CN1166385C - Chinese herbal medicine composition for treating caries pain and its prepn - Google Patents
Chinese herbal medicine composition for treating caries pain and its prepn Download PDFInfo
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- CN1166385C CN1166385C CNB011290706A CN01129070A CN1166385C CN 1166385 C CN1166385 C CN 1166385C CN B011290706 A CNB011290706 A CN B011290706A CN 01129070 A CN01129070 A CN 01129070A CN 1166385 C CN1166385 C CN 1166385C
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- 239000000203 mixture Substances 0.000 title claims abstract description 19
- 208000002925 dental caries Diseases 0.000 title claims abstract description 13
- 241000411851 herbal medicine Species 0.000 title claims abstract description 12
- 208000002193 Pain Diseases 0.000 title abstract description 10
- 230000036407 pain Effects 0.000 title abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 20
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims abstract description 10
- 238000002360 preparation method Methods 0.000 claims abstract description 9
- 239000000047 product Substances 0.000 claims description 14
- 239000012467 final product Substances 0.000 claims description 11
- WABPQHHGFIMREM-UHFFFAOYSA-N lead(0) Chemical compound [Pb] WABPQHHGFIMREM-UHFFFAOYSA-N 0.000 claims description 11
- 239000006071 cream Substances 0.000 claims description 10
- 229940025250 camphora Drugs 0.000 claims description 9
- 239000010238 camphora Substances 0.000 claims description 9
- 208000004371 toothache Diseases 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 2
- 238000007789 sealing Methods 0.000 claims 1
- 210000000214 mouth Anatomy 0.000 abstract description 12
- 238000004140 cleaning Methods 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 7
- 231100000820 toxicity test Toxicity 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
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- 238000000605 extraction Methods 0.000 abstract 2
- 235000007650 Aralia spinosa Nutrition 0.000 abstract 1
- 241000758794 Asarum Species 0.000 abstract 1
- 241000723346 Cinnamomum camphora Species 0.000 abstract 1
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 1
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 1
- 241000951473 Schizonepeta Species 0.000 abstract 1
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- 229960000846 camphor Drugs 0.000 abstract 1
- 229930008380 camphor Natural products 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 238000005728 strengthening Methods 0.000 abstract 1
- 239000000341 volatile oil Substances 0.000 description 8
- 239000002131 composite material Substances 0.000 description 6
- 239000002075 main ingredient Substances 0.000 description 6
- 231100000614 poison Toxicity 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- NFLGAXVYCFJBMK-RKDXNWHRSA-N (+)-isomenthone Natural products CC(C)[C@H]1CC[C@@H](C)CC1=O NFLGAXVYCFJBMK-RKDXNWHRSA-N 0.000 description 4
- 206010019233 Headaches Diseases 0.000 description 4
- 208000032843 Hemorrhage Diseases 0.000 description 4
- NFLGAXVYCFJBMK-UHFFFAOYSA-N Menthone Chemical compound CC(C)C1CCC(C)CC1=O NFLGAXVYCFJBMK-UHFFFAOYSA-N 0.000 description 4
- ZYEMGPIYFIJGTP-UHFFFAOYSA-N O-methyleugenol Chemical group COC1=CC=C(CC=C)C=C1OC ZYEMGPIYFIJGTP-UHFFFAOYSA-N 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
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- 239000003921 oil Substances 0.000 description 4
- 230000007096 poisonous effect Effects 0.000 description 4
- ZMQAAUBTXCXRIC-UHFFFAOYSA-N safrole Chemical compound C=CCC1=CC=C2OCOC2=C1 ZMQAAUBTXCXRIC-UHFFFAOYSA-N 0.000 description 4
- 230000001225 therapeutic effect Effects 0.000 description 4
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 231100000331 toxic Toxicity 0.000 description 3
- 230000002588 toxic effect Effects 0.000 description 3
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 2
- NFLGAXVYCFJBMK-DTWKUNHWSA-N (+)-menthone Chemical compound CC(C)[C@H]1CC[C@H](C)CC1=O NFLGAXVYCFJBMK-DTWKUNHWSA-N 0.000 description 2
- PEYUIKBAABKQKQ-AFHBHXEDSA-N (+)-sesamin Chemical compound C1=C2OCOC2=CC([C@H]2OC[C@H]3[C@@H]2CO[C@@H]3C2=CC=C3OCOC3=C2)=C1 PEYUIKBAABKQKQ-AFHBHXEDSA-N 0.000 description 2
