CN115531277A - Natural herbal composition with hair loss prevention and hair solidification effects and preparation method and application thereof - Google Patents
Natural herbal composition with hair loss prevention and hair solidification effects and preparation method and application thereof Download PDFInfo
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- CN115531277A CN115531277A CN202211513070.8A CN202211513070A CN115531277A CN 115531277 A CN115531277 A CN 115531277A CN 202211513070 A CN202211513070 A CN 202211513070A CN 115531277 A CN115531277 A CN 115531277A
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- 210000004209 hair Anatomy 0.000 title claims abstract description 42
- 230000000694 effects Effects 0.000 title claims abstract description 36
- 230000003658 preventing hair loss Effects 0.000 title claims abstract description 33
- 238000007711 solidification Methods 0.000 title claims abstract description 9
- 230000008023 solidification Effects 0.000 title claims abstract description 9
- 238000002360 preparation method Methods 0.000 title claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 55
- 229910052588 hydroxylapatite Inorganic materials 0.000 claims abstract description 50
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 claims abstract description 50
- 229920001661 Chitosan Polymers 0.000 claims abstract description 40
- 239000008367 deionised water Substances 0.000 claims abstract description 39
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 39
- 239000003607 modifier Substances 0.000 claims abstract description 33
- 238000004090 dissolution Methods 0.000 claims abstract description 25
- 239000002994 raw material Substances 0.000 claims abstract description 22
- 230000004048 modification Effects 0.000 claims abstract description 14
- 238000012986 modification Methods 0.000 claims abstract description 14
- 241000830535 Ligustrum lucidum Species 0.000 claims abstract description 11
- 241001248610 Ophiocordyceps sinensis Species 0.000 claims abstract description 11
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims abstract description 11
- 235000003140 Panax quinquefolius Nutrition 0.000 claims abstract description 11
- 244000046146 Pueraria lobata Species 0.000 claims abstract description 11
- 235000010575 Pueraria lobata Nutrition 0.000 claims abstract description 11
- 235000009108 Urtica dioica Nutrition 0.000 claims abstract description 11
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 11
- 235000008434 ginseng Nutrition 0.000 claims abstract description 11
- 235000001287 Guettarda speciosa Nutrition 0.000 claims abstract description 10
- 241000246044 Sophora flavescens Species 0.000 claims abstract description 9
- 230000035515 penetration Effects 0.000 claims abstract description 8
- 241001289529 Fallopia multiflora Species 0.000 claims abstract description 5
- 244000061520 Angelica archangelica Species 0.000 claims abstract 3
- 244000274883 Urtica dioica Species 0.000 claims abstract 3
- 238000003756 stirring Methods 0.000 claims description 54
- 238000000855 fermentation Methods 0.000 claims description 43
- 230000004151 fermentation Effects 0.000 claims description 43
- 238000005406 washing Methods 0.000 claims description 30
- 235000007164 Oryza sativa Nutrition 0.000 claims description 29
- 235000009566 rice Nutrition 0.000 claims description 29
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 28
- 238000005728 strengthening Methods 0.000 claims description 22
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 14
- 238000001035 drying Methods 0.000 claims description 14
- 239000012747 synergistic agent Substances 0.000 claims description 14
- 241000208340 Araliaceae Species 0.000 claims description 10
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 7
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 7
- 239000007822 coupling agent Substances 0.000 claims description 7
- VQEHIYWBGOJJDM-UHFFFAOYSA-H lanthanum(3+);trisulfate Chemical compound [La+3].[La+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O VQEHIYWBGOJJDM-UHFFFAOYSA-H 0.000 claims description 7
- 238000007789 sealing Methods 0.000 claims description 7
- 229910052708 sodium Inorganic materials 0.000 claims description 7
- 239000011734 sodium Substances 0.000 claims description 7
- 235000010413 sodium alginate Nutrition 0.000 claims description 7
- 229940005550 sodium alginate Drugs 0.000 claims description 7
