CN1189456C - 高纯度己内酰胺的制备方法 - Google Patents

高纯度己内酰胺的制备方法 Download PDF

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Publication number
CN1189456C
CN1189456C CNB981233236A CN98123323A CN1189456C CN 1189456 C CN1189456 C CN 1189456C CN B981233236 A CNB981233236 A CN B981233236A CN 98123323 A CN98123323 A CN 98123323A CN 1189456 C CN1189456 C CN 1189456C
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CN
China
Prior art keywords
hexalin
methylcyclopentanol
pimelinketone
reaction
cyclohexanone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB981233236A
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English (en)
Chinese (zh)
Other versions
CN1226553A (zh
Inventor
徐明锡
朴昇彦
李畅晃
李明弘
李始根
金桢浩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hyosung Corp
Original Assignee
Hyosung Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hyosung Corp filed Critical Hyosung Corp
Publication of CN1226553A publication Critical patent/CN1226553A/zh
Application granted granted Critical
Publication of CN1189456C publication Critical patent/CN1189456C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/08—Oxygen atoms
    • C07D223/10—Oxygen atoms attached in position 2

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Closures For Containers (AREA)
CNB981233236A 1997-12-08 1998-12-08 高纯度己内酰胺的制备方法 Expired - Fee Related CN1189456C (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
KR66783/97 1997-12-08
KR66783/1997 1997-12-08
KR1019970066783A KR100231761B1 (ko) 1997-12-08 1997-12-08 고순도 카프로락탐의 제조방법

Publications (2)

Publication Number Publication Date
CN1226553A CN1226553A (zh) 1999-08-25
CN1189456C true CN1189456C (zh) 2005-02-16

Family

ID=19526727

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB981233236A Expired - Fee Related CN1189456C (zh) 1997-12-08 1998-12-08 高纯度己内酰胺的制备方法

Country Status (8)

Country Link
US (1) US6245907B1 (cg-RX-API-DMAC10.html)
KR (1) KR100231761B1 (cg-RX-API-DMAC10.html)
CN (1) CN1189456C (cg-RX-API-DMAC10.html)
DE (1) DE19856205A1 (cg-RX-API-DMAC10.html)
ID (1) ID21435A (cg-RX-API-DMAC10.html)
IN (1) IN189018B (cg-RX-API-DMAC10.html)
IT (1) IT1303824B1 (cg-RX-API-DMAC10.html)
TW (1) TW555748B (cg-RX-API-DMAC10.html)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100359206B1 (ko) * 2000-02-14 2002-11-04 주식회사 효성 고순도 카프로락탐의 제조 방법
JP4198052B2 (ja) * 2001-07-25 2008-12-17 旭化成ケミカルズ株式会社 シクロヘキサノンオキシムの製造方法
US7022844B2 (en) 2002-09-21 2006-04-04 Honeywell International Inc. Amide-based compounds, production, recovery, purification and uses thereof
US20060189829A1 (en) * 2005-02-18 2006-08-24 Basf Corporation Method of minimizing aldehyde based impurities in a process stream
MY157220A (en) * 2011-07-12 2016-05-13 Asahi Kasei Chemicals Corp Cyclohexanol, method for producing cyclohexanol, and method for producing adipic acid
CN102675176B (zh) * 2012-05-31 2016-12-14 中国天辰工程有限公司 一种以高纯苯为原料生产己内酰胺的方法
EP2895454B1 (en) * 2012-09-14 2016-11-30 ExxonMobil Chemical Patents Inc. Process for separating methylcyclopentanone from cyclohexanone
CN117192026A (zh) * 2023-07-24 2023-12-08 湖北三宁化工股份有限公司 己内酰胺生产过程中溶剂重排反应产物的酸肟比分析方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL7206342A (cg-RX-API-DMAC10.html) 1971-05-18 1972-11-21
NL7613947A (nl) 1976-12-16 1978-06-20 Stamicarbon Werkwijze voor het bereiden van een cycloal- kanol.
TW218865B (cg-RX-API-DMAC10.html) 1992-01-24 1994-01-11 Asahi Carbon Kabushiki Kaisha
JP3789504B2 (ja) * 1995-01-12 2006-06-28 旭化成ケミカルズ株式会社 ε−カプロラクタムの製造方法
US5900482A (en) * 1995-07-20 1999-05-04 Mitsubishi Chemical Corporation Process for the preparation of ε-caprolactam
KR970706249A (ko) 1995-07-20 1997-11-03 미우라 아끼라 엡실론-카프로락탐의 제조방법(process for the preparation of epsilon-caprolactam)

Also Published As

Publication number Publication date
DE19856205A1 (de) 1999-06-10
ITMI982635A1 (it) 1999-06-08
CN1226553A (zh) 1999-08-25
KR100231761B1 (ko) 1999-11-15
ID21435A (id) 1999-06-10
IT1303824B1 (it) 2001-02-23
IN189018B (cg-RX-API-DMAC10.html) 2002-12-07
US6245907B1 (en) 2001-06-12
TW555748B (en) 2003-10-01
KR19990048166A (ko) 1999-07-05

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20050216

Termination date: 20151208

EXPY Termination of patent right or utility model