- KSEBMYQBYZTDHS-HWKANZROSA-M (E)-Ferulic acid Natural products COC1=CC(\C=C\C([O-])=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-M 0.000 description 2
- 241000758795 Aristolochiaceae Species 0.000 description 2
- NFHFNBFYZIJLKZ-UHFFFAOYSA-N Asarinin Natural products CC1(OCC2C1COC2c3ccc4OCOc4c3)c5ccc6OCOc6c5 NFHFNBFYZIJLKZ-UHFFFAOYSA-N 0.000 description 2
- 241000125183 Crithmum maritimum Species 0.000 description 2
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 2
- 208000010201 Exanthema Diseases 0.000 description 2
- 241000628997 Flos Species 0.000 description 2
- 244000246386 Mentha pulegium Species 0.000 description 2
- 235000016257 Mentha pulegium Nutrition 0.000 description 2
- 235000004357 Mentha x piperita Nutrition 0.000 description 2
- 208000003251 Pruritus Diseases 0.000 description 2
- 208000025865 Ulcer Diseases 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 230000036592 analgesia Effects 0.000 description 2
- 230000000202 analgesic effect Effects 0.000 description 2
- 230000000675 anti-caries Effects 0.000 description 2
- 235000019636 bitter flavor Nutrition 0.000 description 2
- 210000000481 breast Anatomy 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 208000002173 dizziness Diseases 0.000 description 2
- PEYUIKBAABKQKQ-UHFFFAOYSA-N epiasarinin Natural products C1=C2OCOC2=CC(C2OCC3C2COC3C2=CC=C3OCOC3=C2)=C1 PEYUIKBAABKQKQ-UHFFFAOYSA-N 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
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- KSEBMYQBYZTDHS-HWKANZROSA-N ferulic acid Chemical compound COC1=CC(\C=C\C(O)=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-N 0.000 description 2
- 229940114124 ferulic acid Drugs 0.000 description 2
- KSEBMYQBYZTDHS-UHFFFAOYSA-N ferulic acid Natural products COC1=CC(C=CC(O)=O)=CC=C1O KSEBMYQBYZTDHS-UHFFFAOYSA-N 0.000 description 2
- 235000001785 ferulic acid Nutrition 0.000 description 2
- 238000005469 granulation Methods 0.000 description 2
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- 235000001050 hortel pimenta Nutrition 0.000 description 2
- 208000014674 injury Diseases 0.000 description 2
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- 229940041616 menthol Drugs 0.000 description 2
- 229940116837 methyleugenol Drugs 0.000 description 2
- PRHTXAOWJQTLBO-UHFFFAOYSA-N methyleugenol Natural products COC1=CC=C(C(C)=C)C=C1OC PRHTXAOWJQTLBO-UHFFFAOYSA-N 0.000 description 2
- 231100000957 no side effect Toxicity 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
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- 206010037844 rash Diseases 0.000 description 2
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- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 description 2
- 231100000397 ulcer Toxicity 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000959626 Calvatia Species 0.000 description 1
- 241000006348 Hemiphragma Species 0.000 description 1
- 229910000805 Pig iron Inorganic materials 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 239000000730 antalgic agent Substances 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000002481 ethanol extraction Methods 0.000 description 1
- 210000004195 gingiva Anatomy 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 229910052957 realgar Inorganic materials 0.000 description 1
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
Abstract
The present invention discloses a Chinese herbal medicine composition for treating caries pain, and a preparation method thereof. The composition is composed of raw materials of weight percentage: 12 to 22% of asarum herb, 5 to 12% of pricklyash peel, 5 to 12% of chuanqiong rhizome, 5 to 12% of mint, 5 to 12% of schizonepeta herb, 5 to 12% of yellow lead and 35 to 60% of camphor. The preparation method comprises the following steps of raw material preparation, mixture, pulverization and extraction; the extraction lasts for 3 minutes in the environment of 100 to 150DEG C, and mist-like substances are collected and sealed. Toxicity tests prove that the composition is actually nontoxic; clinical use proves that the extract of the composition has 100% of excellence rate for the caries pain; the effective rate reaches 98%, and cure rate reaches 96%. The composition also has the functions of strengthening teeth, cleaning the oral cavity and keeping the oral cavity healthy.