- 239000000661 sodium alginate Substances 0.000 claims description 7
- 238000010025 steaming Methods 0.000 claims description 7
- 240000001341 Reynoutria japonica Species 0.000 claims description 6
- 235000018167 Reynoutria japonica Nutrition 0.000 claims description 6
- -1 sodium alkylsulfonate Chemical class 0.000 claims description 5
- 240000007594 Oryza sativa Species 0.000 claims 4
- 230000003656 anti-hair-loss Effects 0.000 abstract description 2
- 235000008216 herbs Nutrition 0.000 abstract description 2
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 244000131316 Panax pseudoginseng Species 0.000 abstract 1
- 241000209094 Oryza Species 0.000 description 25
- 201000004384 Alopecia Diseases 0.000 description 10
- 241000219422 Urtica Species 0.000 description 8
- 231100000360 alopecia Toxicity 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
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- 239000007788 liquid Substances 0.000 description 5
- 210000004761 scalp Anatomy 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 230000003676 hair loss Effects 0.000 description 2
- 208000024963 hair loss Diseases 0.000 description 2
- NOESYZHRGYRDHS-UHFFFAOYSA-N insulin Chemical compound N1C(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(NC(=O)CN)C(C)CC)CSSCC(C(NC(CO)C(=O)NC(CC(C)C)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CCC(N)=O)C(=O)NC(CC(C)C)C(=O)NC(CCC(O)=O)C(=O)NC(CC(N)=O)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CSSCC(NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2C=CC(O)=CC=2)NC(=O)C(CC(C)C)NC(=O)C(C)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2NC=NC=2)NC(=O)C(CO)NC(=O)CNC2=O)C(=O)NCC(=O)NC(CCC(O)=O)C(=O)NC(CCCNC(N)=N)C(=O)NCC(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC(O)=CC=3)C(=O)NC(C(C)O)C(=O)N3C(CCC3)C(=O)NC(CCCCN)C(=O)NC(C)C(O)=O)C(=O)NC(CC(N)=O)C(O)=O)=O)NC(=O)C(C(C)CC)NC(=O)C(CO)NC(=O)C(C(C)O)NC(=O)C1CSSCC2NC(=O)C(CC(C)C)NC(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CC(N)=O)NC(=O)C(NC(=O)C(N)CC=1C=CC=CC=1)C(C)C)CC1=CN=CN1 NOESYZHRGYRDHS-UHFFFAOYSA-N 0.000 description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 2
- 241000213006 Angelica dahurica Species 0.000 description 1
- 102000004877 Insulin Human genes 0.000 description 1
- 108090001061 Insulin Proteins 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000003102 growth factor Substances 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229940125396 insulin Drugs 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000001272 neurogenic effect Effects 0.000 description 1
- 230000001575 pathological effect Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- BHMBVRSPMRCCGG-OUTUXVNYSA-N prostaglandin D2 Chemical compound CCCCC[C@H](O)\C=C\[C@@H]1[C@@H](C\C=C/CCCC(O)=O)[C@@H](O)CC1=O BHMBVRSPMRCCGG-OUTUXVNYSA-N 0.000 description 1
- BHMBVRSPMRCCGG-UHFFFAOYSA-N prostaglandine D2 Natural products CCCCCC(O)C=CC1C(CC=CCCCC(O)=O)C(O)CC1=O BHMBVRSPMRCCGG-UHFFFAOYSA-N 0.000 description 1
- 230000001932 seasonal effect Effects 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
Classifications
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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Abstract
The invention discloses a natural herbal composition with hair loss prevention and hair solidification effects, which comprises the following raw materials in parts by weight: 5-10 parts of nettle, 3-5 parts of kudzu root, 2-4 parts of cacumen biotae, 1-3 parts of polygonum multiflorum, 1-3 parts of glossy privet fruit, 1-3 parts of angelica, 1-2 parts of ginseng, 1-2 parts of sophora flavescens, 1-2 parts of fructus forsythiae, 1-2 parts of cordyceps sinensis, 10-20 parts of chitosan dissolution modifier, 20-30 parts of deionized water and 2-6 parts of hydroxyapatite modification synergist. The composition takes various natural herbs as raw materials, and the chitosan penetration modifier and the hydroxyapatite modification synergist are added, so that the raw materials are mutually cooperated and enhanced, the anti-hair loss and hair-fixing effects of the product are enhanced, and compared with the prior art, the composition has a remarkable synergistic effect.
Description
Technical Field
The invention relates to the technical field of hair washing, in particular to a natural herbal composition with hair loss prevention and hair solidification effects, and a preparation method and application thereof.
