CN118078729B - Cleansing cream with moisturizing and skin care effects and preparation method thereof - Google Patents

Cleansing cream with moisturizing and skin care effects and preparation method thereof Download PDF

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CN118078729B
CN118078729B CN202410487470.9A CN202410487470A CN118078729B CN 118078729 B CN118078729 B CN 118078729B CN 202410487470 A CN202410487470 A CN 202410487470A CN 118078729 B CN118078729 B CN 118078729B
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sodium
cleansing cream
oil
stirring
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CN118078729A (en
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高博闻
王垚
钟一竹竹
高鹿鸣
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Alcohol International Biotechnology Beijing Co ltd
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Alcohol International Biotechnology Beijing Co ltd
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Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to a cleansing cream with moisturizing and skin care effects and a preparation method thereof. The cleansing cream is prepared by adopting a flocculation technology and mainly comprises the following components: sodium lauroyl glutamate, glycerol, ethylhexyl glycerol, polyethylene glycol-8, lauryl hydroxysulfobetaine, betaine, polyquaternium-52, polyethylene glycol-32, PEG-75 lanolin, PEG-120 methyl glucose triisostearate, PEG-120 esters of jojoba wax, aloe vera, sodium polyacrylate grafted starch, modified corn starch, and flavoring ingredients. The cleansing cream provided by the invention meets the requirements of people on fresh use, strong cleansing capability, mildness, no stimulation, skin care effect and fragrance Gao Yayi, is suitable for all skin groups in the whole age group, and is particularly suitable for sensitive muscle groups.

Description

Cleansing cream with moisturizing and skin care effects and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a cleansing cream with moisturizing and skin care effects and a preparation method thereof.
Background
With the improvement of living standard, more and more female consumers use makeup products to beautify the face. Conventional makeup products include foundation, lipstick, mascara, eye shadow, blush, etc., and most of the makeup products are oil-soluble or oil-dispersible in view of the need for sweat resistance, moisture resistance, and makeup removal resistance, and the makeup formulation typically contains a large amount of grease, wax, silicone oil, etc. After the makeup product is applied to the face, the makeup product has strong skin adhesion and is difficult to clean by using a common face cleaning product. If the makeup is not removed sufficiently, the residual makeup may be deposited on the skin, making the skin dull and lack gloss, and dirt deposited on the skin surface may also clog pores, and after a long time, the skin may become rough and dull, and may also cause problems such as pores being large, blackheads, closed acnes, and the like. However, if the cleansing agent is used, there are problems such as skin irritation and skin allergy. Therefore, the makeup removal is the most important link in skin care, and the demand of the makeup removal products with strong cleaning performance, mild and no irritation is large in the market.
Early make-up removal products were typically make-up removal water and make-up removal oil, but these products often had problems with being inconvenient to carry and use. Although the skin care concept of "nourishing skin with oil" has been increasingly favored by consumers in recent years, cleansing products with both cleansing and skin care effects are less common in the market at present, and the general cleansing oil products are easy to feel greasy and have strong irritation when used by consumers. Compared with the cleansing water and cleansing oil in early stage, the cleansing cream is pasty, does not have strong fluidity, can not run off from the finger joints during use, has the characteristics of convenient use and carrying, and is popular with consumers at present. However, most of the cleansing cream products on the market are mainly composed of grease formulations, and are added with wax base to form solid forms, such as mineral wax, synthetic wax, and the like. The product is generally greasy in skin feel, needs to be repeatedly washed by clear water, and has strong tightness after cleaning.
In view of the above problems of the makeup removing products commonly found in the market at present, it would be more convenient for consumers to develop a makeup removing cleansing product with stronger makeup removing cleansing ability, lower irritation, milder, oil nourishing skin concept and skin care effect, fragrance Gao Yayi and portability.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides a cleansing cream with moisturizing and skin care effects and a preparation method thereof. The cleansing cream provided by the invention meets the requirements of people on fresh use, strong cleansing capability, mildness, no stimulation, skin care effect, fragrance Gao Yayi and the like, is suitable for all skin groups in the whole age group, and is particularly suitable for sensitive muscle groups.
In order to achieve the above object, the present invention provides the following technical solutions:
In a first aspect, the invention provides a makeup removing cleansing cream with moisturizing and skin care effects, which comprises the following components in percentage by weight: 5% -40% of amino acid anionic surfactant, 0.01% -0.1% of cationic polymer, 1% -10% of multifunctional surfactant, 1% -20% of viscosity modifier, 10% -40% of moisturizing emollient, 0.2% -1% of perfume ingredient, 0% -2% of preservative and deionized water.
