CN107495053A - A kind of preparation method of compound high calcium protein powder preparation - Google Patents
A kind of preparation method of compound high calcium protein powder preparation Download PDFInfo
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- CN107495053A CN107495053A CN201710735358.2A CN201710735358A CN107495053A CN 107495053 A CN107495053 A CN 107495053A CN 201710735358 A CN201710735358 A CN 201710735358A CN 107495053 A CN107495053 A CN 107495053A
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- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 239000011575 calcium Substances 0.000 title claims abstract description 40
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 40
- 239000000843 powder Substances 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 108090000623 proteins and genes Proteins 0.000 title claims abstract description 15
- 102000004169 proteins and genes Human genes 0.000 title claims abstract description 15
- 150000001875 compounds Chemical class 0.000 title claims abstract description 10
- 108090000765 processed proteins & peptides Proteins 0.000 claims abstract description 19
- 108010073771 Soybean Proteins Proteins 0.000 claims abstract description 13
- 229940001941 soy protein Drugs 0.000 claims abstract description 13
- 235000013305 food Nutrition 0.000 claims abstract description 11
- 235000016709 nutrition Nutrition 0.000 claims abstract description 6
- CBMPTFJVXNIWHP-UHFFFAOYSA-L disodium;hydrogen phosphate;2-hydroxypropane-1,2,3-tricarboxylic acid Chemical compound [Na+].[Na+].OP([O-])([O-])=O.OC(=O)CC(O)(C(O)=O)CC(O)=O CBMPTFJVXNIWHP-UHFFFAOYSA-L 0.000 claims abstract description 5
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 4
- 229960005069 calcium Drugs 0.000 claims description 34
- 238000012545 processing Methods 0.000 claims description 10
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000000047 product Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 235000010469 Glycine max Nutrition 0.000 claims description 8
- 244000068988 Glycine max Species 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 101710089165 Protein white Proteins 0.000 claims description 4
- 239000000428 dust Substances 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 230000035764 nutrition Effects 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 241000251468 Actinopterygii Species 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 229940092124 calcium citrate malate Drugs 0.000 claims description 3
- MKJXYGKVIBWPFZ-CEOVSRFSSA-L calcium;(2s)-2-hydroxypropanoate Chemical compound [Ca+2].C[C@H](O)C([O-])=O.C[C@H](O)C([O-])=O MKJXYGKVIBWPFZ-CEOVSRFSSA-L 0.000 claims description 3
- MPCMQXRREZMSPJ-UHFFFAOYSA-L calcium;2-hydroxybutanedioate;2-hydroxypropane-1,2,3-tricarboxylic acid;pentahydrate Chemical compound O.O.O.O.O.[Ca+2].[O-]C(=O)C(O)CC([O-])=O.OC(=O)CC(O)(C(O)=O)CC(O)=O MPCMQXRREZMSPJ-UHFFFAOYSA-L 0.000 claims description 3
- 210000003022 colostrum Anatomy 0.000 claims description 3
- 235000021277 colostrum Nutrition 0.000 claims description 3
- 235000011869 dried fruits Nutrition 0.000 claims description 3
- 235000013925 ferrous lactate Nutrition 0.000 claims description 3
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 3
- 235000021552 granulated sugar Nutrition 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 239000007981 phosphate-citrate buffer Substances 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000001694 spray drying Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000006228 supernatant Substances 0.000 claims description 3
- 235000011478 zinc gluconate Nutrition 0.000 claims description 3
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 2
- DKKCQDROTDCQOR-UHFFFAOYSA-L Ferrous lactate Chemical compound [Fe+2].CC(O)C([O-])=O.CC(O)C([O-])=O DKKCQDROTDCQOR-UHFFFAOYSA-L 0.000 claims description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 2
- 229930003268 Vitamin C Natural products 0.000 claims description 2
- WHMDKBIGKVEYHS-IYEMJOQQSA-L Zinc gluconate Chemical compound [Zn+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O WHMDKBIGKVEYHS-IYEMJOQQSA-L 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 239000004225 ferrous lactate Substances 0.000 claims description 2
- 229940037907 ferrous lactate Drugs 0.000 claims description 2
- 239000008103 glucose Substances 0.000 claims description 2
