CN116209682B - 中空颗粒的制造方法 - Google Patents

中空颗粒的制造方法 Download PDF

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Publication number
CN116209682B
CN116209682B CN202180064567.3A CN202180064567A CN116209682B CN 116209682 B CN116209682 B CN 116209682B CN 202180064567 A CN202180064567 A CN 202180064567A CN 116209682 B CN116209682 B CN 116209682B
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Prior art keywords
hollow particles
monomer
polymerizable monomer
mass
meth
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CN202180064567.3A
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Chinese (zh)
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CN116209682A (zh
Inventor
渡边真司
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Zeon Corp
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Zeon Corp
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B01J13/18—In situ polymerisation with all reactants being present in the same phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B01J13/18—In situ polymerisation with all reactants being present in the same phase
    • B01J13/185—In situ polymerisation with all reactants being present in the same phase in an organic phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/20—After-treatment of capsule walls, e.g. hardening
    • B01J13/206—Hardening; drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/18—Suspension polymerisation
    • C08F2/20—Suspension polymerisation with the aid of macromolecular dispersing agents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/10—Esters
    • C08F20/12—Esters of monohydric alcohols or phenols
    • C08F20/16—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F20/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F222/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides, or nitriles thereof
    • C08F222/10—Esters
    • C08F222/1006—Esters of polyhydric alcohols or polyhydric phenols
    • C08F222/102—Esters of polyhydric alcohols or polyhydric phenols of dialcohols, e.g. ethylene glycol di(meth)acrylate or 1,4-butanediol dimethacrylate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F265/00—Macromolecular compounds obtained by polymerising monomers on to polymers of unsaturated monocarboxylic acids or derivatives thereof as defined in group C08F20/00
    • C08F265/04—Macromolecular compounds obtained by polymerising monomers on to polymers of unsaturated monocarboxylic acids or derivatives thereof as defined in group C08F20/00 on to polymers of esters
    • C08F265/06—Polymerisation of acrylate or methacrylate esters on to polymers thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L35/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical, and containing at least one other carboxyl radical in the molecule, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • C08L35/02—Homopolymers or copolymers of esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
    • C08F2800/20—Copolymer characterised by the proportions of the comonomers expressed as weight or mass percentages
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2810/00—Chemical modification of a polymer
    • C08F2810/20—Chemical modification of a polymer leading to a crosslinking, either explicitly or inherently

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Polymerisation Methods In General (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Graft Or Block Polymers (AREA)
CN202180064567.3A 2020-09-30 2021-09-28 中空颗粒的制造方法 Active CN116209682B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2020165179 2020-09-30
JP2020-165179 2020-09-30
PCT/JP2021/035538 WO2022071276A1 (ja) 2020-09-30 2021-09-28 中空粒子の製造方法

Publications (2)

Publication Number Publication Date
CN116209682A CN116209682A (zh) 2023-06-02
CN116209682B true CN116209682B (zh) 2025-07-04

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CN202180064567.3A Active CN116209682B (zh) 2020-09-30 2021-09-28 中空颗粒的制造方法

Country Status (4)

Country Link
US (1) US12465901B2 (https=)
JP (1) JP7743837B2 (https=)
CN (1) CN116209682B (https=)
WO (1) WO2022071276A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20230098157A (ko) 2020-10-30 2023-07-03 니폰 제온 가부시키가이샤 중공 입자의 제조 방법 및 중공 입자
KR20230098160A (ko) * 2020-10-30 2023-07-03 니폰 제온 가부시키가이샤 중공 입자의 제조 방법 및 중공 입자
WO2022107674A1 (ja) * 2020-11-20 2022-05-27 日本ゼオン株式会社 中空粒子
WO2023074651A1 (ja) * 2021-10-29 2023-05-04 日本ゼオン株式会社 中空粒子、中空粒子の製造方法、樹脂組成物、及び成形体
EP4613783A1 (en) 2022-10-31 2025-09-10 Zeon Corporation Hollow particles, manufacturing method of hollow particles, resin composition and resin structure

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107922521A (zh) * 2015-09-07 2018-04-17 日本瑞翁株式会社 中空聚合物粒子的水分散液的制造方法
CN110997736A (zh) * 2017-08-01 2020-04-10 日本瑞翁株式会社 胶乳的制造方法和中空树脂颗粒的制造方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4448930B2 (ja) 2000-09-04 2010-04-14 財団法人新産業創造研究機構 中空高分子微粒子及びその製造法
JP4210566B2 (ja) * 2003-08-05 2009-01-21 積水化学工業株式会社 中空樹脂微粒子の製造方法及び中空樹脂微粒子
US7247414B2 (en) * 2003-12-11 2007-07-24 Seiko Epson Corporation Method for producing resin particles and toner using the resin particles
US8465836B2 (en) * 2010-07-27 2013-06-18 Sekisui Chemical Co., Ltd. Method for producing single-hole hollow polymer particles
JP6468780B2 (ja) 2014-09-30 2019-02-13 積水化成品工業株式会社 中空樹脂粒子及びその製造方法
JP6460884B2 (ja) 2015-03-31 2019-01-30 積水化成品工業株式会社 中空樹脂粒子の製造方法
CN109476772B (zh) * 2016-08-02 2021-01-05 松本油脂制药株式会社 树脂中空粒子及其应用
JP7342376B2 (ja) 2019-02-25 2023-09-12 日本ゼオン株式会社 中空樹脂粒子の製造方法
EP3992213A4 (en) * 2019-06-27 2023-07-26 Zeon Corporation PROCESS FOR PRODUCTION OF HOLLOW RESIN PARTICLES
US12485399B2 (en) * 2019-12-06 2025-12-02 Zeon Corporation Hollow particles, resin composition and molded body

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107922521A (zh) * 2015-09-07 2018-04-17 日本瑞翁株式会社 中空聚合物粒子的水分散液的制造方法
CN110997736A (zh) * 2017-08-01 2020-04-10 日本瑞翁株式会社 胶乳的制造方法和中空树脂颗粒的制造方法

Also Published As

Publication number Publication date
US20230381731A1 (en) 2023-11-30
JPWO2022071276A1 (https=) 2022-04-07
CN116209682A (zh) 2023-06-02
JP7743837B2 (ja) 2025-09-25
US12465901B2 (en) 2025-11-11
WO2022071276A1 (ja) 2022-04-07

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