Alternatively, in the makeup removing cleansing cream, the makeup removing cleansing cream comprises the following components in percentage by weight: 15-35% of amino acid anionic surfactant, 0.02-0.08% of cationic polymer, 2-8% of multifunctional surfactant, 5-15% of viscosity modifier, 12-38% of moisturizing emollient, 0.5-1% of perfume ingredient, 0.5-1% of preservative and deionized water.
Alternatively, in the above makeup removing cleansing cream, the amino acid anionic surfactant is selected from one or more of the following: sodium lauroyl glutamate, sodium lauroyl sarcosinate, sodium myristoyl sarcosinate, sodium cocoyl glutamate, potassium cocoyl glycinate, potassium laureth phosphate.
Preferably, the amino acid anionic surfactant is sodium lauroyl glutamate.
Alternatively, in the above cleansing cream, the cationic polymer is selected from one or more of the following: polyquaternium-7, polyquaternium-10, polyquaternium-39, polyquaternium-47 or polyquaternium-52.
Preferably, the cationic polymer is selected from the group consisting of polyquaternium-52.
Alternatively, in the above cleansing cream, the multifunctional surfactant is selected from one or more of the following: polyethylene glycol-8, polyethylene glycol-32, PEG-75 lanolin, lauryl hydroxysulfobetaine, lauramidopropyl betaine, sodium laureth-6 carboxylate, laureth-16 or glycolipid.
Preferably, the multifunctional surfactant is a combination of polyethylene glycol-8, polyethylene glycol-32, PEG-75 lanolin, lauryl hydroxysulfobetaine and betaine.
More preferably, polyethylene glycol-8: polyethylene glycol-32: PEG-75 lanolin: lauryl hydroxysulfobetaine: the proportion of betaine is in the range of (5% -30%): (1% -10%): (0.5% -5%): (0.01% -3.5%).
Alternatively, in the above cleansing cream, the viscosity modifier is selected from one or more of the following: hydroxypropyl starch, PEG-120 methyl glucose dioleate, PEG-120 methyl glucose trioleate, PEG-120 methyl glucose triisostearate, sodium polyacrylate grafted starch, modified corn starch, acrylic acid ester copolymer, PEG-160 sorbitan triisostearate, PEG-150 pentaerythritol tetrastearate or hydrolyzed corn starch.
Preferably, the viscosity modifier is a combination of PEG-120 methyl glucose triisostearate, sodium polyacrylate grafted starch, and modified corn starch.
More preferably, PEG-120 methyl glucose triisostearate: sodium polyacrylate grafted starch: the proportion range of the modified corn starch is (0.1% -5%): (0.05% -0.5%): (0.05% -0.5%).
Alternatively, in the above cleansing cream, the moisturizing emollient is selected from one or more of the following: glycerol, ethylhexyl glycerol, jojoba wax PEG-120 esters, caprylic glycol, glycerol polyether-26, ALOE vera (Aloe BARBADENSIS) leaf juice, carbomer, p-hydroxyacetophenone, 1, 2-pentanediol, cultivated nigella sativa (NIGELLASATIVA) seed extract, cultivated nigella sativa (NIGELLASATIVA) seed oil, chamomile (CHAMOMILLARECUTITA) flower/leaf/stem extract, chamomile (CHAMOMILLA RECUTITA) flower extract, wolfberry (LYCIUM CHINENSE) fruit extract, honey extract, white willow (SALIXALBA) bark extract, mountain ibu (BAROSMABETULINA) leaf extract, pinus (ALCHEMLLA VULGARIS) extract, lactobacillus fermentation product, or bis (PPG-2 myristoleic polyether-10) adipate.
Preferably, the moisturizing emollient is a combination of glycerin, ethylhexyl glycerin, jojoba wax PEG-120 esters, caprylic glycol, ALOE vera (Aloe BARBADENSIS) leaf juice, and carbomers.
More preferably, the glycerol, in weight proportions: ethylhexyl glycerol: jojoba wax PEG-120 esters: octyl glycol: aloe BARBADENSIS (Aloe BARBADENSIS) leaf juice: the carbomer ratio range is (5% -30%): (0.05% -3%) (0.01% -7%): (0.01% -1%): (0.1% -1%): (0.05% -0.8%).
