried fruit juice 4.00g
Sodium acid carbonate 9.00g
Citric acid 14.00g
Icing Sugar 66.96-64.43g
Aspartame 0.60g
Make (full dose) 100g
The main nutrients composition of effervescence type compound amino acid chelate calcium solid of the present invention drink liquid is a standard design by the consumption allowed band of stipulating among the GB14880.
Another object of the present invention has provided the preparation method of above-mentioned a kind of effervescence type compound amino acid chelate calcium solid drink liquid, and this method comprises the following steps:
(1) pressing A component prescription mixes chelating calcium, taurine, zinc gluconate, dried fruit juice with citric acid behind the crushing screening, 50% ethanol that adds the 5-7% of solid grain weight amount is made softwood, 16 mesh sieves wave granulation, boiling calorifies 70 ℃ of oven dry, survey moisture content is 2.0-2.5, granulate, add lysine, Aspartame, finally mix bag distribution packaging;
(2) pressing B component prescription will fruit powder, chelating calcium, sodium acid carbonate mixes with Icing Sugar behind 80-100 order crushing screening, add 50% ethanol and make softwood, 16 mesh sieves wave granulation, the boiling heating is dried under 50 ℃ of conditions earlier, continues and dries under 70 ℃ of conditions, survey moisture content is 2.0-2.5, whole grain adds Aspartame, finally mixes bag distribution packaging;
When product of the present invention used, A group, B group particle were poured in the cup, add and drink after bubble is risen dissolving.
Effervescence type compound amino acid chelate calcium solid drink liquid of the present invention has following characteristics:
(1) science of formula for a product: this product at the crowd that replenishes the calcium mainly be the teenager, the teenager is in the vigorous period of growing, growing tall of child needs replenishing of various nutrients, simple replenishes the calcium in a large number, the dysequilibrium that can cause in-vivo element is unfavorable for teen-age growing on the contrary.Therefore, the prescription design characteristic of this product, the one, selecting " chelating type amino acid calcium " is main component, is aided with teenagers such as lysine, zinc gluconate, taurine simultaneously and encourages necessary nutrient, plays to work in coordination with and augments effect balanced in nutrition.The 2nd, according to the various nutrient limit standard scope design quantities of national food hygienic standard GB14880 regulation, guaranteed the edible for a long time security of teenager.The 3rd, select " chelating type amino acid calcium " and zinc gluconate compatibility can avoid producing the antagonistic effect of Ca-Zn element absorption.Traditional calcium agent mostly is ionized calcium greatly as calcium carbonate, calcium gluconae, calcium lactate etc., its calcium ion need be in the presence of vitamin D, be absorbed by the body by ion channel, because zinc ion also is to be absorbed by the body by ion channel, two kinds of ions are augmented simultaneously and can be influenced to absorb because of the competition passage produces antagonistic effect." chelating type amino acid calcium " has unique absorption mechanism, and it is to enter human body with molecular state, need not the participation of vitamin D, can directly be absorbed by amino acid sites, absorptivity can reach more than 90%, and therefore noiseless the and antagonistic effect to the absorption of other element of ion channel is better than other calcium agent.
(2) novelty of product forms: the calcium agent formulation that existing market is sold is generally tablet (chewable tablets), capsule, pulvis, electuary oral liquid.And this formulation of replenishing the calcium of effervescence type solid drink liquid still belongs to domestic initiation.The novelty of this product forms design is that it has catered to the custom that the teenager likes drinking soda, adds auxiliary material and flavourings such as sodium acid carbonate, citric acid, white granulated sugar, Aspartame, dried fruit juice in prescription, is processed into the effervescence solid particle.During Instant Drinks, fragrant odour not only, foam is abundant, and sweet mouthfeel is suitable, and children and teenager take like a shot.
(3) uniqueness of product technology: its preparation technology of traditional effervescent agent (tablet, particle) is mixed into one-component usually.This product is when technological design, many-sided factor such as the chemical stability of each composition and end product quality is considered from prescription, composition in the prescription is divided into two components of A, B, be processed into granulates and alkali particle respectively, and be packaged into A bag and B bag respectively, and mix adding during Instant Drinks again, take the effervescence granular of this unique technology preparation, not only foam can be abundanter during Instant Drinks, and help the stability of product quality.
The specific embodiment
Embodiment 1
