CN118047658A - 生产卤化丙烷的方法 - Google Patents

生产卤化丙烷的方法 Download PDF

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Publication number
CN118047658A
CN118047658A CN202410185515.7A CN202410185515A CN118047658A CN 118047658 A CN118047658 A CN 118047658A CN 202410185515 A CN202410185515 A CN 202410185515A CN 118047658 A CN118047658 A CN 118047658A
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CN
China
Prior art keywords
reactor
slurry
iron
carbon tetrachloride
ethylene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202410185515.7A
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English (en)
Chinese (zh)
Inventor
J·L·道金斯
D·霍利斯
K·S·克雷默
B·考尔德伍德
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Occidental Chemical Corp
Original Assignee
Occidental Chemical Corp
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Filing date
Publication date
Application filed by Occidental Chemical Corp filed Critical Occidental Chemical Corp
Publication of CN118047658A publication Critical patent/CN118047658A/zh
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/266—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50—Mixing receptacles
    • B01F35/53—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components
    • B01F35/531—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom
    • B01F35/5312—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom with vertical baffles mounted on the walls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2204—Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00768—Baffles attached to the reactor wall vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN202410185515.7A 2016-07-26 2017-07-24 生产卤化丙烷的方法 Pending CN118047658A (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201662366674P 2016-07-26 2016-07-26
US62/366,674 2016-07-26
CN201780046570.6A CN109476568B (zh) 2016-07-26 2017-07-24 生产卤化丙烷的方法
PCT/US2017/043469 WO2018022488A1 (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201780046570.6A Division CN109476568B (zh) 2016-07-26 2017-07-24 生产卤化丙烷的方法

Publications (1)

Publication Number Publication Date
CN118047658A true CN118047658A (zh) 2024-05-17

Family

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Family Applications (3)

Application Number Title Priority Date Filing Date
CN202410185515.7A Pending CN118047658A (zh) 2016-07-26 2017-07-24 生产卤化丙烷的方法
CN201780046570.6A Active CN109476568B (zh) 2016-07-26 2017-07-24 生产卤化丙烷的方法
CN202210506937.0A Active CN114805014B (zh) 2016-07-26 2017-07-24 生产卤化丙烷的方法

Family Applications After (2)

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CN202210506937.0A Active CN114805014B (zh) 2016-07-26 2017-07-24 生产卤化丙烷的方法

Country Status (13)

Country Link
US (1) US10787404B2 (enExample)
EP (3) EP3795554B1 (enExample)
JP (3) JP7017555B2 (enExample)
KR (2) KR102706899B1 (enExample)
CN (3) CN118047658A (enExample)
CA (2) CA3203916C (enExample)
EA (2) EA202191351A3 (enExample)
ES (2) ES2998773T3 (enExample)
FI (1) FI3795554T3 (enExample)
MX (1) MX385668B (enExample)
PT (2) PT3490965T (enExample)
TW (3) TWI860085B (enExample)
WO (1) WO2018022488A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020146722A1 (en) 2019-01-10 2020-07-16 Occidental Chemical Corporation Photochlorination of partially-chlorinated chloromethanes to carbon tetrachloride
EP4031270B1 (en) * 2019-09-18 2026-04-08 Plastrac Inc. A granular material distributor

