CN118001190A - Hair mask with repairing and softening effects and preparation method thereof - Google Patents

Hair mask with repairing and softening effects and preparation method thereof Download PDF

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Publication number
CN118001190A
CN118001190A CN202410219499.9A CN202410219499A CN118001190A CN 118001190 A CN118001190 A CN 118001190A CN 202410219499 A CN202410219499 A CN 202410219499A CN 118001190 A CN118001190 A CN 118001190A
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hair
parts
repairing
softening
mask
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林文东
周家远
黎江玲
李惠珠
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Guxin Zhongshan New Materials Technology Co ltd
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Guxin Zhongshan New Materials Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • A61K8/416Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/463Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/896Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate
    • A61K8/898Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate containing nitrogen, e.g. amodimethicone, trimethyl silyl amodimethicone or dimethicone propyl PG-betaine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to a hair mask with repairing and softening effects and a preparation method thereof, wherein the components of the hair mask with repairing and softening effects comprise a humectant, an emulsifying agent, a hair conditioner, a hair care agent, a thickening agent and a solvent; the hair care agent is a combination of wheat amino acid and cocoa butter. The hair film product can improve the glossiness and softness of hair, enable the hair to be smooth, improve the frizzy feel of the hair, and be fresh and not greasy, and has long effect duration.

Description

Hair mask with repairing and softening effects and preparation method thereof
Technical Field
The invention belongs to the technical field of daily cosmetics, and particularly relates to a hair mask with repairing and softening effects and a preparation method thereof.
Background
Based on the current pursuit of people for beauty, the health problem of hair is also becoming more important. No matter the damage to the hair caused by the environment and the damage to the hair caused by physical hairdressing, the problems of frizziness, bifurcation, knotting and the like are caused to the hair, so that more and more people can choose to use the hair mask to nourish the hair after washing the hair, and the hair is enabled to reappear vitality.
CN106726753a discloses a hair mask and a preparation method thereof. The hair mask provided by the invention comprises the following components in percentage by weight: 1-5% of betaine, 10-20% of behenyl trimethyl ammonium chloride, 1-5% of polydimethylsiloxane, 1-3% of menthol, 10-15% of humectant, 15-25% of nursing agent, 1-5% of gambogin, 1-3% of patchouli alcohol, 0.1-0.5% of EDTA-disodium, 0.1-0.5% of citric acid, 0.1-0.5% of methylparaben, 0.1-0.5% of essence, 1-5% of cetyl hydroxyethyl cellulose and 12-58.6% of water. The hair mask provided by the invention not only can repair damaged hair quality and strengthen hair toughness, but also can moisten scalp hair, relieve itching and remove dandruff. Meanwhile, the hair mask is fresh and comfortable, mild to skin and free of stimulation.
CN114569497a discloses a healthy nourishing hair mask, which comprises the following raw materials in percentage by weight: 78 to 90 percent of alcohol compound, 0.5 to 2 percent of grease compound, 0.5 to 1.5 percent of silicone oil, 0.2 to 10 percent of cationic emulsifier and the balance of water. The application adopts specific cationic emulsifier, alcohol compound and grease for proportioning, so that the prepared hair film has transparent flowing texture at normal temperature, can be converted into cream texture in the using process, and deposits the cationic hair conditioner in the hair care component on the hair in the process, thereby reducing the residue on the scalp, reducing the irritation and improving the repairing effect.
However, the hair mask in the prior art has insufficient hair tail repairing effect after use, so the softening effect is not good, and therefore, development of a hair mask product which can enable hair to be soft and smooth and not frizzy after use and has long effect retention time has important significance.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide the hair mask with the repairing and softening effects and the preparation method thereof.
In order to achieve the aim of the invention, the invention adopts the following technical scheme:
in a first aspect, the present invention provides a hair mask having a restoration and softening effect, wherein the components of the hair mask having the restoration and softening effect include a humectant, an emulsifier, a hair conditioner, a hair care agent, a thickener, and a solvent;
the hair care agent is a combination of wheat amino acid and cocoa butter.