Background
The types of pathological alopecia that are common at present are: seborrheic alopecia, seasonal alopecia, neurogenic alopecia, and also other types of alopecia such as: alopecia caused by aging alopecia, hair loss due to permanent wave, hair loss due to external environment infection, and in vivo immunity decrease (decrease of insulin growth factor 1 and prostaglandin D2). The scalp of seborrheic alopecia is excessively greasy, and excessive sebum secretion is accumulated around hair follicles, even pressing or blocking Mao Nangkong, which makes normal hair growth obstacle.
The existing natural herbal composition has low efficiency for inhibiting the lipsotrichia and low inhibition degree, and based on the fact that the invention further improves and optimizes the treatment.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a natural herbal composition with hair loss prevention and hair strengthening effects, a preparation method and application thereof, so as to solve the problems in the background technology.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the invention provides a natural herbal composition with hair loss prevention and hair solidification effects, which comprises the following raw materials in parts by weight:
5-10 parts of nettle, 3-5 parts of kudzu root, 2-4 parts of cacumen biotae, 1-3 parts of polygonum multiflorum, 1-3 parts of glossy privet fruit, 1-3 parts of angelica, 1-2 parts of ginseng, 1-2 parts of sophora flavescens, 1-2 parts of fructus forsythiae, 1-2 parts of cordyceps sinensis, 10-20 parts of chitosan dissolution modifier, 20-30 parts of deionized water and 2-6 parts of hydroxyapatite modification synergist.
Preferably, the composition comprises the following raw materials in parts by weight:
7.5 parts of nettle, 4 parts of kudzu root, 3 parts of cacumen biotae, 2 parts of fleece-flower root, 2 parts of glossy privet fruit, 2 parts of angelica, 1.5 parts of ginseng, 1.5 parts of sophora flavescens, 1.5 parts of fructus forsythiae, 1.5 parts of cordyceps sinensis, 15 parts of chitosan dissolution modifier, 25 parts of deionized water and 4 parts of hydroxyapatite modification synergist.
Preferably, the preparation method of the chitosan penetration modifier comprises the following steps:
s01: adding 5-10 parts of chitosan into 20-25 parts of deionized water, then adding 1-5 parts of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into a hydrochloric acid solution according to a weight ratio of 1:5, then adding sodium alginate accounting for 5-10% of the total weight of the nano rectorite and sodium dodecyl sulfate accounting for 1-5%, uniformly stirring, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 5-10% of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
Preferably, the mass fraction of the hydrochloric acid solution is 3-6%.
Preferably, the preparation method of the rice fermentation liquor comprises the following steps: washing rice, draining, adding 4-6 times of deionized water, steaming, adding 10-15 times of deionized water, sealing, fermenting, and collecting fermentation broth to obtain rice fermentation broth.
Preferably, the fermentation temperature is 32-35 ℃, and the fermentation time is 2-5h.
Preferably, the preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into 5-10 times of deionized water, then adding 5-10% of lanthanum sulfate and 1-4% of silane coupling agent, uniformly stirring, then adding 2-5% of sodium alkylsulfonate, fully stirring, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
Preferably, the silane coupling agent is a coupling agent KH560.
The invention provides a preparation method of a natural herbal composition with hair loss prevention and hair solidification effects, which comprises the following steps: sequentially adding the raw materials into a stirrer, stirring at 1000-1500r/min for 10-20min, and stirring to obtain natural herbal composition.
The invention also provides application of the natural herbal composition with the effects of preventing hair loss and strengthening hair in hair washing.
Compared with the prior art, the invention has the following beneficial effects:
the composition takes various natural herbs as raw materials, and the chitosan penetration modifier and the hydroxyapatite modification synergist are added, so that the raw materials are mutually cooperated and enhanced, the anti-hair loss and hair-fixing effects of the product are enhanced, and compared with the prior art, the composition has a remarkable synergistic effect.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to specific embodiments, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The natural herbal composition with the effects of preventing hair loss and strengthening hair disclosed by the embodiment comprises the following raw materials in parts by weight:
5-10 parts of nettle, 3-5 parts of kudzu root, 2-4 parts of cacumen biotae, 1-3 parts of polygonum multiflorum, 1-3 parts of glossy privet fruit, 1-3 parts of angelica, 1-2 parts of ginseng, 1-2 parts of sophora flavescens, 1-2 parts of fructus forsythiae, 1-2 parts of cordyceps sinensis, 10-20 parts of chitosan dissolution modifier, 20-30 parts of deionized water and 2-6 parts of hydroxyapatite modification synergist.
