CN1204837C - Extracting and preparing technology for aromatic matter in waste tobacco - Google Patents
Extracting and preparing technology for aromatic matter in waste tobacco Download PDFInfo
- Publication number
- CN1204837C CN1204837C CN 01128925 CN01128925A CN1204837C CN 1204837 C CN1204837 C CN 1204837C CN 01128925 CN01128925 CN 01128925 CN 01128925 A CN01128925 A CN 01128925A CN 1204837 C CN1204837 C CN 1204837C
- Authority
- CN
- China
- Prior art keywords
- tobacco
- aromatic substance
- extraction
- offal
- small amount
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 68
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 68
- 125000003118 aryl group Chemical group 0.000 title claims abstract description 48
- 239000002699 waste material Substances 0.000 title claims abstract description 31
- 239000000126 substance Substances 0.000 claims abstract description 51
- 238000009835 boiling Methods 0.000 claims abstract description 28
- 239000007788 liquid Substances 0.000 claims abstract description 26
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000003513 alkali Substances 0.000 claims abstract description 10
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 150000002576 ketones Chemical class 0.000 claims abstract description 9
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 9
- 235000011837 pasties Nutrition 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims description 41
- 239000000779 smoke Substances 0.000 claims description 28
- 235000019504 cigarettes Nutrition 0.000 claims description 25
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 24
- 238000000605 extraction Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 14
- 239000000284 extract Substances 0.000 claims description 13
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 12
- 235000013305 food Nutrition 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- 238000013459 approach Methods 0.000 claims description 9
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 8
- 239000012141 concentrate Substances 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 8
- 239000000049 pigment Substances 0.000 claims description 8
- 239000000835 fiber Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 244000062730 Melissa officinalis Species 0.000 claims description 4
- 235000010654 Melissa officinalis Nutrition 0.000 claims description 4
- 239000001569 carbon dioxide Substances 0.000 claims description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 4
- 239000000865 liniment Substances 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000012530 fluid Substances 0.000 claims description 2
- 238000002791 soaking Methods 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 235000019640 taste Nutrition 0.000 abstract description 5
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- 241000208134 Nicotiana rustica Species 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 238000004040 coloring Methods 0.000 abstract 1
- 239000003205 fragrance Substances 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000004480 active ingredient Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 238000013461 design Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 229920002522 Wood fibre Polymers 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention relates to a technology for extracting aromatic series substances from the waste tobacco leaves of tobacco smalls, small tobacco sheets, tobacco stalks, etc. and modulating. A liquid aromatic series substance and a liquid tobacco taste substance which are extracted from the waste tobacco leaves of tobacco smalls, small tobacco sheets, etc. are mixed with an aromatic pasty substance which is extracted from the waste tobacco of tobacco smalls, tobacco leaves, tobacco stalks, etc. according to a proportion and stirred fully to get a semi-flow pattern aromatic series modulating agent, wherein the liquid aromatic series substance has a low boiling point, the liquid tobacco taste substance contains a small amount of aromatic series substance which has a medium-high boiling point, and the aromatic pasty substance contains phenol, sugar, ketone, alkali, nitrogen, coloring matter, etc. The present invention has the advantages that environmental pollution is reduced, the tastes of people are satisfied, and the health of people is ensured simultaneously.
Description
Affiliated technical field:
The present invention relates to a kind of method that adopts the low temperature mode to extract aromatic substance and modulate from waste tobaccos such as offal, little smoked sheet, offal, this method is mainly used in to have modulates fragrance and smoke when the regeneration tobacco leaf that falls burnt effect is made cigarette again.