Description
Affiliated technical field: the present invention relates to a kind of herbal composite for the treatment of caries pain and preparation method thereof.
Prior art situation: in the prior art of application Chinese patent; application number is that the main effect of 92100896 tooth-protective gargle is an anti-caries; protection gingiva oral hygiene; it is by bubble-pass bead; Cortex Magnoliae Officinalis; Pericarpium Zanthoxyli; the ethanol extraction assembly of Herba Menthae forms; the nontoxic level in true border; and application number is 92106198 prior art; be to comprise Flos Caryophylli by kinds of traditional Chinese medicines; Herba Menthae; Radix Glycyrrhizae; Radix Sophorae Tonkinensis; Lasiosphaera Seu Calvatia; Herba Taraxaci; big table leaf; Fructus Forsythiae; Flos Lonicerae and other chemical assistant assembly form; its main effect is an anti-caries; application number is 94113223 application for a patent for invention, relates to the treatment toothache; by Herba Senecionis Chrysanthemoidis; Herba lonicerae delavayi; big device piece watt; diversifolious hemiphragma herb; pig-iron nitre; the assembly of aufe nitre forms.Application number is that 96122142 anodyne powder for carious tooth mainly is made up of Realgar, Gypsum Fibrosum, directly be applied on the affected part, application number be 98112734 treatment toothache medicine by ZHIMUYE, flourish Herba Taraxaci, Herba Houttuyniae, Herba Plantaginis, Radix trachycarpi form, dental caries, acute toothache are had certain effect.
In sum, in the existing Chinese patent application, the great majority invention mainly is a caries prevention, and the innovation and creation of the toothache that special for treating produces because of dental caries yet there are no report, analyze some that all adopts Chinese medicine in the above-mentioned prior art, but the subsequent technology means are again with solvent extraction or add other chemical addition agent, and actual human body are had certain toxic and side effects.
Goal of the invention:
The objective of the invention is to be intended to overcome above-mentioned prior art defective provides a kind of pure natural, without any side effects to human body, the herbal composite of the treatment caries pain that obvious effective rate is high;
Another object of the present invention provides the method for preparing said composition;
Technology contents: the herbal composite of treatment caries pain involved in the present invention mainly by: Herba Asari, Pericarpium Zanthoxyli, Rhizoma Chuanxiong, Herba Menthae, Herba Schizonepetae, Plumbum preparatium, Camphora are formed, wherein: Herba Asari 12～22%, Pericarpium Zanthoxyli 5～12%, Rhizoma Chuanxiong 5～12%, Herba Menthae 5～12%, Herba Schizonepetae 5～12%, Plumbum preparatium 5～12%, Camphora 35～60%.
Above-mentioned content all is weight percentage.
In said components, that all raw materials all should be selected is pollution-free, do not have the finished product that goes mouldy.