Prescription:
Chelating type amino acid calcium 3.00g 2.00g
Taurine 0.10g
L-lysine hydrochloride 0.30g
Zinc gluconate 0.04g
Solids-enriched dried fruit juice 3.00g 1.00g
Sodium acid carbonate 0.00g 9.00g
Citric acid 14.00g
Icing Sugar 41.90g 25.06g
Aspartame 0.375g 0.225g
Make (full dose) 100g
(1) pressing A component prescription mixes chelating calcium, taurine, zinc gluconate, dried fruit juice with citric acid behind the crushing screening, 50% ethanol that adds the 5-7% of solid grain weight amount is made softwood, 16 mesh sieves wave granulation, boiling calorifies 70 ℃ of oven dry, survey moisture content is 2.0-2.5, granulate, add lysine, Aspartame, finally mix bag distribution packaging;
(2) pressing B component prescription will fruit powder, chelating calcium, sodium acid carbonate mixes with Icing Sugar behind 80-100 order crushing screening, add 50% ethanol and make softwood, 16 mesh sieves wave granulation, the boiling heating is dried under 50 ℃ of conditions earlier, continues and dries under 70 ℃ of conditions, survey moisture content is 2.0-2.5, whole grain adds Aspartame, finally mixes bag distribution packaging:
Embodiment 2
Chelating type amino acid calcium 3.84g 2.32g
Taurine 0.30g
L-lysine hydrochloride 0.55g
Zinc gluconate 0.055g
Solids-enriched dried fruit juice 3.00g 1.00g
Sodium acid carbonate 0.00g 9.00g
Citric acid 14.00g
Icing Sugar 41.00g 24.745g
Aspartame 0.375g 0.225g
Make (full dose) 100g
(1) pressing A component prescription mixes chelating calcium, taurine, zinc gluconate, dried fruit juice with citric acid behind the crushing screening, 50% ethanol that adds the 5-7% of solid grain weight amount is made softwood, 16 mesh sieves wave granulation, boiling calorifies 70 ℃ of oven dry, survey moisture content is 2.0-2.5, granulate, add lysine, Aspartame, the final mixing;
(2) pressing B component prescription will fruit powder, chelating calcium, sodium acid carbonate mixes with Icing Sugar behind 80-100 order crushing screening, add 50% ethanol and make softwood, 16 mesh sieves wave granulation, the boiling heating is dried under 50 ℃ of conditions earlier, continues and dries under 70 ℃ of conditions, survey moisture content is 2.0-2.5, whole grain adds Aspartame, the final mixing;
Embodiment 3
Chelating type amino acid calcium 4.00g 2.60g
Taurine 0.50g
L-lysine hydrochloride 0.80g
Zinc gluconate 0.07g
Solids-enriched dried fruit juice 3.00g
Sodium acid carbonate 0.00g 9.00g
Citric acid 14.00g
Icing Sugar 39.80g 24.68g
Aspartame 0.375g 0.225g
Make (full dose) 100g
(1) pressing A component prescription mixes chelating calcium, taurine, zinc gluconate, dried fruit juice with citric acid behind the crushing screening, 50% ethanol that adds the 5-7% of solid grain weight amount is made softwood, 16 mesh sieves wave granulation, boiling calorifies 70 ℃ of oven dry, survey moisture content is 2.0-2.5, granulate, add lysine, Aspartame, finally mix bag distribution packaging;
(2) pressing B component prescription will fruit powder, chelating calcium, sodium acid carbonate mixes with Icing Sugar behind 80-100 order crushing screening, add 50% ethanol and make softwood, 16 mesh sieves wave granulation, the boiling heating is dried under 50 ℃ of conditions earlier, continues and dries under 70 ℃ of conditions, survey moisture content is 2.0-2.5, whole grain adds Aspartame, finally mixes bag distribution packaging;
Embodiment 4 chelating calcium effervescence granular agent producing process
Prescription: A group B group
L-aspartase calcium 4.0 2.6
Taurine 0.5 0
L-lysine hydrochloride 0.75 0
Zinc gluconate 0.07 0
Solids-enriched dried fruit juice 3.0 1.0
Sodium acid carbonate 09
Citric acid 14.0 0
Icing Sugar 39.8 24.68
Aspartame 0.375 0.225
Annotate:
A. make wetting agent with 50% ethanol.Consumption: A group adds 8% of grain weight, and the B group adds 10% of grain weight.
B. chelating calcium, zinc, lysine hydrochloride need be converted into the consumption on the prescription according to the percentage composition of raw material.
Production technology:
One, raw material is handled: the 60-80 mesh sieve of pulverizing, sieve.
Two, former powder is divided into two groups:
A organizes granulates: calcium, zinc, taurine, lysine, Icing Sugar, solids-enriched dried fruit juice.
B group alkali particle: calcium, sodium acid carbonate, Icing Sugar, dried fruit juice.
Three, granulate respectively:
A group granulates is granulated:
Granulates supplementary material mixing adds 70% ethanol and makes softwood, waves granulation with 16 orders.Moisture content 2.0-2.5% is surveyed in oven dry about 70 ℃.Whole grain.Add lysine, Aspartame mixing.
B group alkali particle is granulated:
Alkali particle supplementary material mixing adds 70% ethanol system softwood, and 16 eye mesh screens wave granulation, and moisture content 2.0-2.5% is surveyed in 70 ℃ of oven dry.Whole grain.Add the Aspartame mixing.
Four, packing:
A organizes every bag 5 grams, and B organizes every bag 3 grams.
Annotate:
During use, A group, B group particle are poured in the cup, add and drink after bubble is risen dissolving.

