EA201990382A1 - Способы получения галогенированных пропанов - Google Patents

Способы получения галогенированных пропанов

Info

Publication number
EA201990382A1
EA201990382A1 EA201990382A EA201990382A EA201990382A1 EA 201990382 A1 EA201990382 A1 EA 201990382A1 EA 201990382 A EA201990382 A EA 201990382A EA 201990382 A EA201990382 A EA 201990382A EA 201990382 A1 EA201990382 A1 EA 201990382A1
Authority
EA
Eurasian Patent Office
Prior art keywords
reaction mixture
methods
head space
propanes
obtaining halogenated
Prior art date
Application number
EA201990382A
Other languages
English (en)
Other versions
EA038726B1 (ru
Inventor
Джон Л. Докинс
Даррелл Холлис
Кит С. Крамер
Брайан Калдервуд
Original Assignee
Оксидентал Кемикал Корпорейшн
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Оксидентал Кемикал Корпорейшн filed Critical Оксидентал Кемикал Корпорейшн
Publication of EA201990382A1 publication Critical patent/EA201990382A1/ru
Publication of EA038726B1 publication Critical patent/EA038726B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/266—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50—Mixing receptacles
    • B01F35/53—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components
    • B01F35/531—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom
    • B01F35/5312—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom with vertical baffles mounted on the walls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2204—Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00768—Baffles attached to the reactor wall vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Способ получения хлорированных пропанов по реакции четыреххлористого углерода с этиленом в емкостном реакторе, который включает жидкую реакционную смесь и головное пространство над реакционной смесью, при этом газообразный этилен диффундирует из жидкой реакционной смеси в головное пространство при перемешивании реакционной смеси, причем усовершенствование заключается в переносе этилена внутри головного пространства обратно в реакционную смесь через канал внутри перемешивающего устройства, которое перемешивает реакционную смесь.
EA201990382A 2016-07-26 2017-07-24 Способы получения галогенированных пропанов EA038726B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201662366674P 2016-07-26 2016-07-26
PCT/US2017/043469 WO2018022488A1 (en) 2016-07-26 2017-07-24 Methods for producing halogenated propanes

Publications (2)

Publication Number Publication Date
EA201990382A1 true EA201990382A1 (ru) 2019-06-28
EA038726B1 EA038726B1 (ru) 2021-10-11

Family

ID=59791114

Family Applications (2)

Application Number Title Priority Date Filing Date
EA201990382A EA038726B1 (ru) 2016-07-26 2017-07-24 Способы получения галогенированных пропанов
EA202191351A EA202191351A3 (ru) 2016-07-26 2017-07-24 Способы получения галогенированных пропанов

Family Applications After (1)

Application Number Title Priority Date Filing Date
EA202191351A EA202191351A3 (ru) 2016-07-26 2017-07-24 Способы получения галогенированных пропанов

Country Status (12)

Country Link
US (1) US10787404B2 (ru)
EP (2) EP3490965B1 (ru)
JP (3) JP7017555B2 (ru)
KR (2) KR102634847B1 (ru)
CN (3) CN118047658A (ru)
CA (2) CA3031793C (ru)
EA (2) EA038726B1 (ru)
ES (1) ES2849561T3 (ru)
MX (1) MX2019001151A (ru)
PT (1) PT3490965T (ru)
TW (2) TWI816142B (ru)
WO (1) WO2018022488A1 (ru)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3908564A4 (en) 2019-01-10 2022-10-26 Occidental Chemical Corporation PHOTOCHLORINATION OF PARTIALLY CHLORINED CHLOROMETHANE TO CARBON TETRACHLORIDE
EP4031270A4 (en) * 2019-09-18 2023-10-18 Plastrac Inc. GRANULAR MEASUREMENT SYSTEM

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3349010A (en) * 1964-12-10 1967-10-24 Phillips Petroleum Co Method and apparatus for controlling polymer deposition in reboiler
US4605802A (en) * 1982-04-01 1986-08-12 Halocarbon Products Corp. Production of 1,1,1,3-tetrachloropropane
DE3460965D1 (en) * 1983-07-06 1986-11-20 Monsanto Co Process for producing monoadducts of olefins and telogens reactive therewith
US4535194A (en) * 1983-07-06 1985-08-13 Monsanto Co. Process for producing 1,1,2,3-tetrachloropropene
JPH0759605B2 (ja) * 1990-09-07 1995-06-28 三井造船株式会社 ポリマー中の触媒除去装置
US6313360B1 (en) 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
US20040225166A1 (en) 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US8071825B2 (en) 2006-01-03 2011-12-06 Honeywell International Inc. Method for producing fluorinated organic compounds
EP3000802B1 (en) * 2007-12-19 2018-07-11 Occidental Chemical Corporation Methods of making clorinated hydrocarbons
US8835702B2 (en) 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
US8722946B2 (en) * 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
EP2548907A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
JP2014530214A (ja) 2011-09-30 2014-11-17 ハネウェル・インターナショナル・インコーポレーテッド ２，３，３，３−テトラフルオロプロペンの製造方法
US9381451B2 (en) * 2012-03-06 2016-07-05 GM Global Technology Operations LLC Quiescent zone fluid filter
JP6158032B2 (ja) 2012-10-17 2017-07-05 株式会社トクヤマ 反応ガスをリサイクルした塩素化プロパンの製造方法
US8907147B2 (en) * 2013-02-04 2014-12-09 Honeywell International Inc. Synthesis of 1,1,2,3-tetrachloropropene
CA3226491A1 (en) * 2014-05-16 2015-11-19 Occidental Chemical Corporation Method for making 1,1,3,3-tetrachloropropene
CN204779412U (zh) * 2015-07-02 2015-11-18 江苏理文化工有限公司 一种制备四氯丙烷系统
CN105218299B (zh) * 2015-09-30 2020-03-31 巨化集团技术中心 一种用于四氯化碳和烯烃生产氯代烃的连续制备方法
CN105251318B (zh) * 2015-11-06 2017-05-24 铜陵有色金属集团股份有限公司铜冠冶化分公司 一种防止再沸器结晶堵塞的湿法有机胺脱硫解吸塔