The hair conditioner in the hair mask can link and fill damaged hair scales, so that the hair conditioner is more fresh and cool after being used and has higher glossiness; the hair care agent has the advantages that the protective film is formed on the surface of the hair, the hair care agent has high moisture degree on the hair, the hair can be maintained, the softening, repairing and brightening effects of the product can be further improved, the hair is not easy to dry, softer and more beautiful due to the cooperation of the humectant, and the components used by the hair care agent are fresh and not greasy, so that the hair care agent can bring more pleasure to consumers.
Preferably, the components of the hair mask with repairing and softening effects comprise, by weight, 0.1-10 parts of humectant, 1-40 parts of emulsifier, 1-60 parts of hair conditioner, 0.1-20 parts of hair care agent, 0.5-10 parts of thickener and 50-100 parts of solvent.
In the hair mask with the repairing and softening effects, the addition amount of the humectant can be 0.5 part, 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts or 9 parts and the like;
The addition amount of the emulsifier can be 2 parts, 5 parts, 8 parts, 10 parts, 12 parts, 15 parts, 18 parts, 20 parts, 22 parts, 25 parts, 28 parts, 30 parts, 32 parts, 35 parts or 38 parts, etc.;
The hair conditioner may be added in an amount of 2 parts, 5 parts, 8 parts, 10 parts, 15 parts, 20 parts, 25 parts, 30 parts, 35 parts, 40 parts, 45 parts, 50 parts, 55 parts, or the like;
The hair care agent may be added in an amount of 0.5 parts, 0.8 parts, 1 part, 3 parts, 5 parts, 7 parts, 9 parts, 10 parts, 13 parts, 15 parts, 17 parts, 19 parts, or the like;
The addition amount of the thickener may be 0.8 part, 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or the like;
The solvent may be added in an amount of 55 parts, 60 parts, 65 parts, 70 parts, 75 parts, 80 parts, 85 parts, 90 parts, 95 parts, or the like.
Preferably, the components of the hair mask with repairing and softening effects comprise, by weight, 1-8 parts of humectant, 5-35 parts of emulsifier, 10-50 parts of hair conditioner, 1-15 parts of hair care agent, 1-8 parts of thickener and 50-100 parts of solvent.
Preferably, the components of the hair mask with repairing and softening effects comprise, by weight, 2-6 parts of humectant, 10-30 parts of emulsifier, 15-45 parts of hair conditioner, 5-12 parts of hair care agent, 1-5 parts of thickener and 50-100 parts of solvent.
Preferably, the mass ratio of the wheat amino acid to the cocoa butter is 1 (0.1-2), for example, 1:0.2, 1:0.5, 1:0.6, 1:0.8, 1:1, 1:1.1, 1:1.3, 1:1.5, 1:1.7, 1:1.9, etc.
As a preferable technical scheme of the invention, the wheat amino acid and the large flower cocoa resin can better condition hair after being matched with each other in the proportion, nourish hair roots, benefit hair maintenance, and further better care hair, so that the glossiness of hair is higher and the softening effect is better.
Preferably, the emulsifier comprises any one or a combination of at least two of cetyl alcohol, stearyl alcohol, PEG/PPG-19/19 polymethylsiloxane, or cetylstearyl alcohol.
Preferably, the emulsifier comprises a combination of cetyl alcohol, stearyl alcohol, PEG/PPG-19/19 polymethylsiloxane, and cetylstearyl alcohol;
preferably, the mass ratio of the cetyl alcohol, the stearyl alcohol, the PEG/PPG-19/19 polymethylsiloxane and the cetylstearyl alcohol is (1-3): 1-2): 0.5-1.5): 2-4.
In the invention, the emulsifier adopts the combination of cetyl alcohol, stearyl alcohol, PEG/PPG-19/19 polymethylsiloxane and cetylstearyl alcohol, which not only can play a role in system solubilization and ensure that the product has better uniformity, but also can adjust the viscosity of the product and ensure that the product is more fresh and not greasy after being used.