Alternatively, in the cleansing cream, the perfume ingredient includes one or more of the following: the composition comprises a combination of lavender (LAVANDULA HYBRIDA) oil, lavender (LAVANDULA ANGUSTIFOLIA) oil, lavender (LAVANDULA sphica) flower/leaf/stem extract, CITRUS SINENSIS (CITRUS SINENSIS) extract, grapefruit (CITRUS PARADSIS) peel oil, bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, CITRUS (CITRUS RETICULATA) peel extract, lemon (CITRUS LIMON) peel oil, lime (CITRUS AURANTIFOLIA) oil, CITRUS (CITRUS RETICULATA) peel extract, bitter orange (CITRUS AURANTIUM AMARA) peel oil, CITRUS JUNOS) fruit oil, CITRUS grandis (CITRUS GRANDIS) peel oil, CITRUS TANGERINA (CITRUS TANGERINA) peel oil, CITRUS UNSHIU (CITRUS shurier iu) peel extract, CITRUS grandis (CITRUSCLEMENTINA) fruit extract, or lime (CITRUS AURANTIUMDULCIS) oil.
Preferably, the flavor component is a combination of lavender (LAVANDULA HYBRIDA) oil, CITRUS SINENSIS (CITRUS SINENSIS) extract, grapefruit (CITRUS PARADSIS) peel oil, bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, CITRUS (CITRUS RETICULATA) peel extract, and lemon (CITRUS LIMON) peel oil.
More preferably, the lavender (LAVANDULA HYBRIDA) oil, in weight ratio: sweet orange (CITRUS SINENSIS) extract: grapefruit (CITRUS PARADSIS) peel oil: bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil: citrus (CITRUS RETICULATA) peel extract: the ratio of lemon (CITRUS LIMON) peel oil ranges from (0.05% to 1%): (0.05% -1%): (0.005% -0.5%).
Alternatively, the cleansing cream is prepared from the following components by flocculation technology: sodium lauroyl glutamate, polyquaternium-52, polyethylene glycol-8, polyethylene glycol-32, PEG-75 lanolin, lauryl hydroxysulfobetaine, betaine, PEG-120 methyl glucose triisostearate, sodium polyacrylate grafted starch, modified corn starch, glycerol, ethylhexyl glycerol, jojoba wax PEG-120 esters, caprylic glycol, ALOE vera (ALOE BARBADENSIS) leaf juice, carbomer, miscellaneous lavender (LAVANDULA HYBRIDA) oil, CITRUS SINENSIS (CITRUS SINENSIS) extract, grapefruit (CITRUS PARADSIS) peel oil, bergamot (CITRUS AURANTIUM BERGAMIA) peel oil, CITRUS (CITRUS RETICULATA) peel extract, lemon (CITRUS LIMON) peel oil, potassium sorbate, sodium benzoate, sodium chloride, disodium EDTA, sodium hydroxide, and deionized water.
Preferably, the cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 15% -35% sodium lauroyl glutamate, 0.02% -0.088% polyquaternium-52, 5% -30% polyethylene glycol-8, 1% -10% polyethylene glycol-32, 0.5% -5% PEG-75 lanolin, 0.01% -3.5% lauryl hydroxysulfobetaine, 0.02% -7% betaine, 0.1% -50.5% PEG-120 methyl glucose triisostearate, 0.05% -0.5% sodium polyacrylate grafted starch, 0.05% -0.5% modified corn starch, 5% -30% glycerin, 0.05% -3% ethylhexyl glycerin, 0.01% -7% jojoba wax PEG-120 esters, 0.01% -1% octaethylene glycol, 0.1% -1% ALOE vera (ALOE BADENSIS) leaf juice, 0.05% -0.8% carbomer, 0.05% -1% champignon-lavender (LAVANDULA HYBRIDA) oil, 0.05% -1% orange (CIUS) extract, 0.05% -1% orange (CITRIS) extract, 0.05% -0.005% sodium Chloride (CIUS) 0.35, 0.05% -0.001% -35% sodium chloride, 0.005% -0.35% fruit peel (CI5% -0.005) and 0.35% -0.001% fruit peel (sodium chloride), 0.005% -0.35% -0.5% fruit peel (sodium chloride).