The composition of the embodiment comprises the following raw materials in parts by weight:
7.5 parts of nettle, 4 parts of kudzu root, 3 parts of cacumen biotae, 2 parts of fleece-flower root, 2 parts of glossy privet fruit, 2 parts of angelica, 1.5 parts of ginseng, 1.5 parts of sophora flavescens, 1.5 parts of fructus forsythiae, 1.5 parts of cordyceps sinensis, 15 parts of chitosan dissolution modifier, 25 parts of deionized water and 4 parts of hydroxyapatite modification synergist.
The preparation method of the chitosan dissolution modifier of the embodiment comprises the following steps:
s01: adding 5-10 parts of chitosan into 20-25 parts of deionized water, then adding 1-5 parts of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into a hydrochloric acid solution according to a weight ratio of 1:5, then adding sodium alginate accounting for 5-10% of the total weight of the nano rectorite and sodium dodecyl sulfate accounting for 1-5%, uniformly stirring, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 5-10% of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
The mass fraction of the hydrochloric acid solution in this example was 3 to 6%.
The preparation method of the rice fermentation liquid of the embodiment comprises the following steps: washing rice, draining, adding 4-6 times of deionized water, steaming, adding 10-15 times of deionized water, sealing, fermenting, and collecting fermentation broth to obtain rice fermentation broth.
The fermentation temperature of the embodiment is 32-35 ℃, and the fermentation time is 2-5h.
The preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into 5-10 times of deionized water, then adding 5-10% of lanthanum sulfate and 1-4% of silane coupling agent of the total amount of the hydroxyapatite, uniformly stirring, then adding 2-5% of sodium alkylsulfonate of the total amount of the hydroxyapatite, fully stirring, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
The silane coupling agent of the present example is a coupling agent KH560.
The preparation method of the natural herbal composition with the effects of preventing hair loss and strengthening hair of the embodiment comprises the following steps of: the raw materials are sequentially added into a stirrer to be stirred and mixed fully, the stirring speed is 1000-1500r/min, the stirring time is 10-20min, and the natural herbal composition is obtained after the stirring.
The natural herbal composition with the effects of preventing hair loss and strengthening hair in the embodiment is applied to hair washing.
Example 1.
The natural herbal composition with the effects of preventing hair loss and strengthening hair disclosed by the embodiment comprises the following raw materials in parts by weight:
5 parts of nettle, 3 parts of kudzu root, 2 parts of cacumen biotae, 1 part of fleece-flower root, 1 part of glossy privet fruit, 1 part of Chinese angelica, 1 part of ginseng, 1 part of radix sophorae flavescentis, 1 part of fructus forsythiae, 1 part of cordyceps sinensis, 10 parts of chitosan dissolution modifier, 20 parts of deionized water and 2 parts of hydroxyapatite modification synergist.
The preparation method of the chitosan penetration modifier of the embodiment comprises the following steps:
s01: adding 5 parts of chitosan into 20 parts of deionized water, then adding 1 part of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into a hydrochloric acid solution according to a weight ratio of 1:5, then adding sodium alginate accounting for 5% of the total amount of the nano rectorite and sodium dodecyl sulfate accounting for 1%, stirring uniformly, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 5% of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
The mass fraction of the hydrochloric acid solution in this example was 3%.
The preparation method of the rice fermentation liquid of the embodiment comprises the following steps: washing rice, draining, adding 4-6 times of deionized water, steaming, adding 10 times of deionized water, sealing, fermenting, and collecting fermentation broth to obtain rice fermentation broth.
The fermentation temperature in this example was 32 ℃ and the fermentation time was 2h.
The preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into 5 times of deionized water, then adding lanthanum sulfate accounting for 5 percent of the total amount of the hydroxyapatite and silane coupling agent accounting for 1 percent of the total amount of the hydroxyapatite, stirring uniformly, then adding sodium alkylsulfonate accounting for 2 percent of the total amount of the hydroxyapatite, stirring fully, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
The silane coupling agent of the present example is a coupling agent KH560.