Preferably, the humectant comprises sodium polyglutamate.
Preferably, the thickener comprises hydroxyethyl cellulose and/or methyl cellulose.
Preferably, the hair conditioning agent comprises any one or a combination of at least two of amino terminal polydimethylsiloxane, cetyltrimethylammonium chloride, ethylhexyl glycerol, cyclopentadimethicone or behenyl trimethylammonium methyl sulfate.
Preferably, the hair conditioning agent is a combination of amino terminal polydimethylsiloxane, cetyltrimethylammonium chloride, ethylhexyl glycerol, cyclopentadimethicone, and behenyl trimethylammonium methyl sulfate.
The ammonia-end polydimethylsiloxane, cetyltrimethylammonium chloride, ethylhexyl glycerol, cyclopentadimethicone and behenyl trimethylammonium methylsulfate are matched for use, so that the hair can be more effectively smoothed, split and damaged, the hair can be healthier and glossy, the five are matched in a synergistic way, the excellent conditioning performance is realized, the hair is shiny, elegant, easy to comb and smooth, and the hair can be healthier and glossy.
Preferably, the mass ratio of the ammonia end polydimethylsiloxane, the cetyltrimethylammonium chloride, the ethylhexyl glycerol, the cyclopentadimethicone and the beyltrimethylammonium methyl sulfate is (1-4): 1-2): 0.1-1.5): 1-2): 0.1-1.8.
Wherein the first "1-4" may be 1.2, 1.5, 1.8, 2, 2.2, 2.5, 2.8, 3, 3.2, 3.5, or 3.8, etc.;
The first "1-2" may be 1.2, 1.3, 1.4, 1.5, 1.6, 1.7, 1.8, 1.9, etc.;
"0.1-1.5" may be 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1, 1.1, 1.2, 1.3, 1.4, etc.;
The second "1-2" may be 1.2, 1.3, 1.4, 1.5, 1.6, 1.7, 1.8, 1.9, etc.;
"0.1-1.8" may be 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1, 1.1, 1.2, 1.3, 1.4, 1.5, 1.6, 1.7, etc.
Preferably, the solvent comprises any one or a combination of at least two of deionized water, ethanol or isohexadecane.
Preferably, the components of the hair mask with repairing and softening effects further comprise any one or a combination of at least two of preservative, aromatic or pH regulator.
Preferably, the preservative comprises phenoxyethanol.
Preferably, the fragrance comprises a perfume.
Preferably, the pH adjuster comprises acetic acid and/or sodium hydroxide.
In a second aspect, the present invention provides a method for preparing a hair mask with repairing and softening effects according to the first aspect, wherein the method comprises homogenizing a humectant, an emulsifying agent, a hair conditioning agent, a hair care agent and a thickening agent in a solvent to obtain the hair mask with repairing and softening effects.
Preferably, the preparation method comprises the following steps:
(1) Heating deionized water, adding humectant, thickener and isododecane, mixing and homogenizing;
(2) Cooling, adding hair conditioner, emulsifier and ethanol, mixing, and homogenizing;
(3) Continuously cooling, adding a hair care agent, mixing and homogenizing, and standing to obtain the hair mask with repairing and softening effects.
Preferably, the temperature of step (1) is raised to 80-90 ℃, for example, 81 ℃, 83 ℃, 85 ℃, 87 ℃, 89 ℃ or the like.
Preferably, the temperature of the step (2) is reduced to 60-70 ℃, for example 61 ℃, 63 ℃, 65 ℃, 67 ℃, 69 ℃ or the like.
Preferably, the temperature of the step (3) is reduced to 35-45 ℃, for example, 36 ℃, 38 ℃, 40 ℃, 42 ℃, 44 ℃ or the like.
Preferably, step (3) further comprises adding any one or a combination of at least two of a preservative, a fragrance, or a pH adjuster.
Preferably, the mixing in the step (3) is performed in a stirring manner, and the stirring time is 5-20min, for example, 6min, 8min, 10min, 12min, 15min, 17min or 19min, etc.
