TWI860085B - 製造鹵化丙烷之方法 - Google Patents

製造鹵化丙烷之方法 Download PDF

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Publication number
TWI860085B
TWI860085B TW112135146A TW112135146A TWI860085B TW I860085 B TWI860085 B TW I860085B TW 112135146 A TW112135146 A TW 112135146A TW 112135146 A TW112135146 A TW 112135146A TW I860085 B TWI860085 B TW I860085B
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Taiwan
Prior art keywords
reactor
reaction mixture
tank reactor
zone
catalyst
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TW112135146A
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English (en)
Chinese (zh)
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TW202402720A (zh
Inventor
約翰 道金斯
戴瑞爾 荷立斯
凱斯 克拉默
布萊恩 卡得伍
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美商西方化學公司
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Publication of TW202402720A publication Critical patent/TW202402720A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/266—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of hydrocarbons and halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50—Mixing receptacles
    • B01F35/53—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components
    • B01F35/531—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom
    • B01F35/5312—Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom with vertical baffles mounted on the walls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2204—Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00768—Baffles attached to the reactor wall vertical

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
TW112135146A 2016-07-26 2017-07-24 製造鹵化丙烷之方法 TWI860085B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201662366674P 2016-07-26 2016-07-26
US62/366,674 2016-07-26

Publications (2)

Publication Number Publication Date
TW202402720A TW202402720A (zh) 2024-01-16
TWI860085B true TWI860085B (zh) 2024-10-21

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TW112135146A TWI860085B (zh) 2016-07-26 2017-07-24 製造鹵化丙烷之方法
TW110122625A TWI816142B (zh) 2016-07-26 2017-07-24 製造鹵化丙烷之方法
TW106124766A TWI734811B (zh) 2016-07-26 2017-07-24 製造鹵化丙烷之方法

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TW106124766A TWI734811B (zh) 2016-07-26 2017-07-24 製造鹵化丙烷之方法

Country Status (13)

Country Link
US (1) US10787404B2 (enExample)
EP (3) EP4530279A1 (enExample)
JP (3) JP7017555B2 (enExample)
KR (2) KR102634847B1 (enExample)
CN (3) CN109476568B (enExample)
CA (2) CA3203916C (enExample)
EA (2) EA202191351A3 (enExample)
ES (2) ES2849561T3 (enExample)
FI (1) FI3795554T3 (enExample)
MX (1) MX385668B (enExample)
PT (2) PT3795554T (enExample)
TW (3) TWI860085B (enExample)
WO (1) WO2018022488A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020146722A1 (en) 2019-01-10 2020-07-16 Occidental Chemical Corporation Photochlorination of partially-chlorinated chloromethanes to carbon tetrachloride
US10994945B2 (en) * 2019-09-18 2021-05-04 Plastrac Inc. Granular metering system

Citations (3)

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US20040171702A1 (en) * 2001-12-28 2004-09-02 Conocophillips Company Systems and methods for catalyst/hydrocarbon product separation
TW200936538A (en) * 2007-12-19 2009-09-01 Occidental Chem Co Methods of making chlorinated hydrocarbons
CN104549070A (zh) * 2013-10-12 2015-04-29 中国石油化工股份有限公司 一种沸腾床反应器

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US4535194A (en) * 1983-07-06 1985-08-13 Monsanto Co. Process for producing 1,1,2,3-tetrachloropropene
ATE22877T1 (de) * 1983-07-06 1986-11-15 Monsanto Co Verfahren zur herstellung von monoaddukten von olefinen und damit reagierfaehigen telogenen.
JPH0759605B2 (ja) * 1990-09-07 1995-06-28 三井造船株式会社 ポリマー中の触媒除去装置
CH686117A5 (fr) * 1993-07-08 1996-01-15 Biazzi Sa Appareillage de reaction gaz-liquide.
DE4435839A1 (de) * 1994-10-07 1996-04-11 Bayer Ag Schlammphasenreaktor und dessen Verwendung
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US20040225166A1 (en) * 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US8071825B2 (en) 2006-01-03 2011-12-06 Honeywell International Inc. Method for producing fluorinated organic compounds
US8835702B2 (en) 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
US8722946B2 (en) * 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
EP2548907A1 (de) 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
WO2013049744A2 (en) 2011-09-30 2013-04-04 Honeywell International Inc. Process for producing 2,3,3,3-tetrafluoropropene
US9381451B2 (en) * 2012-03-06 2016-07-05 GM Global Technology Operations LLC Quiescent zone fluid filter
JP6158032B2 (ja) 2012-10-17 2017-07-05 株式会社トクヤマ 反応ガスをリサイクルした塩素化プロパンの製造方法
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SI3412648T1 (sl) * 2014-05-16 2020-08-31 Occidental Chemical Corporation Postopek za izdelavo 1,1,3,3-tetrakloropropena
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CN105218299B (zh) * 2015-09-30 2020-03-31 巨化集团技术中心 一种用于四氯化碳和烯烃生产氯代烃的连续制备方法
CN105251318B (zh) * 2015-11-06 2017-05-24 铜陵有色金属集团股份有限公司铜冠冶化分公司 一种防止再沸器结晶堵塞的湿法有机胺脱硫解吸塔

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US20040171702A1 (en) * 2001-12-28 2004-09-02 Conocophillips Company Systems and methods for catalyst/hydrocarbon product separation
TW200936538A (en) * 2007-12-19 2009-09-01 Occidental Chem Co Methods of making chlorinated hydrocarbons
CN104549070A (zh) * 2013-10-12 2015-04-29 中国石油化工股份有限公司 一种沸腾床反应器

Also Published As

Publication number Publication date
CN109476568A (zh) 2019-03-15
CA3031793C (en) 2023-08-15
EA038726B1 (ru) 2021-10-11
EA202191351A2 (ru) 2021-08-31
MX2019001151A (es) 2019-12-16
TW201817698A (zh) 2018-05-16
CN114805014B (zh) 2024-05-03
PT3795554T (pt) 2024-10-29
US20190284118A1 (en) 2019-09-19
CA3031793A1 (en) 2018-02-01
EP3490965A1 (en) 2019-06-05
JP7557570B2 (ja) 2024-09-27
KR102634847B1 (ko) 2024-02-06
EP4530279A1 (en) 2025-04-02
ES2849561T3 (es) 2021-08-19
EA201990382A1 (ru) 2019-06-28
US10787404B2 (en) 2020-09-29
CA3203916A1 (en) 2018-02-01
JP2019522013A (ja) 2019-08-08
CA3203916C (en) 2024-01-23
TWI816142B (zh) 2023-09-21
CN114805014A (zh) 2022-07-29
CN118047658A (zh) 2024-05-17
WO2018022488A1 (en) 2018-02-01
MX385668B (es) 2025-03-18
KR102706899B1 (ko) 2024-09-12
JP2023099154A (ja) 2023-07-11
CN109476568B (zh) 2022-08-30
KR20190059263A (ko) 2019-05-30
EP3795554A1 (en) 2021-03-24
ES2998773T3 (en) 2025-02-21
JP7274551B2 (ja) 2023-05-16
EP3795554B1 (en) 2024-10-02
PT3490965T (pt) 2021-01-29
KR20230087618A (ko) 2023-06-16
EA202191351A3 (ru) 2021-11-30
JP2022024008A (ja) 2022-02-08
TW202402720A (zh) 2024-01-16
TW202138338A (zh) 2021-10-16
TWI734811B (zh) 2021-08-01
EP3490965B1 (en) 2020-11-25
JP7017555B2 (ja) 2022-02-08
FI3795554T3 (fi) 2024-11-21

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