The preparation method of said composition is:
A, selected raw material: select Chinese herbal medicine finished product pollution-free, that nothing is gone mouldy standby;
B, mixing are pulverized: the Chinese herbal medicine finished product of choosing is mixed the back pulverize, be processed into Powdered standby;
C, refinement: the ready raw material in top is packed in the container, container is heated to 100 °～150 ℃, kept 3 minutes, the spray of getting rid of in the collection container, the cooling back forms white cream and get final product, collect cream, seal standby.
The using method of said composition is: at first the affected part is cleaned with clear water, the medicine frost is applied directly over the affected part, got final product in containing 1-3 minute.
Put down in writing in the simple and clear Chinese herbology of being published in November, 1987 by the People's Health Publisher: Herba Asari is an aristolochiaceae plant, it is 26% that herb contains volatile oil, Main Ingredients and Appearance is methyleugenol, safrole etc. in the Shan, other contains asarinin, effectiveness is warm in nature, acrid in the mouth, slightly poisonous, function that pain on the warming the meridian is arranged, is usually used in card such as headache toothache grade; Rhizoma Chuanxiong is a samphire, contains 1% volatile oil, ferulic acid etc., and it is warm in nature, mildly bitter flavor, suffering.Blood-activating and qi-promoting is arranged, the wind analgesic effect Herba Menthae that looses is that labiate contains volatile oil, Main Ingredients and Appearance is a menthol in the oil, menthone and peppermint ester etc., cool in nature, acrid in the mouth, the mediation wind heat is arranged, the refresh oneself, throat, deliver the function of rash, teleneuron there is analgesia itching relieving function, Herba Schizonepetae is a labiate, contain volatile oil, Main Ingredients and Appearance in the oil is slightly warm in nature such as D-menthone and racemization menthone, acrid in the mouth, can control hemorrhage, diseases such as headache and dizziness, the Plumbum preparatium, the bosom is hot, be slightly cold, poisonous, but removing toxic substances and promoting granulation, treatment of ulcer festers, the malignant boil toxic swelling, knife injury is hemorrhage.
Amount to the obvious efficient 100% of the clinical use certificate of 186 routine caries pain patients, effective percentage 98%, cure rate 96% through hospital.
Prove through toxicity test: said composition has no side effect to human body.
The present invention compared with prior art has the following advantages:
1, therapeutic effect is good: through 180 routine clinical uses, obvious effective rate 100%, effective percentage 98%, cure rate 96%.
2, easy to use: with after the affected part cleaning, directly be applied to herein during use, containing 1-3 minute, the cleaning oral cavity that spues got final product;
3, easy to make, with low cost;
4, raw material is simple and easy to, no chemical assistant and other additive;
5, dosage is few, and the treatment cost is low, and treatment once only needs 0.5～0.8 gram, and the patient can fully recover.
Provide embodiment of the present invention below, the present invention be further described:
Implement 1:
This herbal composite mainly by: Herba Asari, Pericarpium Zanthoxyli, Rhizoma Chuanxiong, Herba Menthae, Herba Schizonepetae, Plumbum preparatium, Camphora are formed, wherein: Herba Asari 12%, Pericarpium Zanthoxyli 5%, Rhizoma Chuanxiong 5%, Herba Menthae 5%, Herba Schizonepetae 5%, Plumbum preparatium 12%, Camphora 56%.
Above-mentioned content all is weight percentage.
In said components, all raw materials all should be selected finished product pollution-free, that nothing is gone mouldy, grade is higher.
The preparation method of said composition is:
A, selected raw material: select Chinese herbal medicine finished product pollution-free, that nothing is gone mouldy standby;
B, mixing are pulverized: the Chinese herbal medicine finished product of choosing is mixed the back pulverize, be processed into Powdered standby;
C, refinement: the ready raw material in top is packed in the container, container is heated to 100 ℃, kept 3 minutes, the spray of getting rid of in the collection container, the cooling back forms white cream and get final product, collect cream, seal standby.
