CN1205167C - 2-羟基萘-3-羧酸的结晶及其制造方法 - Google Patents
2-羟基萘-3-羧酸的结晶及其制造方法 Download PDFInfo
- Publication number
- CN1205167C CN1205167C CNB008013438A CN00801343A CN1205167C CN 1205167 C CN1205167 C CN 1205167C CN B008013438 A CNB008013438 A CN B008013438A CN 00801343 A CN00801343 A CN 00801343A CN 1205167 C CN1205167 C CN 1205167C
- Authority
- CN
- China
- Prior art keywords
- carboxylic acid
- hydroxy naphthalene
- acid
- crystallization
- naphthalene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C65/00—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C65/01—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing hydroxy or O-metal groups
- C07C65/105—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing hydroxy or O-metal groups polycyclic
- C07C65/11—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing hydroxy or O-metal groups polycyclic with carboxyl groups on a condensed ring system containing two rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
酸析温度(℃) | 平均粒径(μm) | 297μm以上的比例(%) | 74μm以下的比例(%) | |
实施例1 | 160 | 367.4 | 88.16 | 0.69 |
实施例2 | 140 | 263.5 | 75.59 | 0.79 |
实施例3 | 120 | 156.7 | 14.09 | 2.52 |
比较例1 | 110 | 92.7 | 1.07 | 17.18 |
比较例2 | 100 | 71.5 | 1.39 | 45.78 |
实施例4 | - | 214.6 | 50.74 | 3.77 |
实施例5 | - | 265.5 | 75.07 | 0.45 |
实施例6 | - | 195.5 | 33.80 | 5.50 |
实施例7 | - | 172.1 | 28.88 | 6.83 |
实施例8 | - | 212.4 | 48.94 | 10.04 |
实施例9 | - | 236.0 | 56.09 | 5.44 |
粒度分布(%) | |||||||
20Mon(710μ) | 48Mon(297μ) | 83Mon(170μ) | 140Mon(106μ) | 200Mon(74μ) | 330Mon(45μ) | 330Mon通过量 | |
实施例1 | 21.43 | 66.73 | 8.12 | 2.15 | 0.88 | 0.59 | 0.10 |
实施例2 | 0.20 | 75.39 | 20.31 | 2.83 | 0.49 | 0.59 | 0.20 |
实施例3 | 0.00 | 14.09 | 43.35 | 32.85 | 7.19 | 1.94 | 0.58 |
比较例1 | 0.10 | 0.97 | 7.38 | 44.95 | 29.42 | 14.27 | 2.91 |
比较例2 | 0.30 | 1.09 | 3.47 | 17.74 | 31.62 | 33.39 | 12.39 |
实施例4 | 0.74 | 50.00 | 21.91 | 14.71 | 8.87 | 2.71 | 1.0 |
实施例5 | 0.51 | 74.56 | 22.47 | 1.58 | 0.43 | 0.43 | 0.2 |
实施例6 | 0.20 | 33.60 | 45.00 | 13.20 | 2.50 | 3.10 | 2.4 |
实施例7 | 0.20 | 28.68 | 26.71 | 30.17 | 7.41 | 4.45 | 2.38 |
实施例8 | 0.72 | 48.22 | 28.44 | 8.82 | 3.76 | 5.50 | 4.54 |
实施例9 | 2.90 | 53.19 | 24.89 | 9.01 | 4.57 | 3.96 | 1.48 |
ML值 | 色度 | ||||
L(光亮度) | a(红度) | b(黄度) | HW(白度) | ||
实施例1 | - | 40.41 | 4.12 | 16.32 | 6.91 |
实施例2 | 1.33 | 56.23 | 0.21 | 26.79 | 10.09 |
实施例3 | 1.23 | 66.14 | 3.87 | 31.66 | 13.83 |
比较例1 | 1.17 | 76.13 | 0.43 | 34.21 | 20.75 |
比较例2 | 1.03 | 80.82 | -0.51 | 36.68 | 22.97 |
实施例4 | 1.80 | 38.15 | 6.61 | 18.26 | 4.61 |
实施例5 | 1.17 | 56.45 | 3.77 | 25.51 | 11.29 |
实施例6 | 1.37 | 54.49 | 7.38 | 28.25 | 7.70 |
实施例7 | 1.40 | 62.84 | 5.43 | 28.81 | 13.62 |
实施例8 | 0.23 | 84.42 | -4.70 | 36.21 | 27.59 |
实施例9 | 0.40 | 76.85 | -2.71 | 30.43 | 25.65 |
表观比重(g/cc) | 松弛/密实(%) | 压缩度(%) | 刮铲角(度) | 溶解时间 | ||
松弛 | 密实 | |||||
实施例1 | 0.547 | 0.601 | 91.01 | 9.0 | 50.4 | 17分35秒 |
实施例2 | 0.514 | 0.578 | 88.93 | 11.1 | 48.4 | 8分55秒 |
实施例3 | 0.341 | 0.474 | 71.94 | 28.1 | 61.6 | 12分11秒 |
比较例1 | 0.312 | 0.422 | 73.93 | 26.1 | 63.3 | 25分 |
比较例2 | 0.262 | 0.429 | 61.07 | 38.9 | 74.2 | 29分 |
实施例4 | - | - | - | - | - | 15分39秒 |
实施例5 | 0.355 | 0.459 | 77.34 | 22.7 | 66.5 | 9分44秒 |
实施例6 | 0.493 | 0.554 | 88.99 | 11.0 | 47.4 | 16分9秒 |
实施例7 | 0.622 | 0.687 | 90.54 | 9.5 | 47.1 | 7分28秒 |
实施例8 | 0.591 | 0.699 | 54.55 | 15.4 | 62.3 | 15分39秒 |
实施例9 | 0.478 | 0.618 | 77.35 | 22.6 | 50.0 | 7分49秒 |
距离(cm) | 高度(cm) | |
实施例1 | 5 | 10 |
实施例2 | 10 | 7 |
实施例3 | 30 | 15 |
比较例1 | 50 | 30 |
比较例2 | >100 | 25 |
实施例4 | 20 | 13 |
实施例5 | 15 | 10 |
实施例6 | 30 | 15 |
实施例7 | 35 | 15 |
实施例8 | 20 | 17 |
实施例9 | 15 | 12 |
Claims (5)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP127158/1999 | 1999-05-07 | ||
JP12715899 | 1999-05-07 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1316985A CN1316985A (zh) | 2001-10-10 |
CN1205167C true CN1205167C (zh) | 2005-06-08 |
Family