Preferably, the time of standing in the step (3) is 1-2h, for example, 1.1h, 1.3h, 1.5h, 1.7h or 1.9h, etc.
Other specific point values in the numerical ranges are selectable, and will not be described in detail herein.
Compared with the prior art, the invention has the following beneficial effects:
(1) The hair conditioner in the hair mask can link and fill damaged hair scales, so that the hair conditioner is more fresh and cool after being used and has higher glossiness; the hair care agent has the advantages that the protective film is formed on the surface of the hair, the hair care agent has high moisture degree on the hair, the hair can be maintained, the softening, repairing and brightening effects of the product can be further improved, the hair is not easy to dry, softer and more beautiful due to the cooperation of the humectant, and the components used by the hair care agent are fresh and not greasy, so that the hair care agent can bring more pleasure to consumers.
(2) The preparation method of the hair mask with the repairing and softening effects has the advantages of simple operation steps, low cost and easy industrialized mass production.
Detailed Description
In order to further describe the technical means adopted by the present invention and the effects thereof, the following describes the technical scheme of the present invention in combination with the preferred embodiments of the present invention, but the present invention is not limited to the scope of the embodiments.
The following examples and comparative examples relate to the following partial materials and brand information:
the remaining materials can be used as long as they are purchased from a regular dealer.
Examples 1 to 3
The formulation and the dosage of the hair mask with the repairing and softening effects are shown in table 1, and the dosage units of all components in the table are parts;
TABLE 1
The preparation method of the hair mask with the repairing and softening effects comprises the following steps:
(1) Heating deionized water to 85 ℃, adding a humectant, a thickener and isododecane, and mixing and homogenizing for 5min at 600 rpm;
(2) Cooling to 65deg.C, adding hair conditioner, emulsifier and ethanol, mixing at 800rpm, homogenizing for 10min;
(3) Continuously cooling to 40 ℃, then adding a hair care agent, a preservative and a fragrance, mixing and homogenizing for 10min at 800rpm, then adding a pH regulator to adjust the pH of the system to 7.0+/-0.5, and standing for 2h to obtain the hair mask with repairing and softening effects.
Example 4
This example provides a hair mask with a repair and softening effect which differs from example 1 only in that the formulation does not include an amino-terminal polydimethylsiloxane, the reduction of which is proportionally distributed to cetyltrimethylammonium chloride, ethylhexyl glycerol, cyclopenta-dimethicone and behenyl trimethylammonium methyl sulfate, and the rest of the components and the addition amounts are the same as in example 1, and the preparation method is referred to in example 1.
Example 5
This example provides a hair mask with a restoration and softening effect, which differs from example 1 only in that cetyltrimethylammonium chloride is not included in the formulation, the reduction amount thereof is distributed into the amino-terminal polydimethylsiloxane, the ethylhexyl glycerol, the cyclopenta-dimethicone and the behenyl trimethylammonium methyl sulfate in parts ratio, and the rest components and the addition amount are the same as example 1, and the preparation method is referred to example 1.
Example 6
This example provides a hair mask with a repair and softening effect, which differs from example 1 only in that the formulation does not include ethylhexyl glycerin, and the reduction amount of the ethylhexyl glycerin is distributed to the amino-terminal polydimethylsiloxane, cetyltrimethylammonium chloride, cyclopenta-dimethicone and behenyl trimethylammonium methyl sulfate according to the part ratio, and the rest of the components and the addition amount are the same as those of example 1, and the preparation method is referred to example 1.
Example 7
This example provides a hair mask with a repair and softening effect which differs from example 1 only in that the formulation does not include cyclopentadimethicone, the reduction of which is distributed in parts by weight to the amino terminal dimethicone, cetyltrimethylammonium chloride, ethylhexyl glycerol and behenyl trimethylammonium methyl sulfate, the remaining components and the addition amounts are the same as example 1, and the preparation method is referred to example 1.