Background technology:
The quality of tobacco quality is to depend on inherent aromatic substance of tobacco leaf and special chemical composition.A series of means such as tobacco leaf picking, post-production, baking, modulation are the effective links that forms chemical balance.It is to be feature with fragrance that the sense organ of cigarette product requires, and fragrance characteristic reaches the physiological requirement that meets suction.Therefore, fragrance and smoke are the cores of cigarette product, and the development of China's flue-cured tobacco cigarette product is based on English flue-cured tobacco all the time, has formed exclusive product type.In the evolution of product,, arrive development such as the aspect that improves security of products again by emphasizing to increase output in the past to improving quality.This evolution increases and improves the technology content of product beyond doubt, drives the development of cigarette product quality with science and technology.Falling burnt engineering is exactly an important science and technology of implementing for the security that improves cigarette product.From falling burnt technology, present method is the ratio that pipe tobacco is adjusted structure, adjustment stem, expanded cut tobacco, from auxiliary material, takes certain means that filter tip is punched, uses high saturating obbbin, the technological means such as filter tip that extend, but all be that certain limit is arranged.Therefore, using reconstituted tobacco is a kind ofly very importantly to fall burnt means, but all is that certain limit is arranged.Therefore, using reconstituted tobacco is a kind of very important burnt means of falling.The raw material sources of regeneration tobacco leaf are waste material and the out of use raw materials in some production processes, it can not only accelerate flammability, the filling value is very high, can dilute main smoke airflow, simultaneously, to falling Jiao is very effective, and by after using on the tobacco structure, burnt 2-3mg can fall in the consumption of every increase by 10%.Cigarette product uses reconstituted tobacco can effectively reduce harmful substance---the tar of cigarette product.
When extracting the active ingredient of processing material in the waste tobacco, normally the extraction of effectively classifying of effective fragrance component of material, different material compositions has different difference, and main aroma substance is present in positions such as the flower, leaf, stem, root of material, the active constituent content difference at each position.These aromatic substances exist with different chemical constitutions, handle by special technique, have formed various physical forms and have been used by people.
Summary of the invention:
The purpose of this invention is to provide a kind of method that adopts the low temperature mode from waste tobaccos such as offal, little smoked sheet, offal, to extract aromatic substance and modulate, according to the different physical forms and the distribution situation of active ingredient, extract aromatic substance and active ingredient from tobacco waste, be backfilling in the reconstituted tobacco having the tobacco property material, quality, the aesthetic quality of reconstituted tobacco reached or near tobacco material.And use that can be a large amount of, play reduction and consume, save tobacco leaf, reduce tar, turn waste into wealth, be a kind of tobacco material of environment-friendly type.
The invention is characterized in: the low boiling aromatic substance that is in a liquid state that the waste tobacco that (A) is made up of offal and little smoked sheet etc. extracts by overcritical low temperature, the waste tobacco of being made up of offal and little smoked sheet etc. with (B) extracts through extraction kettle, condenser condenses, the food grade phosphoric acid acidifying, the smoke material that is in a liquid state that contains a small amount of middle higher boiling aromatic substance that obtains after concentrating, and (C) by offal, tobacco, the waste tobacco that offal etc. are formed is through soaking steam dissolving fiber, the food grade phosphoric acid acidifying, what obtain after concentrating contains phenol, sugar, ketone, alkali, nitrogen, pigments etc. are the material of paste, mix by weight proportion, in airtight modulation jar, fully stir, obtain the aromatic series modulator of semi-fluid attitude.
The detailed process that the present invention extracts the low boiling aromatic substance that is in a liquid state is: will be added by the waste tobacco that offal and little smoked sheet etc. is formed in the means of supercritical extraction device, feed liquid carbon dioxide as medium, below-20 ℃ and 2 below the handkerchief, through 20-40 minute, the brown low boiling aromatic substance that contains a small amount of smoke material that obtains being in a liquid state.
The detailed process that the present invention extracts the smoke material is: will be added by the waste tobacco that offal and little smoked sheet etc. is formed in the extraction kettle, extraction is more than at least 8 hours under 50-80 ℃ and normal temperature, the liquid that obtains is through condenser condenses, after its temperature is reduced to 10-25 ℃, add food grade phosphoric acid and carry out acidifying, obtain the acid solution that pH value is 6.2-6.8, process reclaims distillation and concentrates the brown smoke material that contains a small amount of middle higher boiling aromatic substance that obtains being in a liquid state.
