CA3203916C - Methods for producing halogenated propanes - Google Patents

Methods for producing halogenated propanes Download PDF

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Publication number
CA3203916C
CA3203916C CA3203916A CA3203916A CA3203916C CA 3203916 C CA3203916 C CA 3203916C CA 3203916 A CA3203916 A CA 3203916A CA 3203916 A CA3203916 A CA 3203916A CA 3203916 C CA3203916 C CA 3203916C
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CA
Canada
Prior art keywords
reactor
slurry
still
zone
reaction mixture
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Active
Application number
CA3203916A
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English (en)
French (fr)
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CA3203916A1 (en
Inventor
John L. Dawkins
Darrell Hollis
Keith S. Kramer
Brian CALDERWOOD
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Occidental Chemical Corp
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Occidental Chemical Corp
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Publication of CA3203916A1 publication Critical patent/CA3203916A1/en
Application granted granted Critical
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/266—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50—Mixing receptacles
    • B01F35/53—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components
    • B01F35/531—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom
    • B01F35/5312—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom with vertical baffles mounted on the walls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2204—Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00768—Baffles attached to the reactor wall vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA3203916A 2016-07-26 2017-07-24 Methods for producing halogenated propanes Active CA3203916C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201662366674P 2016-07-26 2016-07-26
US62/366,674 2016-07-26
CA3031793A CA3031793C (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CA3031793A Division CA3031793C (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes

Publications (2)

Publication Number Publication Date
CA3203916A1 CA3203916A1 (en) 2018-02-01
CA3203916C true CA3203916C (en) 2024-01-23

Family

ID=59791114

Family Applications (2)

Application Number Title Priority Date Filing Date
CA3203916A Active CA3203916C (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes
CA3031793A Active CA3031793C (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes

Family Applications After (1)

Application Number Title Priority Date Filing Date
CA3031793A Active CA3031793C (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes

Country Status (13)

Country Link
US (1) US10787404B2 (enExample)
EP (3) EP3795554B1 (enExample)
JP (3) JP7017555B2 (enExample)
KR (2) KR102706899B1 (enExample)
CN (3) CN118047658A (enExample)
CA (2) CA3203916C (enExample)
EA (2) EA202191351A3 (enExample)
ES (2) ES2998773T3 (enExample)
FI (1) FI3795554T3 (enExample)
MX (1) MX385668B (enExample)
PT (2) PT3490965T (enExample)
TW (3) TWI860085B (enExample)
WO (1) WO2018022488A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020146722A1 (en) 2019-01-10 2020-07-16 Occidental Chemical Corporation Photochlorination of partially-chlorinated chloromethanes to carbon tetrachloride
EP4031270B1 (en) * 2019-09-18 2026-04-08 Plastrac Inc. A granular material distributor