Example 8
This example provides a hair mask with a repair and softening effect which differs from example 1 only in that the formulation does not include behenyl trimethylammonium methylsulfate, the reduced amount of which is distributed in parts by weight into the amino-terminal polydimethylsiloxane, cetyltrimethylammonium chloride, ethylhexyl glycerol and cyclopentadimethicone, and the rest of the components and the added amounts are the same as in example 1, and the preparation method is referred to in example 1.
Example 9
This example provides a hair mask with a restoration and softening effect which differs from example 1 only in that no cetyl alcohol is included in the formulation, the reduced amounts thereof being distributed in parts ratio to stearyl alcohol, PEG/PPG-19/19 polymethylsiloxane and cetylstearyl alcohol, the remaining components and amounts added being in accordance with example 1, the preparation being as described in reference to example 1.
Example 10
This example provides a hair mask with a restoration and softening effect which differs from example 1 only in that stearyl alcohol is not included in the formulation, the reduced amounts thereof are distributed in parts ratio to cetyl alcohol, PEG/PPG-19/19 polymethylsiloxane and cetylstearyl alcohol, and the remaining components and added amounts are the same as in example 1, the preparation method being referred to in example 1.
Example 11
This example provides a hair mask with a restoration and softening effect which differs from example 1 only in that the formulation does not include PEG/PPG-19/19 polymethylsiloxane, the reduced amounts of which are distributed in parts to cetyl alcohol, stearyl alcohol and cetylstearyl alcohol, the remaining components and amounts of addition being in accordance with example 1, the preparation being as described in reference to example 1.
Example 12
This example provides a hair mask with a restoration and softening effect which differs from example 1 only in that no cetostearyl alcohol is included in the formulation, the reduced amounts thereof are distributed in parts ratio to cetyl alcohol, stearyl alcohol and PEG/PPG-19/19 polymethylsiloxane, the remaining components and added amounts are in accordance with example 1, the preparation method being as described in reference to example 1.
Comparative example 1
This comparative example provides a hair film with a restoration and softening effect which differs from example 1 only in that the formulation does not include a hair conditioner, the reduced amount of which is proportionally distributed to the components of the hair conditioner in parts, the remaining components and the added amounts are the same as example 1, and the preparation method is referred to example 1.
Comparative example 2
This comparative example provides a hair film with a restoration and softening effect which differs from example 1 only in that the formulation does not include a hair care agent, the reduced amount of which is proportionally distributed to the components of the hair conditioner in parts, the remaining components and the added amounts are the same as example 1, and the preparation method is referred to example 1.
Comparative example 3
This comparative example provides a hair mask having a repairing and softening effect which is different from example 1 only in that the formulation does not include wheat amino acid, the reduction amount of which is complemented by cocoa butter and the remaining components and addition amounts are the same as in example 1, and the preparation method is referred to in example 1.
Comparative example 4
This comparative example provides a hair mask having a repair and softening effect which is different from example 1 only in that the formulation does not include cocoa butter, the reduction amount of which is complemented by wheat amino acid, and the remaining components and addition amounts are the same as in example 1, and the preparation method is referred to in example 1.
Test example 1 stability test
Stability testing includes high temperature, low temperature, and cold and hot cycle testing. Namely, the hair mask with repairing and softening effects of examples 1-12 and comparative examples 1-4 is placed at 48 ℃ and 15 ℃ below zero for 6 months respectively, whether the appearance of the product is cloudy, layered and other abnormal phenomena are observed regularly, the cold and hot cycle (once in 24h cold and hot cycle) is carried out at the cold and hot cycle temperature of-10 ℃ per 42 ℃, and whether the appearance of the product is abnormal is observed once per week after one month. The test results are shown in Table 2.