The present invention produces and contains the detailed process that phenol, sugar, ketone, alkali, nitrogen, pigment etc. are pasty masses and be: the waste tobacco that will mainly be made up of tobacco leaf, offal, the cigarette ridge etc. is soaked in water, feed steam simultaneously, under form at steam airtight solution temperature 90-100 ℃ and the normal pressure, soak and dissolve fiber at least more than 12 hours, add food grade phosphoric acid again and carry out acidifying, obtain the acid solution that pH value is 6.2-6.8, concentrate the material that obtains being the balm shape through reclaiming distillation.
The low boiling aromatic substance that contains a small amount of smoke material of the present invention, contain a small amount of in the higher boiling aromatic substance the smoke material and contain the technical indicator that the materials of organisms such as phenol, sugar, ketone, alkali, nitrogen, pigment modulates and be: refraction index 1.4140-1.4170; Mixed solution density is 1.2070-1.1820.
The low boiling aromatic substance that contains a small amount of smoke material of the present invention, contain a small amount of in the smoke material of higher boiling fragrance group material and the material that contains organisms such as phenol, sugar, ketone, alkali, nitrogen, the pigment temperature and pressure when modulating be normal temperature and pressure.
The present invention can be according to the different places of production or the varying environment zone or the waste tobacco in different times, and according to the requirement of cigarette mouthfeel and technical indicator, carry out segmentation---time, temperature etc. are extracted desired substance, and, carry out modulation in various degree by different cigarette product design typifications and the demand on tobacco structure.
The aromatic series modulator main application that modulator approach of the present invention produced is: after the substrate that reproduces smoked sheet forms, tobacco aroma by the modulator approach modulation, fragrance, trace element reaches the fragrance of line drawing again, fragrance, materials such as balm, adopt rubbing method, promptly be sprayed in the substrate, make that the wood fibre breath of reproducing smoked sheet is heavy, burn mouth, defectives such as smokeless hay-scented flavor are eliminated, fundamentally improved the value of reproducing smoked sheet, can form the style and the type of required product, and can be according to the designing requirement of different product, by the modulation of the technology of the present invention, produce different-style, type, the reconstituted tobacco of sugar alkali ratio.
The present invention has also solved large-area environmental pollution, has reduced sewage disposal; Simultaneously the contained tar of reconstituted tobacco itself is low, has ensured that when satisfying people's taste people's is healthy.
The specific embodiment:
Embodiment 1 modulates based on the different cigarette product that contains cigarette fragrance mouthfeel of needs:
At first extract the low boiling aromatic substance be in a liquid state: in the waste tobacco that will form by offal and little smoked sheet etc. in the adding means of supercritical extraction device, feed liquid carbon dioxide as medium, at-20 ℃ and 2 handkerchiefs, through 30 minutes, the brown low boiling aromatic substance that contains a small amount of smoke material that obtains being in a liquid state.
Next extracts the smoke material: will be added by the waste tobacco that offal and little smoked sheet etc. is formed in the extraction kettle, extraction is 10 hours under 60 ℃ and normal temperature, the liquid that obtains is through condenser condenses, after its temperature is reduced to 20 ℃, add food grade phosphoric acid and carry out acidifying, obtain pH value and be 6.6 acid solution, concentrate and get through reclaiming distillation.
Produce then and contain phenol, sugar, ketone, alkali, nitrogen, pigment etc. and be pasty masses: the waste tobacco that will mainly be made up of tobacco leaf, offal, the cigarette ridge etc. is soaked in water, feed steam simultaneously, under 100 ℃ of the airtight solution temperatures and normal pressure that steam forms, soak and dissolved fiber in 15 hours, add food grade phosphoric acid again and carry out acidifying, obtain pH value and be 6.6 acid solution, concentrate and get through reclaiming distillation.
