CN1243135C - 掺钛蓝宝石和蓝宝石复合激光晶体的生长方法 - Google Patents
掺钛蓝宝石和蓝宝石复合激光晶体的生长方法 Download PDFInfo
- Publication number
- CN1243135C CN1243135C CN 03114821 CN03114821A CN1243135C CN 1243135 C CN1243135 C CN 1243135C CN 03114821 CN03114821 CN 03114821 CN 03114821 A CN03114821 A CN 03114821A CN 1243135 C CN1243135 C CN 1243135C
- Authority
- CN
- China
- Prior art keywords
- sapphire
- crystal
- growth
- autoclave
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000013078 crystal Substances 0.000 title claims abstract description 55
- 229910052594 sapphire Inorganic materials 0.000 title claims abstract description 31
- 239000010980 sapphire Substances 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 23
- 239000002131 composite material Substances 0.000 title claims abstract description 11
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 22
- 239000010931 gold Substances 0.000 claims description 22
- 229910052737 gold Inorganic materials 0.000 claims description 22
- 230000006798 recombination Effects 0.000 claims description 10
- 238000005215 recombination Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 7
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 5
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000007664 blowing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 238000005498 polishing Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 3
- 238000005520 cutting process Methods 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 238000007789 sealing Methods 0.000 claims description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 2
- 229910052719 titanium Inorganic materials 0.000 abstract 2
- 239000010936 titanium Substances 0.000 abstract 2
- 239000000758 substrate Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 12
- 230000003287 optical effect Effects 0.000 description 9
- 239000000463 material Substances 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000010959 steel Substances 0.000 description 4
- 239000004568 cement Substances 0.000 description 3
- 239000002178 crystalline material Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000009514 concussion Effects 0.000 description 2
- 230000010748 Photoabsorption Effects 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 239000003637 basic solution Substances 0.000 description 1
- 239000004567 concrete Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Images
Landscapes
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
Description
成分 | 方案1 | 方案2 | 方案3 |
蓝宝石(Wt%) | 80 | 85 | 90 |
氢氧化铝(Wt%) | 20 | 15 | 10 |
成分 | 浓度(mol/L) |
K2CO3 | 1 |
KOH | 1.5 |
NaCO3 | 0.5 |
H2O | 添加量 |
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 03114821 CN1243135C (zh) | 2003-01-10 | 2003-01-10 | 掺钛蓝宝石和蓝宝石复合激光晶体的生长方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 03114821 CN1243135C (zh) | 2003-01-10 | 2003-01-10 | 掺钛蓝宝石和蓝宝石复合激光晶体的生长方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1425807A CN1425807A (zh) | 2003-06-25 |
CN1243135C true CN1243135C (zh) | 2006-02-22 |
Family
ID=4790493
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 03114821 Expired - Fee Related CN1243135C (zh) | 2003-01-10 | 2003-01-10 | 掺钛蓝宝石和蓝宝石复合激光晶体的生长方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1243135C (zh) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100358194C (zh) * | 2006-03-07 | 2007-12-26 | 上海大学 | 复合Ti:Al2O3激光棒的制备方法 |
CN103726105A (zh) * | 2013-10-11 | 2014-04-16 | 中国科学院上海光学精密机械研究所 | 钛宝石晶体生长装置及其生长方法 |
CN104651936A (zh) * | 2015-02-06 | 2015-05-27 | 蚌埠诺德科技有限公司 | 一种掺质蓝宝石晶体的原料配方 |
CN109280963B (zh) * | 2018-08-24 | 2020-06-19 | 中国科学院合肥物质科学研究院 | 一种复合板状激光晶体及其导模法制备方法 |
CN112338344A (zh) * | 2020-10-29 | 2021-02-09 | 河海大学常州校区 | 一种蓝宝石的高温自膨胀压力扩散焊接方法 |
-
2003
- 2003-01-10 CN CN 03114821 patent/CN1243135C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CN1425807A (zh) | 2003-06-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN1243135C (zh) | 掺钛蓝宝石和蓝宝石复合激光晶体的生长方法 | |
CN110295392A (zh) | 一种可调谐激光晶体掺铬钪酸钆及其制备方法 | |
CN1477239A (zh) | 复合激光晶体的生长方法 | |
CN1206392C (zh) | 掺钕钒酸钇和钒酸钇复合激光晶体的生长方法 | |
CN112430847A (zh) | 铥铒镝三掺杂氟化铅中红外激光晶体、制备方法及应用 | |
CN1186483C (zh) | 掺钕钇铝石榴石和钇铝石榴石复合激光晶体的制备方法 | |
CN111519242B (zh) | 基于横向平移结晶法制备大尺寸Ce,Nd:YAG晶体的方法 | |
CN1041004C (zh) | 掺镱的钒酸钇激光晶体及其制备方法 | |
CN102586870A (zh) | 掺钬氟化钆钇钡晶体及其生长方法 | |
CN101880908A (zh) | 一种原生多段式钒酸钇激光晶体的制备方法 | |
CN1236110C (zh) | 祖母绿和绿柱石复合激光晶体的生长方法 | |
Mat | Laser crystals with low phonon frequencies | |
CN109023524B (zh) | 一种铒钬镨三掺杂氟化铅中红外激光晶体及其制备方法 | |
CN101864595B (zh) | 掺铒氟化钆锂晶体及其生长方法 | |
CN1249273C (zh) | 掺钛蓝宝石激光晶体的生长方法 | |
US9493887B1 (en) | Heterogeneous single vanadate based crystals for Q-switched lasers and microlasers and method for forming same | |
CN103103610A (zh) | 一种掺钕氟化钇钆锂晶体及其生长方法 | |
CN100494517C (zh) | Re3+,Cr5+:LnVO4自调制激光晶体及制备方法与应用 | |
CN101481213B (zh) | 2μm高磷含量氟磷酸盐激光玻璃及其制备方法 | |
CN1865533A (zh) | 提拉法生长高温挥发性晶体的保温罩 | |
CN1075568C (zh) | 掺钕离子的钒酸钆钇激光晶体 | |
CN1030798A (zh) | 掺钕和铈的钇铝石榴石激光晶体的生长技术 | |
CN101717998A (zh) | 掺钕的硅酸钇镥激光晶体及其制备方法 | |
RU2324018C2 (ru) | Серийный способ выращивания кристаллов галлий-скандий-гадолиниевых гранатов для пассивных лазерных затворов | |
CN1292105C (zh) | 共掺钠和镱氟化钙激光晶体及其生长方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Jiangsu Jixing New Materials Co.,Ltd. Assignor: Shanghai Optical Precision Machinery Inst., Chinese Academy of Sciences Contract record no.: 2012320000409 Denomination of invention: Growing method titanium-doped sapphire and sapphire composite laser crystal Granted publication date: 20060222 License type: Exclusive License Open date: 20030625 Record date: 20120406 |
|
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060222 Termination date: 20170110 |
|
CF01 | Termination of patent right due to non-payment of annual fee |