ID=14953082
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB008013438A Expired - Fee Related CN1205167C (zh) | 1999-05-07 | 2000-05-01 | 2-羟基萘-3-羧酸的结晶及其制造方法 |
Country Status (11)
Country | Link |
---|---|
US (1) | US6403827B1 (zh) |
EP (1) | EP1095929B1 (zh) |
JP (1) | JP3664653B2 (zh) |
KR (1) | KR20010053395A (zh) |
CN (1) | CN1205167C (zh) |
AT (1) | ATE275537T1 (zh) |
CA (1) | CA2336671A1 (zh) |
DE (1) | DE60013529T2 (zh) |
DK (1) | DK1095929T3 (zh) |
ES (1) | ES2230095T3 (zh) |
WO (1) | WO2000068177A1 (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100531592B1 (ko) | 1999-10-26 | 2005-11-28 | 가부시키가이샤 우에노 세이야꾸 오요 겡뀨조 | 2-히드록시나프탈렌-3-카르복실산의 조립물 및 그의제조방법 |
JP4878695B2 (ja) * | 2001-04-20 | 2012-02-15 | 上野製薬株式会社 | ナフトール誘導体の造粒物およびその製法 |
US6755367B2 (en) * | 2002-04-02 | 2004-06-29 | International Business Machines Corporation | Sensing position of pin on tape inside cartridge shell |
JP5189001B2 (ja) * | 2009-01-26 | 2013-04-24 | 上野製薬株式会社 | 2,6−ナフタレンジカルボン酸の製造方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4239913A (en) * | 1977-10-25 | 1980-12-16 | Kabushiki Kaisha Veno Seiyaku Oyo Kenkyujo | Process for preparing 2-hydroxynaphthalenecarboxylic acids |
JPS5535042A (en) * | 1978-09-06 | 1980-03-11 | Ueno Seiyaku Oyo Kenkyusho:Kk | Preparation of 2-hydroxynaphthalene-3-carboxylic acid |
-
2000
- 2000-05-01 KR KR1020017000128A patent/KR20010053395A/ko not_active Application Discontinuation
- 2000-05-01 JP JP2000617158A patent/JP3664653B2/ja not_active Expired - Lifetime
- 2000-05-01 DK DK00922924T patent/DK1095929T3/da active
- 2000-05-01 ES ES00922924T patent/ES2230095T3/es not_active Expired - Lifetime
- 2000-05-01 EP EP00922924A patent/EP1095929B1/en not_active Expired - Lifetime
- 2000-05-01 CA CA002336671A patent/CA2336671A1/en not_active Abandoned
- 2000-05-01 WO PCT/JP2000/002862 patent/WO2000068177A1/ja not_active Application Discontinuation
- 2000-05-01 AT AT00922924T patent/ATE275537T1/de not_active IP Right Cessation
- 2000-05-01 US US09/720,994 patent/US6403827B1/en not_active Expired - Lifetime
- 2000-05-01 DE DE60013529T patent/DE60013529T2/de not_active Expired - Lifetime
- 2000-05-01 CN CNB008013438A patent/CN1205167C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1095929B1 (en) | 2004-09-08 |
KR20010053395A (ko) | 2001-06-25 |
CN1316985A (zh) | 2001-10-10 |
US6403827B1 (en) | 2002-06-11 |
DE60013529D1 (de) | 2004-10-14 |
CA2336671A1 (en) | 2000-11-16 |
ES2230095T3 (es) | 2005-05-01 |
DK1095929T3 (da) | 2005-01-17 |
DE60013529T2 (de) | 2005-09-29 |
WO2000068177A1 (fr) | 2000-11-16 |
EP1095929A4 (en) | 2001-08-22 |
ATE275537T1 (de) | 2004-09-15 |
JP3664653B2 (ja) | 2005-06-29 |
EP1095929A1 (en) | 2001-05-02 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: UENO FINE CHEMICALS INDUSTRY Free format text: FORMER OWNER: CO., LTD. UENO SCIENCE Effective date: 20080926 |
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C41 | Transfer of patent application or patent right or utility model | ||
C56 | Change in the name or address of the patentee |
Owner name: CO., LTD. UENO SCIENCE Free format text: FORMER NAME OR ADDRESS: K.K. URENO SEIYAKU OYO KENKYUJO |
|
CP03 | Change of name, title or address |
Address after: Osaka City, Osaka of Japan Patentee after: Ueno Technology Co.,Ltd. Address before: Osaka City, Osaka of Japan Patentee before: Kabushiki Kaisha UENO SEIYAKU OYO KENKYUJO |
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TR01 | Transfer of patent right |
Effective date of registration: 20080926 Address after: Osaka City, Osaka of Japan Patentee after: UENO FINE CHEMICALS INDUSTRY, LTD. Address before: Osaka City, Osaka of Japan Patentee before: Ueno Technology Co.,Ltd. |
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C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20050608 Termination date: 20140501 |