The smoke material of higher boiling aromatic substance and the technical indicator that pasty masses is modulated are in will containing the low boiling aromatic substance of a small amount of smoke material and containing on a small quantity: refraction index 1.4140-1.4170; Mixed solution density is 1.19000-1.1820.
Embodiment 2 modulates based on the cigarette product that needs the smoke mouthfeel:
At first extract the low boiling aromatic substance be in a liquid state: in the waste tobacco that will form by offal and little smoked sheet etc. in the adding means of supercritical extraction device, feed liquid carbon dioxide as medium, at-30 ℃ and 1 handkerchief, through 30 minutes, the brown low boiling aromatic substance that contains a small amount of smoke material that obtains being in a liquid state.
Next extracts the smoke material: will be added by the waste tobacco that offal and little smoked sheet etc. is formed in the extraction kettle, extraction is 12 hours under 60 ℃ and normal temperature, the liquid that obtains is through condenser condenses, after its temperature is reduced to 10 ℃, add food grade phosphoric acid and carry out acidifying, obtain pH value and be 6.3 acid solution, concentrate and get through reclaiming distillation.
Produce then and contain phenol, sugar, ketone, alkali, nitrogen, pigment etc. and be pasty masses: the waste tobacco that will mainly be made up of tobacco leaf, offal, the cigarette ridge etc. is soaked in water, feed steam simultaneously, under 95 ℃ of the airtight solution temperatures and normal pressure that steam forms, soak and dissolved fiber in 13 hours, add food grade phosphoric acid again and carry out acidifying, obtain pH value and be 6.3 acid solution, concentrate and get through reclaiming distillation.
The smoke material of higher boiling aromatic substance and the technical indicator that pasty masses is modulated are in will containing the low boiling aromatic substance of a small amount of smoke material and containing on a small quantity: refraction index 1.4160-1.4170; Mixed solution density is 1.2070-1.1920.
The present invention can be according to the different places of production or the varying environment zone or the waste tobacco in different times, and according to the requirement of cigarette mouthfeel and technical indicator, carry out segmentation---time, temperature etc. are extracted desired substance, and, carry out modulation in various degree by different cigarette product design typifications and the demand on tobacco structure.
The present invention has not only solved large-area environmental pollution, has reduced sewage disposal; Simultaneously the contained tar of reconstituted tobacco itself is low, has ensured that when satisfying people's taste people's is healthy.
Claims (6)
1, the extraction and the modulator approach of aromatic substance in the useless cigarette, it is characterized in that: the low boiling aromatic substance that is in a liquid state that the waste tobacco that (A) is made up of offal and little smoked sheet etc. extracts by overcritical low temperature, the waste tobacco of being made up of offal and little smoked sheet etc. with (B) extracts through extraction kettle, condenser condenses, the food grade phosphoric acid acidifying, the smoke material that is in a liquid state that contains a small amount of middle higher boiling aromatic substance that obtains after concentrating, and (C) by offal, tobacco, the waste tobacco that offal etc. are formed is through soaking steam dissolving fiber, the food grade phosphoric acid acidifying, what obtain after concentrating contains phenol, sugar, ketone, alkali, nitrogen, pigments etc. are the material of paste, mix by weight proportion, in airtight modulation jar, fully stir, obtain the aromatic series modulator of semi-fluid attitude.
2, the extraction and the modulator approach of aromatic substance in the useless cigarette according to claim 1, it is characterized in that: the detailed process that the present invention extracts the low boiling aromatic substance that is in a liquid state is: will be added by the waste tobacco that offal and little smoked sheet etc. is formed in the means of supercritical extraction device, feed liquid carbon dioxide as medium, below-20 ℃ and 2 below the handkerchief, through 20-40 minute, the brown low boiling aromatic substance that contains a small amount of smoke material that obtains being in a liquid state.