The preparation method of the natural herbal composition with the effects of preventing hair loss and strengthening hair of the embodiment comprises the following steps of: the raw materials are sequentially added into a stirrer to be stirred and mixed fully, the stirring speed is 1000r/min, the stirring time is 10min, and the natural herbal composition is obtained after the stirring.
The natural herbal composition with the effects of preventing hair loss and strengthening hair in the embodiment is applied to hair washing.
Example 2.
The natural herbal composition with the effects of preventing hair loss and strengthening hair disclosed by the embodiment comprises the following raw materials in parts by weight:
10 parts of nettle, 5 parts of kudzu root, 4 parts of cacumen biotae, 3 parts of polygonum multiflorum, 3 parts of glossy privet fruit, 3 parts of angelica, 2 parts of ginseng, 2 parts of sophora flavescens, 2 parts of fructus forsythiae, 2 parts of cordyceps sinensis, 20 parts of chitosan dissolution modifier, 30 parts of deionized water and 6 parts of hydroxyapatite modification synergist.
The preparation method of the chitosan penetration modifier of the embodiment comprises the following steps:
s01: adding 10 parts of chitosan into 25 parts of deionized water, then adding 5 parts of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into a hydrochloric acid solution according to the weight ratio of 1:5, then adding sodium alginate accounting for 10 percent of the total amount of the nano rectorite and sodium dodecyl sulfate accounting for 5 percent of the total amount of the nano rectorite, uniformly stirring, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 10% of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
The mass fraction of the hydrochloric acid solution in this example was 6%.
The preparation method of the rice fermentation liquid of the embodiment comprises the following steps: washing rice, draining, adding 6 times of deionized water, steaming, adding 15 times of deionized water, sealing, fermenting, and collecting fermentation broth to obtain rice fermentation broth.
The fermentation temperature in this example was 35 ℃ and the fermentation time was 5 hours.
The preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into 10 times of deionized water, then adding lanthanum sulfate accounting for 10 percent of the total amount of the hydroxyapatite and silane coupling agent accounting for 4 percent of the total amount of the hydroxyapatite, stirring uniformly, then adding alkyl sodium sulfonate accounting for 5 percent of the total amount of the hydroxyapatite, stirring fully, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
The silane coupling agent of the present example is a coupling agent KH560.
The preparation method of the natural herbal composition with the effects of preventing hair loss and strengthening hair of the embodiment comprises the following steps of: the raw materials are sequentially added into a stirrer to be stirred and mixed fully, the stirring speed is 1500r/min, the stirring time is 20min, and the natural herbal composition is obtained after the stirring.
The natural herbal composition with the effects of preventing hair loss and strengthening hair in the embodiment is applied to hair washing.
Example 3.
The natural herbal composition with the effects of preventing hair loss and strengthening hair disclosed by the embodiment comprises the following raw materials in parts by weight:
7.5 parts of nettle, 4 parts of kudzu root, 3 parts of cacumen biotae, 2 parts of fleece-flower root, 2 parts of glossy privet fruit, 2 parts of angelica, 1.5 parts of ginseng, 1.5 parts of sophora flavescens, 1.5 parts of fructus forsythiae, 1.5 parts of cordyceps sinensis, 15 parts of chitosan dissolution modifier, 25 parts of deionized water and 4 parts of hydroxyapatite modification synergist.
The preparation method of the chitosan dissolution modifier of the embodiment comprises the following steps:
s01: adding 7.5 parts of chitosan into 22.5 parts of deionized water, then adding 3 parts of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into a hydrochloric acid solution according to the weight ratio of 1:5, then adding sodium alginate accounting for 7.5 percent of the total amount of the nano rectorite and sodium dodecyl sulfate accounting for 3 percent of the total amount of the nano rectorite, uniformly stirring, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 7.5 percent of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
The mass fraction of the hydrochloric acid solution in this example was 4.5%.
The preparation method of the rice fermentation liquid of the embodiment comprises the following steps: washing the rice with water, draining, adding 5 times of deionized water, steaming, adding 12.5 times of deionized water, sealing, fermenting, and collecting the fermentation broth to obtain the rice fermentation broth.