More preferably, the cleansing cream is prepared from the following components in percentage by weight by flocculation technology: 20% -25% sodium lauroyl glutamate, 0.02% -0.08% polyquaternium-52, 5% -20% polyethylene glycol-8, 0.1% -0.5% polyethylene glycol-32, 0.5% -2% PEG-75 lanolin, 0.1% -2% lauryl hydroxysulfobetaine, 1% -5% betaine, 0.5% -2% PEG-120 methyl glucose triisostearate, 0.1% -0.3% sodium polyacrylate grafted starch, 0.05% -0.3% modified corn starch, 10% -25% glycerin, 0.1% -1% ethylhexyl glycerin, 0.5% -5% jojoba wax PEG-120 esters, 0.1% -1% octaethylene glycol, 0.1% -0.8% ALOE vera (ALOE BADENSIS) leaf juice, 0.05% -0.5% carbomer, 0.1% -0.5% miscellaneous lavender (LAVANDULA HYBRIDA) oil, 0.1% -0.5% orange (CITRIS) extract, 0.01% -0.35% sodium Citrate (CITRUS) extract, 0.05% -0.35% sodium chloride (0.01% -0.001% -0.35% fruit peel oil, 0.01% -0.35% sodium chloride (sodium chloride) and the balance of orange peel oil (sodium chloride, 0.01% -0.001% -0.35% -0.01% -2% fruit peel oil.
Most preferably, the cleansing cream is prepared from the following components in percentage by weight by flocculation technology: 23% sodium lauroyl glutamate, 0.06% polyquaternium-52, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOEs barbansis) leaf juice, 0.2% carbomer, 0.4% miscellaneous lavender (LAVANDULA HYBRIDA) oil, 0.3% sweet orange (CITRUSs) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, 0.05% CITRUS (CITRUS RETICULATA) peel extract, 0.05% lemon (citrusn) fruit oil, 0.00125% potassium sorbate, 0.00575% sodium chloride, sodium benzoate, and the balance sodium chloride, 0.1% sodium chloride, and deionized water.
In a second aspect, the present invention provides a method for preparing the cleansing cream of the first aspect, which is characterized in that: the preparation method comprises the following steps:
(1) Adding the multifunctional surfactant, the moisturizing emollient and part of deionized water into a water pot, uniformly stirring, filtering and pumping into a main pot, adding 1.0% of evaporated water, and stirring in vacuum to ensure no larger caking;
(2) Heating by adjusting stirring speed, homogenizing after reaching the target temperature of 90-95deg.C, uncovering for observation, adding amino acid anionic surfactant after no transparent particles, vacuum, keeping temperature at no lower than 85deg.C after adding amino acid anionic surfactant, keeping warm, stirring until completely dissolving, and continuously adding a small amount of foam on the surface;
(3) Weighing cationic polymer, adding the rest deionized water, heating to 80-85deg.C, and stirring uniformly;
(4) Sequentially adding various viscosity regulators and preservatives, adjusting the stirring speed, stirring in vacuum, adding the dissolved cationic polymer in the step (3) into a main pot, and stirring until uniform;
(5) Opening and cooling, maintaining vacuum, cooling to below 50deg.C, adding flavoring components, and stirring;
(6) Continuously slowly cooling to paste, keeping vacuum, heating to 50-55deg.C, maintaining the temperature, stirring, scraping large blocks on stirring paddles until no caking is generated;
(7) And (3) adjusting the stirring speed, cooling to 41-42 ℃ for displaying, discharging cooling water of the emulsifying tank when the materials are in a uniform yogurt-like liquid state, and discharging the materials at the bottom of the pot.
Alternatively, in the preparation method, in the step (2), the amino acid anionic surfactant is added in a plurality of times, after each addition, a pot cover is covered, and the stirring speed is adjusted in vacuum to homogenize, so that the cationic polymer in the dissolved step (3) is added to the main pot independently in the step (4).
Compared with the prior art, the invention has the beneficial effects that:
(1) The cleansing cream formula of the invention takes amino acid surfactant as a main body, has high solid content and forms a solid form. The invention forms a semi-colloid complex by a flocculation technology through anionic surfactants and cationic polymers of specific types, so that dirt in the air and superfluous grease on the skin surface are more easily adsorbed, and the skin can be directly washed away by clean water, but humectant components and various plant extracts in the formula can be reserved at the same time, so that sebum films can be maintained simultaneously in the skin cleaning process, and skin moisture and soft feel can be improved.
(2) The cleansing cream formula disclosed by the invention is high in safety and nontoxic, so that the protein denaturation degree is extremely low, and the cleansing cream formula disclosed by the invention uses amino acid surfactants and various components with moisturizing and skin-protecting effects so as to reduce the dryness of skin after repeated cleaning by using the cleansing cream disclosed by the invention.
(3) The flocculation technology adopted by the formula of the cleansing cream can also wrap fragrance ingredients, and continuously brings pleasure to the cleaning process. The fragrance in the formula of the cleansing cream comes from cradle fragrance. The aroma components comprise the aroma of fruits of five Rutaceae plants and the aroma of lavender. Wherein, the fruits of the five Rutaceae plants have strong citrus smell, which helps the user to relieve anxiety and emotion and helps the body to clean dirty gas. Lavender has strong oxidation resistance and antibacterial activity, can clean bacteria on the surface of skin, has strong pacifying effect, and can purify the body and mind.