- 235000019871 vegetable fat Nutrition 0.000 claims description 2
- 235000019154 vitamin C Nutrition 0.000 claims description 2
- 239000011718 vitamin C Substances 0.000 claims description 2
- 239000011670 zinc gluconate Substances 0.000 claims description 2
- 229960000306 zinc gluconate Drugs 0.000 claims description 2
- 239000011710 vitamin D Substances 0.000 claims 1
- 208000001132 Osteoporosis Diseases 0.000 abstract description 3
- 238000000605 extraction Methods 0.000 abstract description 3
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 230000037180 bone health Effects 0.000 abstract description 2
- 239000000284 extract Substances 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract description 2
- 238000002386 leaching Methods 0.000 abstract description 2
- 238000004088 simulation Methods 0.000 abstract description 2
- 210000002784 stomach Anatomy 0.000 abstract description 2
- 229940043430 calcium compound Drugs 0.000 abstract 1
- 150000001674 calcium compounds Chemical class 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 description 9
- 229940088594 vitamin Drugs 0.000 description 3
- 235000013343 vitamin Nutrition 0.000 description 3
- 229930003231 vitamin Natural products 0.000 description 3
- 239000011782 vitamin Substances 0.000 description 3
- 150000003722 vitamin derivatives Chemical class 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- 235000001727 glucose Nutrition 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- CAXNYFPECZCGFK-UHFFFAOYSA-N 2-phenyl-2-pyridin-2-ylacetonitrile Chemical compound C=1C=CC=NC=1C(C#N)C1=CC=CC=C1 CAXNYFPECZCGFK-UHFFFAOYSA-N 0.000 description 1
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 229940036811 bone meal Drugs 0.000 description 1
- 239000002374 bone meal Substances 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- FYHXNYLLNIKZMR-UHFFFAOYSA-N calcium;carbonic acid Chemical compound [Ca].OC(O)=O FYHXNYLLNIKZMR-UHFFFAOYSA-N 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 150000002304 glucoses Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000008821 health effect Effects 0.000 description 1
- 235000004280 healthy diet Nutrition 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 230000002485 urinary effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
- A23L33/165—Complexes or chelates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
- A23L33/185—Vegetable proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Inorganic Chemistry (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of preparation method of compound high calcium protein powder preparation, in the present invention leaching agent is used as by the use of disodium hydrogen phosphate citric acid solution, simulation human stomach pH extracts to fish-bone nutritional ingredient, handled off field in high-voltage pulse electric simultaneously, fully solubility calcium in extraction fish-bone, Soyprotein peptide chelating calcium is prepared with Soyprotein peptide chelating afterwards, with slightly solubility calcium in food enrichment, solubility calcium compounds, improve absorption of the human body to solubility calcium in fish-bone, effectively facilitate bone health, reduce the probability for suffering from osteoporosis, improve product quality and eating mouth feel.
Description
Technical field
The invention belongs to field of food, and in particular to a kind of preparation method of compound high calcium protein powder preparation.
Background technology
Protein is one of indispensable seven big important nutrient of human body.Human body passes through daily animal food and plant
Physical property food absorbs animal protein and vegetable protein.As the health perception of people increasingly strengthens and income level
Raising, normal meals approach can not meet the needs of to albumen quality, and the consumption for also not meeting people's healthy diet will
Ask.Accordingly, it is desirable to more healthy protein uptake mode.
Calcium is the most abundant mineral matter element of mankind's in-vivo content, and its physiological metabolism plays particularly important to health
Effect.Calcium intake shortage can cause various diseases, particularly osteoporosis.Animal Bone such as pig, chicken etc. are that current calcium product comes
The important channel in source.