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3349010A (en) * 1964-12-10 1967-10-24 Phillips Petroleum Co Method and apparatus for controlling polymer deposition in reboiler
JPS521756A (en) * 1975-06-24 1977-01-07 Sumikin Kozai Kogyo Kk Rotary vane device to mix substances having different specific graviti es
US4605802A (en) * 1982-04-01 1986-08-12 Halocarbon Products Corp. Production of 1,1,1,3-tetrachloropropane
US4535194A (en) 1983-07-06 1985-08-13 Monsanto Co. Process for producing 1,1,2,3-tetrachloropropene
EP0131561B1 (en) * 1983-07-06 1986-10-15 Monsanto Company Process for producing monoadducts of olefins and telogens reactive therewith
JPH0759605B2 (ja) * 1990-09-07 1995-06-28 三井造船株式会社 ポリマー中の触媒除去装置
CH686117A5 (fr) * 1993-07-08 1996-01-15 Biazzi Sa Appareillage de reaction gaz-liquide.
DE4435839A1 (de) * 1994-10-07 1996-04-11 Bayer Ag Schlammphasenreaktor und dessen Verwendung
US6313360B1 (en) 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
WO2005068407A1 (en) * 2004-01-07 2005-07-28 Conocophillips Company Systems and methods for catalyst/hydrocarbon product separation
US20040225166A1 (en) * 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US8071825B2 (en) 2006-01-03 2011-12-06 Honeywell International Inc. Method for producing fluorinated organic compounds
DK2231565T3 (da) * 2007-12-19 2014-05-26 Occidental Chem Co Fremgangsmåder til fremstilling af clorerede carbonhydrider
US8722946B2 (en) 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
US8835702B2 (en) 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
EP2548907A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
KR20140071457A (ko) 2011-09-30 2014-06-11 허니웰 인터내셔날 인코포레이티드 2,3,3,3-테트라플루오로프로펜의 제조 방법
US9381451B2 (en) * 2012-03-06 2016-07-05 GM Global Technology Operations LLC Quiescent zone fluid filter
JP6158032B2 (ja) 2012-10-17 2017-07-05 株式会社トクヤマ 反応ガスをリサイクルした塩素化プロパンの製造方法
US8907147B2 (en) * 2013-02-04 2014-12-09 Honeywell International Inc. Synthesis of 1,1,2,3-tetrachloropropene
CN104549070B (zh) * 2013-10-12 2016-08-24 中国石油化工股份有限公司 一种沸腾床反应器
CA3226491C (en) * 2014-05-16 2026-04-07 Occidental Chemical Corporation Method for making 1,1,3,3-tetrachloropropene
CN204779412U (zh) * 2015-07-02 2015-11-18 江苏理文化工有限公司 一种制备四氯丙烷系统
CN105218299B (zh) * 2015-09-30 2020-03-31 巨化集团技术中心 一种用于四氯化碳和烯烃生产氯代烃的连续制备方法
CN105251318B (zh) * 2015-11-06 2017-05-24 铜陵有色金属集团股份有限公司铜冠冶化分公司 一种防止再沸器结晶堵塞的湿法有机胺脱硫解吸塔

Also Published As

Publication number Publication date
CN109476568B (zh) 2022-08-30
TW202138338A (zh) 2021-10-16
TW201817698A (zh) 2018-05-16
JP2022024008A (ja) 2022-02-08
JP2023099154A (ja) 2023-07-11
CN114805014B (zh) 2024-05-03
US10787404B2 (en) 2020-09-29
EA202191351A3 (ru) 2021-11-30
MX2019001151A (es) 2019-12-16
EA201990382A1 (ru) 2019-06-28
PT3795554T (pt) 2024-10-29
EP3795554A1 (en) 2021-03-24
EA038726B1 (ru) 2021-10-11
EP3795554B1 (en) 2024-10-02
CN114805014A (zh) 2022-07-29
EP3490965A1 (en) 2019-06-05
KR20190059263A (ko) 2019-05-30
JP7274551B2 (ja) 2023-05-16
CN118047658A (zh) 2024-05-17
TWI816142B (zh) 2023-09-21
KR102634847B1 (ko) 2024-02-06
TWI860085B (zh) 2024-10-21
TWI734811B (zh) 2021-08-01
EP4530279A1 (en) 2025-04-02
CA3031793C (en) 2023-08-15
CA3031793A1 (en) 2018-02-01
EP3490965B1 (en) 2020-11-25
JP2019522013A (ja) 2019-08-08
EA202191351A2 (ru) 2021-08-31
ES2998773T3 (en) 2025-02-21
CA3203916A1 (en) 2018-02-01
JP7017555B2 (ja) 2022-02-08
CN109476568A (zh) 2019-03-15
MX385668B (es) 2025-03-18
US20190284118A1 (en) 2019-09-19
KR102706899B1 (ko) 2024-09-12
TW202402720A (zh) 2024-01-16
PT3490965T (pt) 2021-01-29
ES2849561T3 (es) 2021-08-19
KR20230087618A (ko) 2023-06-16
JP7557570B2 (ja) 2024-09-27
FI3795554T3 (fi) 2024-11-21
WO2018022488A1 (en) 2018-02-01

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