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US3349010A (en) * 1964-12-10 1967-10-24 Phillips Petroleum Co Method and apparatus for controlling polymer deposition in reboiler
JPS521756A (en) * 1975-06-24 1977-01-07 Sumikin Kozai Kogyo Kk Rotary vane device to mix substances having different specific graviti es
US4605802A (en) * 1982-04-01 1986-08-12 Halocarbon Products Corp. Production of 1,1,1,3-tetrachloropropane
US4535194A (en) 1983-07-06 1985-08-13 Monsanto Co. Process for producing 1,1,2,3-tetrachloropropene
EP0131561B1 (en) * 1983-07-06 1986-10-15 Monsanto Company Process for producing monoadducts of olefins and telogens reactive therewith
JPH0759605B2 (ja) * 1990-09-07 1995-06-28 三井造船株式会社 ポリマー中の触媒除去装置
CH686117A5 (fr) * 1993-07-08 1996-01-15 Biazzi Sa Appareillage de reaction gaz-liquide.
DE4435839A1 (de) * 1994-10-07 1996-04-11 Bayer Ag Schlammphasenreaktor und dessen Verwendung
US6313360B1 (en) 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
WO2005068407A1 (en) * 2004-01-07 2005-07-28 Conocophillips Company Systems and methods for catalyst/hydrocarbon product separation
US20040225166A1 (en) * 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US8071825B2 (en) 2006-01-03 2011-12-06 Honeywell International Inc. Method for producing fluorinated organic compounds
DK2231565T3 (da) * 2007-12-19 2014-05-26 Occidental Chem Co Fremgangsmåder til fremstilling af clorerede carbonhydrider
US8722946B2 (en) 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
US8835702B2 (en) 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
EP2548907A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
KR20140071457A (ko) 2011-09-30 2014-06-11 허니웰 인터내셔날 인코포레이티드 2,3,3,3-테트라플루오로프로펜의 제조 방법
US9381451B2 (en) * 2012-03-06 2016-07-05 GM Global Technology Operations LLC Quiescent zone fluid filter
JP6158032B2 (ja) 2012-10-17 2017-07-05 株式会社トクヤマ 反応ガスをリサイクルした塩素化プロパンの製造方法
US8907147B2 (en) * 2013-02-04 2014-12-09 Honeywell International Inc. Synthesis of 1,1,2,3-tetrachloropropene
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CA3226491C (en) * 2014-05-16 2026-04-07 Occidental Chemical Corporation Method for making 1,1,3,3-tetrachloropropene
CN204779412U (zh) * 2015-07-02 2015-11-18 江苏理文化工有限公司 一种制备四氯丙烷系统
CN105218299B (zh) * 2015-09-30 2020-03-31 巨化集团技术中心 一种用于四氯化碳和烯烃生产氯代烃的连续制备方法
CN105251318B (zh) * 2015-11-06 2017-05-24 铜陵有色金属集团股份有限公司铜冠冶化分公司 一种防止再沸器结晶堵塞的湿法有机胺脱硫解吸塔

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Publication number Publication date
CN109476568B (zh) 2022-08-30
TW202138338A (zh) 2021-10-16
TW201817698A (zh) 2018-05-16
JP2022024008A (ja) 2022-02-08
JP2023099154A (ja) 2023-07-11
CN114805014B (zh) 2024-05-03
US10787404B2 (en) 2020-09-29
EA202191351A3 (ru) 2021-11-30
MX2019001151A (es) 2019-12-16
EA201990382A1 (ru) 2019-06-28
PT3795554T (pt) 2024-10-29
EP3795554A1 (en) 2021-03-24
EA038726B1 (ru) 2021-10-11
EP3795554B1 (en) 2024-10-02
CN114805014A (zh) 2022-07-29
EP3490965A1 (en) 2019-06-05
KR20190059263A (ko) 2019-05-30
JP7274551B2 (ja) 2023-05-16
TWI816142B (zh) 2023-09-21
KR102634847B1 (ko) 2024-02-06
TWI860085B (zh) 2024-10-21
TWI734811B (zh) 2021-08-01
EP4530279A1 (en) 2025-04-02
CA3031793C (en) 2023-08-15
CA3031793A1 (en) 2018-02-01
EP3490965B1 (en) 2020-11-25
JP2019522013A (ja) 2019-08-08
EA202191351A2 (ru) 2021-08-31
ES2998773T3 (en) 2025-02-21
CA3203916A1 (en) 2018-02-01
JP7017555B2 (ja) 2022-02-08
CN109476568A (zh) 2019-03-15
MX385668B (es) 2025-03-18
US20190284118A1 (en) 2019-09-19
KR102706899B1 (ko) 2024-09-12
CA3203916C (en) 2024-01-23
TW202402720A (zh) 2024-01-16
PT3490965T (pt) 2021-01-29
ES2849561T3 (es) 2021-08-19
KR20230087618A (ko) 2023-06-16
JP7557570B2 (ja) 2024-09-27
FI3795554T3 (fi) 2024-11-21
WO2018022488A1 (en) 2018-02-01

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