Put down in writing in the simple and clear Chinese herbology of being published in November, 1987 by the People's Health Publisher: Herba Asari is an aristolochiaceae plant, it is 26% that herb contains volatile oil, Main Ingredients and Appearance is methyleugenol, safrole etc. in the Shan, other contains asarinin, effectiveness is warm in nature, acrid in the mouth, slightly poisonous, function that pain on the warming the meridian is arranged, is usually used in disease such as headache toothache grade; Rhizoma Chuanxiong is a samphire, contains 1% volatile oil, ferulic acid etc., and it is warm in nature, mildly bitter flavor, suffering.Blood-activating and qi-promoting is arranged, the wind analgesic effect Herba Menthae that looses is that labiate contains volatile oil, Main Ingredients and Appearance is a menthol in the oil, menthone and peppermint ester etc., cool in nature, acrid in the mouth, the mediation wind heat is arranged, the refresh oneself, throat, deliver the function of rash, teleneuron there is analgesia itching relieving function, Herba Schizonepetae is a labiate, contain volatile oil, Main Ingredients and Appearance in the oil is slightly warm in nature such as D-menthone and racemization menthone, acrid in the mouth, can control hemorrhage, diseases such as headache and dizziness, the Plumbum preparatium, the bosom is hot, be slightly cold, poisonous, but removing toxic substances and promoting granulation, treatment of ulcer festers, the malignant boil toxic swelling, knife injury is hemorrhage.
The using method of said composition is: at first the affected part is cleaned with clear water, the medicine frost is applied directly over the affected part, got final product in containing 1-3 minute.
Amount to the obvious efficient 100% of the clinical use certificate of 186 routine caries pain patients, effective percentage 98%, cure rate 96% through hospital.
Prove through toxicity test: said composition has no side effect to human body.
The present invention compared with prior art has the following advantages: therapeutic effect is good: through 180 routine clinical uses, obvious effective rate 100%, effective percentage 98%, cure rate 96%; Easy to use: with after the affected part cleaning, directly be applied to herein during use, containing 1-3 minute, the cleaning oral cavity that spues got final product; Easy to make, with low cost; Raw material is simple and easy to, no chemical assistant and other additive; Dosage is few, and the treatment cost is low, and treatment once only needs 0.5～0.8 gram, and the patient can fully recover.
Embodiment 2:
This herbal composite mainly by: Herba Asari, Pericarpium Zanthoxyli, Rhizoma Chuanxiong, Herba Menthae, Herba Schizonepetae, Plumbum preparatium, Camphora are formed, wherein: Herba Asari 17%, Pericarpium Zanthoxyli 9%, Rhizoma Chuanxiong 9%, Herba Menthae 9%, Herba Schizonepetae 9%, Plumbum preparatium 9%, Camphora 38%.
Above-mentioned content all is weight percentage.
In said components, all raw materials all should be selected finished product pollution-free, that nothing is gone mouldy, grade is higher.
The preparation method of said composition is:
A, selected raw material: select Chinese herbal medicine finished product pollution-free, that nothing is gone mouldy, standby;
B, mixing are pulverized: the Chinese herbal medicine finished product of choosing is mixed the back pulverize, be processed into Powdered standby;
C, refinement: the ready raw material in top is packed in the container, container is heated to 130 ℃, kept 2 minutes, the spray of getting rid of in the collection container, the cooling back forms white cream and get final product, collect cream, seal standby.
The present invention compared with prior art has the following advantages: therapeutic effect is good: through 180 routine clinical uses, obvious effective rate 100%, effective percentage 98%, cure rate 96%; Easy to use: with after the affected part cleaning, directly be applied to herein during use, containing 1-3 minute, the cleaning oral cavity that spues got final product; Easy to make, with low cost; Raw material is simple and easy to, no chemical assistant and other additive; Dosage is few, and the treatment cost is low, and treatment once only needs 0.5～0.8 gram, and the patient can fully recover.