In recent years, high nutrient is prepared from disposal from fishery product processing to be increasingly taken seriously, therefrom obtain high-quality calcium
Also new research direction is turned into.Fish-bone calcium content is very high, and belongs to calcium phosphate, close to skeleton, has absorptivity height, people
The advantages of body side reaction is small, it is a kind of high-quality natural calcium source.
The content of the invention
The present invention provides a kind of preparation method of compound high calcium protein powder preparation, improves solubility calcium in albumen powder and contains
Amount, improve product quality and eating mouth feel.
The present invention is achieved by the following technical solutions：
A kind of preparation method of compound high calcium protein powder preparation, including processing step in detail below：
（1）Fish-bone pre-processes：
Fish-bone is cleared up with clear water, removes the remnants flesh of fish, is dried, and medicinal herb grinder crushes, and crosses 100 mesh sieves, standby；Preparing pH is
2.0-4.0 disodium hydrogen phosphate-citrate buffer solution；
It is 1 according to fixed solid-liquid ratio:12, above-mentioned fishbone dust is added in cushioning liquid, after high-pressure pulse electric is handled, mistake
Filter, retain filtrate, determine solubility calcium content；
（2）The chelated calcium preparation of Soyprotein peptide：
According to peptide/calcium mol ratio 2:1 ratio, appropriate Soyprotein peptide is weighed, add in 55-65 DEG C of warm water and dissolve, adjust peptide
Concentration is 0.2mol/L, adds step afterwards（1）After filtrate, 0.1mol/L potassium hydroxide regulation pH to 6.7-7.3, control are added
For temperature at 27-32 DEG C, chelatropic reaction 25-40 minutes, reaction adds the absolute ethyl alcohol of 9 times of reaction volumes after terminating, and mixing is equal
It is even, 8-15 minutes are centrifuged in 4500-6000r/min, abandoning supernatant, take precipitation to dry, obtain Soyprotein peptide chelating calcium；
（3）After adding water stirring it is fully dissolved 60-85 parts soybean separation protein white powder, 43-62 part soyabean protein powders, egg is made into
Bai Hanliang 2-5% solution, through high pressure homogenizer 80-120MPa processing after, spray drying, obtain egg mix white powder；
（4）By 2-15 parts colostrum, 4-11 parts white granulated sugar, 3-8 parts edible glucose, 12-24 parts phosphatide, 3-9 part food nutritions
Hardening agent, 3-13 parts vegetable fat powder, 4-16 part dried fruit juices, after co-grinding, cross 100-150 mesh sieves；
（5）Mixing, packaging：
By step（2）Product and above-mentioned egg mix white powder, step（4）Material is added in mixer and mixed, rotating speed 20-30r/min,
Minute time 30-40, add in packing machine hopper, packed afterwards.
Wherein, the step（1）In high-pressure pulse electric processing, strobe pulse number is 5-10, flow velocity 12-15mL/
Min, pulse strength 10-25kV/cm.
Wherein, the step（4）Middle food enrichment is composed of the following raw materials by weight：0.05-0.8 part carbonic acid
Calcium, 0.2-2 parts L-calcium lactate, 0.5-2 parts calcium citrate malate, 1-3 parts ferrous lactate, 2-4 parts zinc gluconate, 1-3 parts
Vitamin C, 1-3 part vitamin Ds3。
The present invention has the beneficial effect that：
By the use of disodium hydrogen phosphate-citric acid solution as leaching agent in the present invention, human stomach pH is to fish-bone nutrition for simulation
Composition is extracted, while is handled off field in high-voltage pulse electric, improves extraction efficiency, fully extracts solubility calcium in fish-bone, and
On its nutritional ingredient without influence；Soyprotein peptide chelating calcium is prepared with Soyprotein peptide chelating afterwards, on the one hand changes traditional work
The method that fishbone dust is directly used in skill, absorption of the human body to solubility calcium in fish-bone is improved, while avoided because adding bone meal
Particle causes the problem of taste bad, improves product quality and eating mouth feel；Another aspect and indissoluble in food enrichment
Property calcium, solubility calcium compounding, improve product calcium content, fully supplement needed by human body nutrition, trace element, while raw soybeans point
Urinary calcium can be prevented to lose from albumen, both, which act synergistically down, can effectively facilitate bone health, reduce the probability for suffering from osteoporosis；
In addition obtain albumen powder emulsifying activity through high-pressure homogeneous processing the egg mix white powder of soybean separation protein white powder and soyabean protein powder
To raising, the emulsifying property of product is improved to a certain extent, improves albumen powder solid beverage mouthfeel.