TABLE 2
Numbering device 48℃ -15℃ -10℃/42℃
Example 1 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 2 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 3 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 4 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 5 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 6 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 7 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 8 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Example 9 Cloudiness Layering of material Layering of material
Example 10 Uniform texture and no layering phenomenon Cloudiness Layering of material
Example 11 Layering of material Layering of material Cloudiness
Example 12 Layering of material Uniform texture and no layering phenomenon Layering of material
Comparative example 1 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Comparative example 2 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Comparative example 3 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
Comparative example 4 Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon Uniform texture and no layering phenomenon
From the data in table 2, the hair mask with repairing and softening effects provided by the invention has excellent high-low temperature stability, and can not generate turbidity and layering phenomena in high-temperature or low-temperature environments, wherein the type of the emulsifier is selected to influence the stability of the system.
Test example 2 combing force test
The combing force refers to the friction resistance of the hair to the comb, and the smaller the combing force is, the better the flexibility of the hair is. The combing property test of the hair is to simulate the friction resistance and the resistance change condition encountered when combing with a comb at each stage in the hair washing process of a consumer through a dynamic combing property tester of the hair, so as to judge the combing property of the hair washing and caring product. The invention uses the hair combing device to measure the combing force of the hair, and judges the softening effect of the hair through the combing force.
Object of measurement: the hair films of examples 1-12 and comparative examples 1-4 of the present invention, and two commercial hair care products with a restoration and softening effect.
The testing method comprises the following steps:
(1) Fixing a standard hair bundle on a carding instrument through a clamping plate, carding for 10 times by using a comb, and measuring carding force by using a hair carding instrument;
(2) Opening a shower nozzle to start showering, setting the water flow speed to be about 100ml/s, setting the water temperature to be (40+/-5) DEG C, and starting comb carding;
(3) Uniformly coating a sample of 4+/-0.5 g on a standard hair bundle, opening a shower nozzle to start showering after 10min, and combing for about 10 times by a comb while flushing;
(4) The hair was left under constant temperature and humidity for 24 hours, then combed with a comb about 10 times, and the combing force (gf) was measured with a hair combing machine.
The results are shown in Table 3
TABLE 3 Table 3
As can be seen from Table 3, the hair films prepared in examples 1-3 of the present invention have significantly improved softening effects relative to the commercially available hair care products.
From examples 4-8, it is clear that the choice of the type of hair conditioner according to the invention also has an effect on improving the softening effect of the hair.
Examples 9 to 12 show that the type of emulsifier affects the miscibility and viscosity of the product and thus the hair softening effect.
As can be seen from comparative examples 1 and 2, the hair conditioner and the hair care agent are used in combination, and the hair film of the present invention has a better effect of improving hair flexibility, and when either one of them is absent, the effect of improving hair flexibility of the product is reduced.
As can be seen from comparative examples 3-4, the hair care agent selected by the invention has a synergistic interaction between the wheat amino acid and the cocoa butter, and the combination of the wheat amino acid and the cocoa butter can better improve the softening effect of hair, and the lack of any one can reduce the softening effect.
Test example 3 gloss test
Measuring: hair masks with restoration and softening efficacy of inventive examples 1-12 and comparative examples 1-4.
The testing method comprises the following steps: 160 adult volunteers with the same hair volume and hair length between 18 and 45 years old are selected and randomly divided into 16 groups, the hair films with repairing and softening effects of the invention in examples 1 to 12 and comparative examples 1 to 4 are respectively tried, the samples to be tested are used for 1 time per night by each group of volunteers, 4+/-0.5 g of each sample is used, and the glossiness of the hair of each volunteer is respectively detected by using a Novo-Gloss glossiness meter on 0 day and 15 days in an evaluation experiment. The results are shown in Table 4.
TABLE 4 Table 4
As can be seen from Table 4, the hair films prepared in examples 1-3 of the present invention have a significant improvement in the degree of head gloss over the commercial hair care products.
From examples 4-8, it is clear that the selection of the type of hair conditioning agent according to the present invention has an effect on improving the gloss of the hair.
From comparative examples 1-2, it is clear that when either the hair conditioner or the hair care agent is absent, the product is inferior in improvement of the glossiness of hair, and the hair conditioner and the hair care agent are better in the combination use effect.