Claims (1)

1. an effervescence type compound amino acid chelate calcium solid drink liquid is characterized in that this effervescence solid drink liquid comprises that following two components are that A group and B group formation 100% are formed; And prepare by following method:
(1) component
A group B group
Chelating type amino acid calcium 3.0g-4.0g 2.6g
Taurine 0.1g-0.5g 0
L-lysine hydrochloride 0.3g-0.75g 0
Zinc gluconate 0.04g-0.07g 0
Solids-enriched dried fruit juice 3.0g 1.0g
Sodium acid carbonate 0 9.0g
Citric acid 14.0g 0
Icing Sugar 39.8g 24.68g
Aspartame 0.375g 0.225g
Make (full dose) 100g
(2) preparation
I presses A component prescription chelating calcium, taurine, zinc gluconate, dried fruit juice, Icing Sugar is mixed with citric acid behind the crushing screening, 50% ethanol that adds the 5-7% of solid grain weight amount is made softwood, 16 mesh sieves wave granulation, boiling calorifies 70 ℃ of oven dry, survey moisture content is 2.0-2.5, granulate, add lysine, Aspartame, finally mix bag distribution packaging;
II presses B component prescription will fruit powder, chelating calcium, sodium acid carbonate mixes with Icing Sugar behind 80-100 order crushing screening, add 50% ethanol and make softwood, 16 mesh sieves wave granulation, the boiling heating is dried under 50 ℃ of conditions earlier, continues and dries under 70 ℃ of conditions, survey moisture content is 2.0-2.5, whole grain adds Aspartame, finally mixes bag distribution packaging.
CNB031168132A 2003-05-08 2003-05-08 Effervescent solid beverage of amino acid chelated calcium and its prepn Expired - Fee Related CN1293831C (en)

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CN1293831C true CN1293831C (en) 2007-01-10

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1292756C (en) * 2005-08-08 2007-01-03 李海涛 Effervescence tablet preparation for replenishing nutritious elements to human being and its preparation method
CN106552105A (en) * 2016-10-24 2017-04-05 广西圣保堂健康产业股份有限公司 A kind of effervescent tablet of enhancing immunity and preparation method thereof
CN107434753A (en) * 2017-07-26 2017-12-05 南京大学 Effervescent tablet of 5 amino-laevulic acids and its derivative and preparation method thereof
CN107495053A (en) * 2017-08-24 2017-12-22 太和县三九药业有限公司 A kind of preparation method of compound high calcium protein powder preparation

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85105693A (en) * 1984-12-19 1986-11-19 路易·拉维 Prepare non-hygroscopic prescription of pulverulent water-soluble of lasting effervescent beverage(s) and preparation method thereof
CN1266652A (en) * 1999-03-12 2000-09-20 江苏康禾食品总厂 Amino acid effervescing agent

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85105693A (en) * 1984-12-19 1986-11-19 路易·拉维 Prepare non-hygroscopic prescription of pulverulent water-soluble of lasting effervescent beverage(s) and preparation method thereof
CN1266652A (en) * 1999-03-12 2000-09-20 江苏康禾食品总厂 Amino acid effervescing agent

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