Detailed Description
The invention will be further illustrated with reference to specific examples. It should be understood that the detailed description and specific examples are intended for purposes of illustration only and are not intended to limit the scope of the invention.
The specific techniques or conditions are not identified in the examples and are described in the literature in this field or are carried out in accordance with the product specifications. The reagents or equipment used were conventional products available for purchase through regular channels, with no manufacturer noted.
The experimental methods in the following examples are conventional methods unless otherwise specified. The test materials used in the examples described below, unless otherwise specified, are all commercially available products.
Preparation examples:
Example 1:
The cleansing cream with the moisturizing and skin care effects is prepared from the following components in percentage by weight by adopting a flocculation technology: 23% sodium lauroyl glutamate, 0.06% polyquaternium-52, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOEs barbansis) leaf juice, 0.2% carbomer, 0.4% miscellaneous lavender (LAVANDULA HYBRIDA) oil, 0.3% sweet orange (CITRUSs) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, 0.05% CITRUS (CITRUS RETICULATA) peel extract, 0.05% lemon (citrusn) fruit oil, 0.00125% potassium sorbate, 0.00575% sodium chloride, sodium benzoate, and the balance sodium chloride, 0.1% sodium chloride, and deionized water.
The preparation method of the cleansing cream comprises the following steps:
(1) Adding the multifunctional surfactant, the moisturizing emollient and part of deionized water into a water pot, uniformly stirring, filtering and pumping into a main pot, adding 1.0% of evaporated water, and stirring in vacuum to ensure no larger caking;
(2) Heating at 90-95deg.C, homogenizing, uncovering, observing, adding amino acid anionic surfactant, vacuum, adding amino acid anionic surfactant for several times, covering pot cover, vacuum adjusting stirring speed, homogenizing, keeping temperature at no lower than 85deg.C, keeping warm, stirring until completely dissolving, and adding a small amount of foam;
(3) Weighing cationic polymer, adding the rest deionized water, heating to 80-85deg.C, and stirring uniformly;
(4) Sequentially adding various viscosity regulators and preservatives, adjusting the stirring speed, stirring in vacuum, adding the dissolved cationic polymer in the step (3) into a main pot separately, and stirring until uniform;
(5) Opening and cooling, maintaining vacuum, cooling to below 50deg.C, adding flavoring components, and stirring;
(6) Continuously slowly cooling to paste, keeping vacuum, heating to 50-55deg.C, maintaining the temperature, stirring, scraping large blocks on stirring paddles until no caking is generated;
(7) And (3) adjusting the stirring speed, cooling to 41-42 ℃ for displaying, discharging cooling water of the emulsifying tank when the materials are in a uniform yogurt-like liquid state, and discharging the materials at the bottom of the pot.
Example 2:
The cleansing cream with the moisturizing and skin care effects is prepared from the following components in percentage by weight by adopting a flocculation technology: 20% sodium lauroyl glutamate, 0.08% polyquaternium-52, 12% polyethylene glycol-8, 0.1% polyethylene glycol-32, 2% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 25% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOE BADENSIS) leaf juice, 0.2% carbomer, 0.4% champignon (LAVANDULA HYBRIDA) oil, 0.3% sweet orange (CITRUS SINENSIS) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, 0.05% CITRUS (CITRUS RETICULATA) peel extract, 0.05% lemon (CIUS MOLIN) peel oil, 0.00125% potassium sorbate, 0.00575% sodium chloride, sodium benzoate, and the balance sodium chloride, 0.1% sodium chloride, and deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Example 3
The cleansing cream with the moisturizing and skin care effects is prepared from the following components in percentage by weight by adopting a flocculation technology: 25% sodium lauroyl glutamate, 0.03% polyquaternium-52, 8% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 15% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOEs barbansis) leaf juice, 0.2% carbomer, 0.4% miscellaneous lavender (LAVANDULA HYBRIDA) oil, 0.3% sweet orange (CITRUSs) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, 0.05% CITRUS (CITRUS RETICULATA) peel extract, 0.05% lemon (citrusn) fruit oil, 0.00125% potassium sorbate, 0.00575% sodium chloride, sodium benzoate, and the balance sodium chloride, 0.1% sodium chloride, and deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Comparative example 1:
the cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 23% sodium lauroyl sarcosinate, 0.06% polyquaternium-52, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOE vera bardansis) leaf juice, 0.2% carbomer, 0.4% lavender (LAVANDULA HYBRIDA) oil, 0.3% sweet orange (CITRUSs SINENSIS) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, 0.05% CITRUS (CITRUS RETICULATA) peel extract, 0.05% lemon (citruson) peel oil, 0.00125% potassium sorbate, 0.00575% sodium chloride, sodium benzoate, and the balance sodium chloride, 0.1.1% sodium chloride, and deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Comparative example 2:
The cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 23% sodium lauroyl glutamate, 0.06% polyquaternium-10, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOEs barbansis) leaf juice, 0.2% carbomer, 0.4% miscellaneous lavender (LAVANDULA HYBRIDA) oil, 0.3% sweet orange (CITRUSs) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil, 0.05% CITRUS (CITRUS RETICULATA) peel extract, 0.05% lemon (citrusn) fruit oil, 0.00125% potassium sorbate, 0.00575% sodium chloride, sodium benzoate, and the balance sodium chloride, 0.1% sodium chloride, and deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Comparative example 3:
The cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 23.06% sodium lauroyl glutamate, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% caprylyl glycol, 0.4975% ALOE vera (ALOE barbannsis) leaf juice, 0.2% carbomer, 0.4% champignon (LAVANDULA HYBRIDA) oil, 0.3% orange (CITRUSs SINENSIS) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) peel oil, 0.05% CITRUS peel extract, 0.05% lemon (CITRUS mon) peel oil, 0.00125% potassium sorbate, 24% sodium benzoate, sodium chloride, the balance being sodium chloride, 0.1.1% sodium chloride, and deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Comparative example 4:
The cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 23% sodium lauroyl glutamate, 0.06% polyquaternium-52, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18.4975% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.2% carbomer, 0.4% champignon (LAVANDULA HYBRIDA) oil, 0.3% orange (CITRUSs sinesis) extract, 0.05% grapefruit (CITRUS PARADSIS) peel oil, 0.05% bergamot (CITRUS AURANTIUM BERGAMIA) peel oil, 0.05% CITRUS (CITRUS RETICULATA) extract, 0.05% lemon (CITRUS) peel oil, 0.00125% potassium sorbate 0.00575%, 0.175% sodium benzoate, 0.1% sodium edta, and the balance sodium chloride, deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Comparative example 5:
The cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 23% sodium lauroyl glutamate, 0.06% polyquaternium-52, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% ALOE vera (ALOE vera) leaf juice, 0.2% carbomer, 0.4% champignon (LAVANDULA HYBRIDA) oil, 0.5% sweet orange (CITRUSs sinesis) extract, 0.00125% potassium sorbate, 0.00575% sodium benzoate, 0.175% sodium chloride, 0.1% disodium edta, 0.1% sodium hydroxide, and the balance deionized water.
The preparation method of the makeup removing cleansing cream is the same as that of example 1.
Effect examples:
1. stability test:
The samples prepared in examples 1 to 3 and comparative examples 1 to 5 were uniformly placed in a high and low temperature oven for 90 days, and the change of the appearance state of the samples was observed.
The test results are shown in table 1 below.
The experimental results in table 1 show that the cleansing cream products of the present invention shown in examples 1-3 are stable both at low temperatures and at high temperatures. However, the cleansing cream shown in comparative examples 1 to 3 was stable at low temperatures, but oil bleeding occurred to various degrees under high temperature conditions, indicating that the components of the cleansing cream had some effect on the overall stability of the product.
2. Mildness test:
Mildness test method: the basic principle of the method of erythrocyte hemolysis test (Red blood cell test RBC) is to measure the damage of chemicals to cell membranes and the resulting change in permeability of cell membranes, and to evaluate the damage degree of cell membranes by measuring the amount of hemoglobin leaking from erythrocytes, which has a direct correlation with the irritation of the product. RBC experiments are mainly used internationally for eye irritation research of cosmetics products, raw materials and other chemicals. The present invention thus determines the mildness of the formulation by testing the formulation by erythrocyte hemolysis assay.
The specific method comprises the following steps: the haemolysis rate and the H 50 value (i.e. the concentration of the test substance at which 50% of the erythrocytes are haemolysed) can be calculated by spectrophotometry of the absorbance of the suspension of erythrocytes after the action of the chemical. The H 50 value is small, namely, obvious hemolysis can occur by adding a small amount of sample, which indicates that the sample has large irritation and poor mildness. A large H 50 value indicates that the sample has small irritation and increased mildness.
The test results are shown in table 2 below.