As can be seen from comparative examples 3-4, the choice of the type of hair care agent in the present invention also affects the gloss of the hair after the volunteer uses the product of the present invention.
Test example 4 consumer sensory effect evaluation
96 Female volunteers aged between 30-35 years were selected as subjects, and randomized into 16 groups of 6 persons each. The testing method comprises the following steps: the hair mask with repairing and softening effects of the invention examples 1-12 and comparative examples 1-4 are used by the test subjects, and are used for 1 time per night, 4+/-0.5 g for 15 days continuously, and the use effect is scored by the test subjects after the use is finished, and the hair mask is prepared by 10 scores: more than 9 minutes, the indication is very good and very satisfactory; 8-9 are preferably divided; a score of 7-8 is moderately acceptable; a score of 7 or less is not good and unacceptable. The scores for each group were 6-person averages and the results are shown in table 5.
TABLE 5
Sample of Softening effect Repairing effect Refreshing effect
Example 1 9.4 9.4 9.1
Example 2 9.3 9.5 9.6
Example 3 9.5 9.3 9.4
Example 4 8.5 8.8 9.0
Example 5 8.4 8.4 9.1
Example 6 7.9 8.7 8.7
Example 7 9.0 8.3 8.9
Example 8 8.7 8.7 8.4
Example 9 8.9 8.3 8.1
Example 10 8.7 8.5 8.3
Example 11 9.0 8.8 7.8
Example 12 8.4 7.9 7.9
Comparative example 1 7.5 8.2 7.1
Comparative example 2 7.9 7.6 7.4
Comparative example 3 8.3 9.0 8.8
Comparative example 4 8.9 8.2 8.6
As can be seen from Table 5, the product of the present invention has a good use effect, and is popular among testers in terms of softening effect, repairing effect and refreshing effect.
The applicant states that the present invention is described by way of the above examples as a hair mask having a repairing and softening effect and a method for preparing the same, but the present invention is not limited to the above examples, i.e. it is not meant that the present invention must be practiced by relying on the above examples. It should be apparent to those skilled in the art that any modification of the present invention, equivalent substitution of raw materials for the product of the present invention, addition of auxiliary components, selection of specific modes, etc., falls within the scope of the present invention and the scope of disclosure.
The preferred embodiments of the present invention have been described in detail above, but the present invention is not limited to the specific details of the above embodiments, and various simple modifications can be made to the technical solution of the present invention within the scope of the technical concept of the present invention, and all the simple modifications belong to the protection scope of the present invention.
In addition, the specific features described in the above embodiments may be combined in any suitable manner, and in order to avoid unnecessary repetition, various possible combinations are not described further.

Claims (10)

1. The hair mask with the repairing and softening effects is characterized in that the components of the hair mask with the repairing and softening effects comprise a humectant, an emulsifying agent, a hair conditioning agent, a hair care agent, a thickening agent and a solvent;
the hair care agent is a combination of wheat amino acid and cocoa butter.
2. The hair mask with repairing and softening effects according to claim 1, wherein the components of the hair mask with repairing and softening effects comprise, by weight, 0.1-10 parts of humectant, 1-40 parts of emulsifier, 1-60 parts of hair conditioner, 0.1-20 parts of hair care agent, 0.5-10 parts of thickener and 50-100 parts of solvent;
Preferably, the components of the hair mask with repairing and softening effects comprise, by weight, 1-8 parts of humectant, 5-35 parts of emulsifier, 10-50 parts of hair conditioner, 1-15 parts of hair care agent, 1-8 parts of thickener and 50-100 parts of solvent;
preferably, the components of the hair mask with repairing and softening effects comprise, by weight, 2-6 parts of humectant, 10-30 parts of emulsifier, 15-45 parts of hair conditioner, 5-12 parts of hair care agent, 1-5 parts of thickener and 50-100 parts of solvent.
3. The hair mask with repairing and softening effects according to claim 1 or 2, wherein the mass ratio of the wheat amino acid to the cocoa butter is 1 (0.1-2).