Implement 3: this herbal composite mainly by: Herba Asari, Pericarpium Zanthoxyli, Rhizoma Chuanxiong, Herba Menthae, Herba Schizonepetae, Plumbum preparatium, Camphora are formed, wherein: Herba Asari 12%, Pericarpium Zanthoxyli 5%, Rhizoma Chuanxiong 5%, Herba Menthae 5%, Herba Schizonepetae 12%, Plumbum preparatium 12%, Camphora 49%.
Above-mentioned content all is weight percentage.
In said components, that all raw materials all should be selected is pollution-free, do not have the finished product that goes mouldy.
The preparation method of said composition is:
A, selected raw material: select the Chinese herbal medicine finished product pollution-free, that nothing is gone mouldy, grade is higher, standby;
B, mixing are pulverized: the Chinese herbal medicine finished product of choosing is mixed the back pulverize, be processed into Powdered standby;
C, refinement: the ready raw material in top is packed in the container, container is heated to 130 ℃, kept 2 minutes, the spray of getting rid of in the collection container, the cooling back forms white cream and get final product, collect cream, seal standby.
The present invention compared with prior art has the following advantages: therapeutic effect is good: through 180 routine clinical uses, obvious effective rate 100%, effective percentage 98%, cure rate 96%; Easy to use: with after the affected part cleaning, directly be applied to herein during use, containing 1-3 minute, the cleaning oral cavity that spues got final product; Easy to make, with low cost; Raw material is simple and easy to, no chemical assistant and other additive; Dosage is few, and the treatment cost is low, and treatment once only needs 0.5～0.8 gram, and the patient can fully recover.
Claims (1)
1, the compositions of the toothache that caused by dental caries of a kind of treatment is characterized in that it is made by described method by following weight percentages:
Raw material: Herba Asari 12-22%, Pericarpium Zanthoxyli 5-12%, Rhizoma Chuanxiong 5-12%, Herba Menthae 5-12%, Plumbum preparatium 5-12%, Camphora 35-60%,
Preparation method: A, selected raw material: select Chinese herbal medicine finished product pollution-free, that nothing is gone mouldy;
B, mixing are pulverized: the Chinese herbal medicine finished product mix homogeneously with choosing is ground into Powdered standby;
C, refinement: the above-mentioned powder of getting ready is packed in the container, container is heated to 100～150 ℃ kept 3 minutes, the spray that produces in the collection container, the cooling back forms white cream, collects the cream sealing and gets final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011290706A CN1166385C (en) | 2001-11-15 | 2001-11-15 | Chinese herbal medicine composition for treating caries pain and its prepn |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011290706A CN1166385C (en) | 2001-11-15 | 2001-11-15 | Chinese herbal medicine composition for treating caries pain and its prepn |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1398611A CN1398611A (en) | 2003-02-26 |
| CN1166385C true CN1166385C (en) | 2004-09-15 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB011290706A Expired - Fee Related CN1166385C (en) | 2001-11-15 | 2001-11-15 | Chinese herbal medicine composition for treating caries pain and its prepn |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100361684C (en) * | 2005-08-26 | 2008-01-16 | 贵州奥特药业有限公司 | Chinese medicinal preparation for treating decayed teeth and preparation process thereof |
| CN109432292A (en) * | 2018-12-24 | 2019-03-08 | 四川芝林宜健生物科技有限公司 | It is a kind of for treat toothache external application Chinese medicine and preparation method |
| CN115770205A (en) * | 2021-09-04 | 2023-03-10 | 武汉左点科技有限公司 | Oral cavity cleaning liquid and preparation method and application thereof |
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2001
- 2001-11-15 CN CNB011290706A patent/CN1166385C/en not_active Expired - Fee Related
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| Publication number | Publication date |
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| CN1398611A (en) | 2003-02-26 |
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