Embodiment
A kind of preparation method of compound high calcium protein powder preparation, including processing step in detail below：
（1）Fish-bone pre-processes：
Fish-bone is cleared up with clear water, removes the remnants flesh of fish, is dried, and medicinal herb grinder crushes, and crosses 100 mesh sieves, standby；Preparing pH is
2.5 disodium hydrogen phosphate-citrate buffer solution；
It is 1 according to fixed solid-liquid ratio:12, above-mentioned fishbone dust is added in cushioning liquid, after high-pressure pulse electric is handled, selection
Umber of pulse is 6, flow velocity 14mL/min, pulse strength 20kV/cm, is filtered after the completion of extraction, retains filtrate, and measure is soluble
Calcium content；
（2）The chelated calcium preparation of Soyprotein peptide：
According to peptide/calcium mol ratio 2:1 ratio, appropriate Soyprotein peptide is weighed, add in 60 DEG C of warm water and dissolve, regulation peptide is dense
Spend for 0.2mol/L, add step afterwards（1）After filtrate, 0.1mol/L potassium hydroxide regulation pH to 7.0 is added, control temperature exists
30 DEG C, chelatropic reaction 30 minutes, reaction adds the absolute ethyl alcohol of 9 times of reaction volumes after terminating, be well mixed, in 5500r/
Min is centrifuged 10 minutes, abandoning supernatant, takes precipitation to dry, and obtains Soyprotein peptide chelating calcium；
（3）After adding water stirring it is fully dissolved 80 parts of soybean separation protein white powders, 45 parts of soyabean protein powders, protein content is made into
In 4% solution, after high pressure homogenizer 100MPa processing, spray drying, egg mix white powder is obtained；
（4）By 8 parts of colostrums, 6 portions of white granulated sugars, 5 parts of edible glucoses, 16 parts of phosphatide, 6 parts of food enrichments, 10 parts of plants
Fat is last, 8 parts of dried fruit juices, after co-grinding, crosses 100 mesh sieves；
（5）Mixing, packaging：
By step（2）Product and above-mentioned egg mix white powder, step（4）Material is added in mixer and mixed, rotating speed 30r/min, when
Between 30 minutes, afterwards add packing machine hopper in, packed.