Table 2: mild test results of the make-up removal cleansing cream of the present invention
The experimental results in table 2 show that the cleansing cream products of the present invention shown in examples 1-3 have a higher mildness, with the H 50 value of the product of example 1 being highest. However, the cleansing cream shown in comparative examples 1 to 5, except that the H 50 value of comparative example 5 was close to that of examples 1 to 3, the H 50 values of the remaining four comparative examples were all reduced to different extents, indicating that the components of the cleansing cream have a large influence on the mildness of the product.
3. Susceptibility assessment of small-scale volunteers:
the products of examples 1 to 3 and comparative examples 1 to 5 prepared in the above preparation examples were compared, and the evaluation was made in volunteers on the indexes of flavor, mildness, easy-to-rinse property, moisture retention and the like.
The evaluation method comprises the following steps: the detection is carried out by means of sensory evaluation by adopting a volunteer for trial. Volunteers were all 18-40 years old, equally male and female. The group was divided into 8 groups of 8 persons each.
Fragrance evaluation: preference degree of fragrance before and during use.
Mildness assessment: during use, the product's mildness is felt.
Easy rinse performance evaluation: it is felt whether the bath lotion is easy to wash.
Moisture retention evaluation: by touching the skin, the moisturizing performance of the skin after use is felt.
By scoring the products of examples 1-3 and comparative examples 1-5 for flavor, mildness, easy rinse performance and post use moisturization performance, each total score was 10 points, the highest score was 10 points, the lowest score was 1 point, and the average score was taken. The evaluation period was 4 weeks.
The evaluation results are shown in table 3 below.
Table 3: evaluation results of the susceptibility of Small volunteers of the cleansing cream of the present invention
The experimental results in table 3 show that the cleansing cream products of the present invention shown in examples 1-3 have a higher volunteer use sensitivity score in terms of fragrance, mildness, ease of rinsing and moisturization.
However, the cleansing cream shown in comparative examples 1 to 5 has a significant reduction in the scores in terms of the indexes of fragrance, mildness, ease of flushing, moisture retention and the like due to replacement or deletion of a part of the components of the cleansing cream product of the present invention, which indicates that the components of the cleansing cream have a significant influence on the use experience of the product.
4. Large-scale consumer product usage and tolerability feedback results
60 Subjects were enrolled and 60 subjects were eventually counted, with an average age of 29.40.+ -. 0.89 years, from 18 to 37 years. The cleansing cream product of the present invention prepared in preparation example 1 was used at least 1 time per day.
Each subject used the test samples as required within 28 days, and showed no adverse reaction according to the adverse reaction recording results according to cosmetic safety technical Specification 2015.
The subject agrees with each index after 28 days using the cleansing cream product of the present invention prepared in example 1 as shown in table 4 below.
Table 4: subject agrees with each index after 28 days using the cleansing cream product of the present invention prepared in example 1
Evaluation index: the number of people with N being more than or equal to 4 is counted by dividing 1 into 'very different agreements', 2 into 'different agreements', 3 into 'agreements', and 4 into 'very agreements'.
It will be apparent to those skilled in the art that various modifications and variations can be made to the present invention without departing from the spirit or scope of the invention. Thus, it is intended that the present invention also include such modifications and alterations insofar as they come within the scope of the appended claims or the equivalents thereof.

Claims (4)

1. A cleansing cream with moisturizing and skin care functions is characterized in that: the cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 20% -25% sodium lauroyl glutamate, 0.02% -0.08% polyquaternium-52, 5% -20% polyethylene glycol-8, 0.1% -0.5% polyethylene glycol-32, 0.5% -2% PEG-75 lanolin, 0.1% -2% lauryl hydroxysulfobetaine, 1% -5% betaine, 0.5% -2% PEG-120 methyl glucose triisostearate, 0.1% -0.3% sodium polyacrylate grafted starch, 0.05% -0.3% modified corn starch, 10% -25% glycerin, 0.1% -1% ethylhexyl glycerin, 0.5% -5% jojoba wax PEG-120 esters, 0.1% -1% octaethylene glycol, 0.1% -0.8% aloe vera leaf juice, 0.05% -0.5% carbomer, 0.1% -0.5% champignon oil, 0.1% -0.5% orange extract, 0.01% -0.1% grapefruit oil, 0.01% -0.3% sodium polyacrylate grafted starch, 0.05% -0.001% sodium chloride, and the balance of sodium hydroxide, 0.001% -0.001% sodium chloride, 0.05% -2% orange peel, 0.001% -0.05% -sodium chloride, and the balance sodium chloride.