3, the extraction and the modulator approach of aromatic substance in the useless cigarette according to claim 1, it is characterized in that: the detailed process that the present invention extracts the smoke material is: will be added by the waste tobacco that offal and little smoked sheet etc. is formed in the extraction kettle, extraction is more than at least 8 hours under 50-80 ℃ and normal temperature, the liquid that obtains is through condenser condenses, after its temperature is reduced to 10-25 ℃, add food grade phosphoric acid and carry out acidifying, obtain the acid solution that pH value is 6.2-6.8, process reclaims distillation and concentrates the brown smoke material that contains a small amount of middle higher boiling aromatic substance that obtains being in a liquid state.
4, the extraction and the modulator approach of aromatic substance in the useless cigarette according to claim 1, it is characterized in that: the present invention produces and contains phenol, sugar, ketone, alkali, nitrogen, the detailed process that pigment etc. are balm shape material is: will be mainly by tobacco leaf, offal, the waste tobacco of compositions such as the cigarette ridge is soaked in water, feed steam simultaneously, under form at steam airtight solution temperature 90-100 ℃ and the normal pressure, soak and dissolve fiber at least more than 12 hours, add food grade phosphoric acid again and carry out acidifying, obtain the acid solution that pH value is 6.2-6.8, concentrate the material that obtains being the balm shape through reclaiming distillation.
5, the extraction and the modulator approach of aromatic substance in the useless cigarette according to claim 1 is characterized in that: the low boiling aromatic substance of a small amount of smoke material, the smoke material that contains a small amount of middle higher boiling aromatic substance and the technical indicator that pasty masses is modulated of containing of the present invention is: refraction index 1.4140-1.4170; Mixed solution density is 1.2070-1.1820.
6, the extraction and the modulator approach of aromatic substance in the useless cigarette according to claim 5 is characterized in that: the low boiling aromatic substance that contains a small amount of smoke material of the present invention, contain a small amount of in the smoke material of higher boiling aromatic substance and the pasty masses temperature and pressure when modulating be normal temperature and pressure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01128925 CN1204837C (en) | 2001-09-30 | 2001-09-30 | Extracting and preparing technology for aromatic matter in waste tobacco |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01128925 CN1204837C (en) | 2001-09-30 | 2001-09-30 | Extracting and preparing technology for aromatic matter in waste tobacco |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1408288A CN1408288A (en) | 2003-04-09 |
| CN1204837C true CN1204837C (en) | 2005-06-08 |
Family
ID=4668735
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 01128925 Expired - Lifetime CN1204837C (en) | 2001-09-30 | 2001-09-30 | Extracting and preparing technology for aromatic matter in waste tobacco |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1204837C (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102199490B (en) * | 2010-03-24 | 2012-11-21 | 郑州轻工业学院 | Method for extracting neutral aroma compositions in tobacco |
| CN102613691B (en) * | 2012-03-23 | 2014-09-10 | 华南理工大学 | Preparation method and application of tobacco flavor |
| CN105950294A (en) * | 2016-05-28 | 2016-09-21 | 黄宇松 | Lavandula pedunculata flower aromatic material extraction method |
| CN111876256A (en) * | 2020-07-16 | 2020-11-03 | 云南中烟工业有限责任公司 | Fresh and sweet flavor type tobacco essence and preparation method and application thereof |
| CN112056607B (en) * | 2020-09-29 | 2023-05-26 | 云南中烟工业有限责任公司 | Device and method for on-line perfuming of spice with high and low boiling point components |
-
2001
- 2001-09-30 CN CN 01128925 patent/CN1204837C/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CN1408288A (en) | 2003-04-09 |
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Effective date of registration: 20120331 Address after: 610071 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee after: China Tobacco Chuanyu Industrial Co., Ltd. Address before: 610071, No. two, Hongxing Road, Chengdu, 86 Patentee before: China Tobacco Chuanyu Industrial Corporation |
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Effective date of registration: 20161219 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610071 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industry Co., Ltd. |
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