Wherein, the step（4）Middle food enrichment is composed of the following raw materials by weight：0.2 part of calcium carbonate, 1 part
L-calcium lactate, 1 part of calcium citrate malate, 2 parts of ferrous lactates, 3 parts of zinc gluconates, 2 parts of vitamin Cs, 3 parts of vitamin Ds3。
Claims (3)
1. a kind of preparation method of compound high calcium protein powder preparation, it is characterised in that including processing step in detail below：
（1）Fish-bone pre-processes：
Fish-bone is cleared up with clear water, removes the remnants flesh of fish, is dried, and medicinal herb grinder crushes, and crosses 100 mesh sieves, standby；Preparing pH is
2.0-4.0 disodium hydrogen phosphate-citrate buffer solution；
It is 1 according to fixed solid-liquid ratio:12, above-mentioned fishbone dust is added in cushioning liquid, after high-pressure pulse electric is handled, mistake
Filter, retain filtrate, determine solubility calcium content；
（2）The chelated calcium preparation of Soyprotein peptide：
According to peptide/calcium mol ratio 2:1 ratio, appropriate Soyprotein peptide is weighed, add in 55-65 DEG C of warm water and dissolve, adjust peptide
Concentration is 0.2mol/L, adds step afterwards（1）After filtrate, 0.1mol/L potassium hydroxide regulation pH to 6.7-7.3, control are added
For temperature at 27-32 DEG C, chelatropic reaction 25-40 minutes, reaction adds the absolute ethyl alcohol of 9 times of reaction volumes after terminating, and mixing is equal
It is even, 8-15 minutes are centrifuged in 4500-6000r/min, abandoning supernatant, take precipitation to dry, obtain Soyprotein peptide chelating calcium；
（3）After adding water stirring it is fully dissolved 60-85 parts soybean separation protein white powder, 43-62 part soyabean protein powders, egg is made into
Bai Hanliang 2-5% solution, through high pressure homogenizer 80-120MPa processing after, spray drying, obtain egg mix white powder；
（4）By 2-15 parts colostrum, 4-11 parts white granulated sugar, 3-8 parts edible glucose, 12-24 parts phosphatide, 3-9 part food nutritions
Hardening agent, 3-13 parts vegetable fat powder, 4-16 part dried fruit juices, after co-grinding, cross 100-150 mesh sieves；
（5）Mixing, packaging：
By step（2）Product and above-mentioned egg mix white powder, step（4）Material is added in mixer and mixed, rotating speed 20-30r/min,
Minute time 30-40, add in packing machine hopper, packed afterwards.
2. the preparation method of a kind of compound high calcium protein powder preparation according to claims 1, it is characterised in that described
Step（1）In high-pressure pulse electric processing, strobe pulse number is 5-10, flow velocity 12-15mL/min, pulse strength 10-
25kV/cm。
3. the preparation method of a kind of compound high calcium protein powder preparation according to claims 1, it is characterised in that described
Step（4）Middle food enrichment is composed of the following raw materials by weight：0.05-0.8 parts calcium carbonate, 0.2-2 parts L-calcium lactate,
0.5-2 parts calcium citrate malate, 1-3 parts ferrous lactate, 2-4 parts zinc gluconate, 1-3 parts vitamin C, 1-3 part vitamins
D3。
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710735358.2A CN107495053A (en) | 2017-08-24 | 2017-08-24 | A kind of preparation method of compound high calcium protein powder preparation |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710735358.2A CN107495053A (en) | 2017-08-24 | 2017-08-24 | A kind of preparation method of compound high calcium protein powder preparation |
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| Publication Number | Publication Date |
|---|---|
| CN107495053A true CN107495053A (en) | 2017-12-22 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109349646A (en) * | 2018-11-09 | 2019-02-19 | 贵州梵净山生态农业股份有限公司 | The extracting method of calcium constituent in a kind of ox bone |
| CN110140877A (en) * | 2019-06-25 | 2019-08-20 | 江西师范大学 | A kind of high calcium flesh of fish rice cake and preparation method thereof |
| CN114468287A (en) * | 2021-12-31 | 2022-05-13 | 天津市元生泰科技有限公司 | Formula and preparation method of chelated calcium suitable for astronauts |
| CN115997925A (en) * | 2022-12-07 | 2023-04-25 | 安徽全康药业有限公司 | Protein powder capable of supplementing calcium and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109349646A (en) * | 2018-11-09 | 2019-02-19 | 贵州梵净山生态农业股份有限公司 | The extracting method of calcium constituent in a kind of ox bone |
| CN110140877A (en) * | 2019-06-25 | 2019-08-20 | 江西师范大学 | A kind of high calcium flesh of fish rice cake and preparation method thereof |
| CN114468287A (en) * | 2021-12-31 | 2022-05-13 | 天津市元生泰科技有限公司 | Formula and preparation method of chelated calcium suitable for astronauts |
| CN115997925A (en) * | 2022-12-07 | 2023-04-25 | 安徽全康药业有限公司 | Protein powder capable of supplementing calcium and preparation method thereof |
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Application publication date: 20171222 |