2. The make-up removal cleansing cream of claim 1, wherein: the cleansing cream is prepared from the following components in percentage by weight by adopting a flocculation technology: 23% sodium lauroyl glutamate, 0.06% polyquaternium-52, 10% polyethylene glycol-8, 0.141% polyethylene glycol-32, 1% PEG-75 lanolin, 1.05% lauryl hydroxysulfobetaine, 2% betaine, 1% PEG-120 methyl glucose triisostearate, 0.235% sodium polyacrylate grafted starch, 0.175% modified corn starch, 18% glycerol, 0.18% ethylhexyl glycerol, 1% jojoba wax PEG-120 esters, 0.42% octaethylene glycol, 0.4975% aloe vera leaf juice, 0.2% carbomer, 0.4% champignon oil, 0.3% sweet orange extract, 0.05% grapefruit peel oil, 0.05% bergamot fruit oil, 0.05% citrus peel extract, 0.00125% potassium sorbate, 0.00575% sodium benzoate, 0.175% sodium chloride, 0.1% disodium EDTA, 0.1% balance sodium hydroxide and deionized water.
3. A process for preparing a make-up removal cleansing cream as claimed in claim 1 or claim 2, characterized in that: the preparation method comprises the following steps:
(1) Adding a multifunctional surfactant, a moisturizing emollient and part of deionized water into a water kettle, uniformly stirring, filtering, pumping into a main kettle, adding 1.0% of evaporated water, and stirring under vacuum to ensure no large caking, wherein the multifunctional surfactant is polyethylene glycol-8, polyethylene glycol-32, PEG-75 lanolin, lauryl hydroxysulfobetaine and betaine, and the moisturizing emollient is glycerol, ethylhexyl glycerol, huo Baba wax PEG-120 esters, caprylyl glycol, aloe vera leaf juice and carbomer;
(2) Heating by adjusting stirring speed, homogenizing after reaching the target temperature of 90-95 ℃, uncovering and observing to ensure that transparent particles are not present, adding an amino acid anionic surfactant, vacuum, keeping the temperature at not lower than 85 ℃ after the addition of the amino acid anionic surfactant is finished, keeping warm and stirring until the amino acid anionic surfactant is completely dissolved, and continuously adding a small amount of foam on the surface, wherein the amino acid anionic surfactant is sodium lauroyl glutamate;
(3) Weighing a cationic polymer, adding the rest deionized water, heating to 80-85 ℃, and uniformly stirring for standby, wherein the cationic polymer is polyquaternium-52;
(4) Sequentially adding various viscosity regulators and preservatives, adjusting stirring speed, stirring in vacuum, adding the dissolved cationic polymer in the step (3) into a main pot, and stirring until uniformity, wherein the viscosity regulators are PEG-120 methyl glucose triisostearate, sodium polyacrylate grafted starch and modified corn starch, the preservatives are potassium sorbate and sodium benzoate, and the cationic polymer is polyquaternium-52;
(5) Cooling, keeping vacuum, and adding fragrant components when the temperature is below 50deg.C, and continuously stirring, wherein the fragrant components are oleum Lavandula Angustifolia, fructus Citri sinensis extract, grape fruit peel oil, bergamot fruit oil, mandarin orange peel extract and lemon fruit peel oil;
(6) Continuously slowly cooling to paste, keeping vacuum, heating to 50-55deg.C, maintaining the temperature, stirring, scraping large blocks on stirring paddles until no caking is generated;
(7) And (3) adjusting the stirring speed, cooling to 41-42 ℃ for displaying, discharging cooling water of the emulsifying tank when the materials are in a uniform yogurt-like liquid state, and discharging the materials at the bottom of the pot.
4. A method of preparation according to claim 3, characterized in that: in the step (2), adding the amino acid anionic surfactant in multiple times, covering a pot cover after each addition, and vacuum adjusting and stirring to homogenize the mixture until the mixture does not have large caking, in the step (4), adding the dissolved cationic polymer in the step (3) into a main pot independently, wherein the amino acid anionic surfactant is sodium lauroyl glutamate and the cationic polymer is polyquaternium-52.
CN202410487470.9A 2024-04-23 Cleansing cream with moisturizing and skin care effects and preparation method thereof Active CN118078729B (en)

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Application Number Priority Date Filing Date Title
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CN118078729B true CN118078729B (en) 2024-07-16

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Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
"俊平橙净无忧氨基酸洁面慕斯（春夏限定）";杭州耕香生物科技有限公司;《国产非特殊用途化妆品备案平台》;20190303;1-10 *

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