4. A hair film having a restoration and softening efficacy according to any one of claims 1 to 3, wherein said emulsifier comprises any one or a combination of at least two of cetyl alcohol, stearyl alcohol, PEG/PPG-19/19 polymethylsiloxane or cetostearyl alcohol;
Preferably, the emulsifier comprises a combination of cetyl alcohol, stearyl alcohol, PEG/PPG-19/19 polymethylsiloxane, and cetylstearyl alcohol;
preferably, the mass ratio of the cetyl alcohol, the stearyl alcohol, the PEG/PPG-19/19 polymethylsiloxane and the cetylstearyl alcohol is (1-3): 1-2): 0.5-1.5): 2-4.
5. The hair mask with restoration and softening efficacy according to any one of claims 1 to 4, wherein said humectant comprises sodium polyglutamate;
preferably, the thickener comprises hydroxyethyl cellulose and/or methyl cellulose.
6. A hair film having a restoration and softening efficacy according to any one of claims 1 to 5, wherein said hair conditioning agent comprises any one or a combination of at least two of amino-terminal polydimethylsiloxane, cetyltrimethylammonium chloride, ethylhexyl glycerol, cyclopenta-dimethicone, or behenyl trimethylammonium methyl sulfate;
preferably, the hair conditioner is a combination of amino-terminal polydimethylsiloxane, cetyltrimethylammonium chloride, ethylhexyl glycerol, cyclopentadimethicone, and behenyl trimethylammonium methylsulfate;
preferably, the mass ratio of the ammonia end polydimethylsiloxane, the cetyltrimethylammonium chloride, the ethylhexyl glycerol, the cyclopentadimethicone and the beyltrimethylammonium methyl sulfate is (1-4): 1-2): 0.1-1.5): 1-2): 0.1-1.8.
7. A hair film having a restoration and softening efficacy according to any one of claims 1 to 6, wherein said solvent comprises any one or a combination of at least two of deionized water, ethanol or isohexadecane;
Preferably, the components of the hair mask with repairing and softening effects further comprise any one or a combination of at least two of preservative, aromatic or pH regulator;
preferably, the preservative comprises phenoxyethanol;
Preferably, the fragrance comprises a perfume;
Preferably, the pH adjuster comprises acetic acid and/or sodium hydroxide.
8. A method for preparing a hair film with repairing and softening effects according to any one of claims 1 to 7, wherein the method comprises homogenizing a humectant, an emulsifier, a hair conditioner, a hair care agent and a thickener in a solvent to obtain the hair film with repairing and softening effects.
9. The method of manufacturing according to claim 8, wherein the method of manufacturing comprises:
(1) Heating deionized water, adding humectant, thickener and isododecane, mixing and homogenizing;
(2) Cooling, adding hair conditioner, emulsifier and ethanol, mixing, and homogenizing;
(3) Continuously cooling, adding a hair care agent, mixing and homogenizing, and standing to obtain the hair mask with repairing and softening effects.
10. The method of claim 9, wherein the temperature in step (1) is raised to 80-90 ℃;
Preferably, the temperature in the step (2) is reduced to 60-70 ℃;
preferably, the temperature in the step (3) is reduced to 35-45 ℃;
Preferably, step (3) further comprises adding any one or a combination of at least two of a preservative, a fragrance, or a pH adjuster;
Preferably, the mixing in the step (3) is performed in a stirring manner, and the stirring time is 5-20min;
Preferably, the time of standing in the step (3) is 1-2h.
CN202410219499.9A 2024-02-28 2024-02-28 Hair mask with repairing and softening effects and preparation method thereof Pending CN118001190A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202410219499.9A CN118001190A (en) 2024-02-28 2024-02-28 Hair mask with repairing and softening effects and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202410219499.9A CN118001190A (en) 2024-02-28 2024-02-28 Hair mask with repairing and softening effects and preparation method thereof

Publications (1)

Publication Number Publication Date
CN118001190A true CN118001190A (en) 2024-05-10

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Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Link
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