Also Published As

Publication number Publication date
KR102706899B1 (ko) 2024-09-12
MX2019001151A (es) 2019-12-16
TWI734811B (zh) 2021-08-01
KR20230087618A (ko) 2023-06-16
US20190284118A1 (en) 2019-09-19
JP2019522013A (ja) 2019-08-08
EA038726B1 (ru) 2021-10-11
PT3490965T (pt) 2021-01-29
KR102634847B1 (ko) 2024-02-06
CN114805014B (zh) 2024-05-03
EA202191351A2 (ru) 2021-08-31
TWI816142B (zh) 2023-09-21
CA3031793A1 (en) 2018-02-01
WO2018022488A1 (en) 2018-02-01
EA202191351A3 (ru) 2021-11-30
JP2022024008A (ja) 2022-02-08
TW202138338A (zh) 2021-10-16
TW202402720A (zh) 2024-01-16
ES2849561T3 (es) 2021-08-19
JP7017555B2 (ja) 2022-02-08
EP3795554A1 (en) 2021-03-24
TW201817698A (zh) 2018-05-16
CN109476568B (zh) 2022-08-30
EP3795554B1 (en) 2024-10-02
JP7557570B2 (ja) 2024-09-27
EP3490965A1 (en) 2019-06-05
EP3490965B1 (en) 2020-11-25
CA3031793C (en) 2023-08-15
US10787404B2 (en) 2020-09-29
JP2023099154A (ja) 2023-07-11
CA3203916A1 (en) 2018-02-01
CN118047658A (zh) 2024-05-17
JP7274551B2 (ja) 2023-05-16
KR20190059263A (ko) 2019-05-30
CN114805014A (zh) 2022-07-29
CN109476568A (zh) 2019-03-15
CA3203916C (en) 2024-01-23

Similar Documents

Publication Publication Date Title
HUE056900T2 (hu) Korszerû architektúrájú reaktor CO2, CO és más kémiai vegyületek elektrokémiai reakciójához
MX2016011241A (es) Reformado con vapor.
EA201990382A1 (ru) Способы получения галогенированных пропанов
MX2017004848A (es) Proceso.
MX2018014050A (es) Precursor de dioxoxido de cloro y metodos de uso del mismo.
SA517382172B1 (ar) مفاعل قابل للغمر لإنتاج مبيد حيوي وطريقة
EA201891221A1 (ru) Способ эпоксидирования олефина
EA201791300A1 (ru) Флюидные системы, содержащие канал инкубации, включающие в себя флюидные системы, образованные литьевым формованием
MX2020004182A (es) Metodo y sistema para formar y para hacer reaccionar cataliticamente una mezcla de reactivos - modalidad de reactor.
WO2019098834A8 (en) An apparatus and methods for dispensing and foaming of a product
EA201790022A1 (ru) Реакционная камера для химического реактора и выполненный на ее основе химический реактор
UA117138C2 (uk) Пристрій та спосіб тепломасообміну між газом і рідиною
IN2014DN10907A (ru)
BR112015020774A2 (pt) método de refino de 1,5-diaminopentano e 1,5-diaminopentano
MX2017007777A (es) Metodo para realizar las paredes internas de reactores cataliticos.
EA201891625A1 (ru) Способ эпоксидирования олефина
PH12016501889A1 (en) Process and device for producing fuel hydrocarbon oil
EA201691757A1 (ru) Способ получения синтез-газа
PH12019550215A1 (en) Device for generating hydrogen gas
PE20161192A1 (es) Sintesis fischer-tropsch
WO2015018962A3 (es) Quemador para un sistema de reformado de hidrocarburos y alcoholes, sistema de reformado de hidrocarburos y alcoholes que lo comprende y procedimiento asociado
MX344135B (es) Método y aparato para homogeneizar y estabilizar residuo que contiene fierro.
MX2017006952A (es) Metodo para producir peroxido de lauroilo en polvo.
EA201591248A1 (ru) Устройство для реакции синтеза углеводородов
MX2016000638A (es) Reactor para preparar cianuro de hidrogeno mediante el proceso de andrussow, equipo que comprende el reactor y proceso que usa tal equipo.