The fermentation temperature in this example was 33.5 ℃ and the fermentation time was 3.5h.
The preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into deionized water 7.5 times of the weight of the hydroxyapatite, adding lanthanum sulfate 7.5 percent of the total weight of the hydroxyapatite and silane coupling agent 2.5 percent of the total weight of the hydroxyapatite, uniformly stirring, then adding sodium alkylsulfonate 3.5 percent of the total weight of the hydroxyapatite, fully stirring, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
The silane coupling agent of the present example is a coupling agent KH560.
The preparation method of the natural herbal composition with the effects of preventing hair loss and strengthening hair of the embodiment comprises the following steps of: the raw materials are sequentially added into a stirrer to be stirred and mixed fully, the stirring speed is 1250r/min, the stirring time is 15min, and the natural herbal composition is obtained after the stirring.
The natural herbal composition with the effects of preventing hair loss and strengthening hair in the embodiment is applied to hair washing.
Example 4.
The natural herbal composition with the effects of preventing hair loss and strengthening hair disclosed by the embodiment comprises the following raw materials in parts by weight:
6 parts of nettle, 4 parts of kudzu root, 3 parts of cacumen biotae, 1.2 parts of fleece-flower root, 1.5 parts of glossy privet fruit, 1.5 parts of angelica, 1.5 parts of ginseng, 1 part of radix sophorae flavescentis, 2 parts of fructus forsythiae, 1.5 parts of cordyceps sinensis, 12 parts of chitosan dissolution modifier, 22 parts of deionized water and 3 parts of hydroxyapatite modification synergist.
The preparation method of the chitosan dissolution modifier of the embodiment comprises the following steps:
s01: adding 6 parts of chitosan into 22 parts of deionized water, then adding 2 parts of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into a hydrochloric acid solution according to a weight ratio of 1:5, then adding sodium alginate accounting for 6% of the total amount of the nano rectorite and sodium dodecyl sulfate accounting for 2%, stirring uniformly, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 6% of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
The mass fraction of the hydrochloric acid solution in this example was 4%.
The preparation method of the rice fermentation liquid of the embodiment comprises the following steps: washing the rice with water, draining, adding 5 times of deionized water, steaming, adding 12 times of deionized water, sealing, fermenting, and collecting the fermentation broth to obtain the rice fermentation broth.
The fermentation temperature in this example was 33 ℃ and the fermentation time was 2.2h.
The preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into deionized water 6 times, adding lanthanum sulfate 6% of the total amount of the hydroxyapatite and silane coupling agent 2%, uniformly stirring, adding alkyl sodium sulfonate 3% of the total amount of the hydroxyapatite, fully stirring, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
The silane coupling agent of the present example is a coupling agent KH560.
The preparation method of the natural herbal composition with the effects of preventing hair loss and strengthening hair of the embodiment comprises the following steps of: the raw materials are sequentially added into a stirrer to be stirred and mixed fully, the stirring speed is 1220r/min, the stirring time is 12min, and the natural herbal composition is obtained after the stirring.
The natural herbal composition with the effects of preventing hair loss and strengthening hair in the embodiment is applied to hair washing.
Comparative example 1.
The difference from example 3 is that no chitosan penetration modifier was added.
Comparative example 2.
Unlike example 3, the preparation of the chitosan penetration modifier did not include the addition of the rice fermentation broth.
Comparative example 3.
The difference of the embodiment 3 is that the modified nano rectorite is not added in the preparation of the chitosan dissolution modifier.
Comparative example 4.
The difference from the example 3 is that the modified nano-rectorite is replaced by the rectorite.
Comparative example 5.
The difference from example 3 is that no hydroxyapatite modifying synergist was added.
Selecting 100 testers, dividing 10 testers into one group, taking 10 groups in total, testing the oil content of the scalp by using an oil tester Sebumeter SM815 for the testers in advance, recording the data as D0, then sequentially sending the products prepared in the embodiments 1-5 and the comparative examples 1-5 to each member, washing hair once by adopting the product for two days, testing 10ml each time, lasting for 50 days, testing the oil content of the skin on 14 th day, 28 th day and 50 th day respectively, and recording the data;
the change rate of fat content = { (fat content after use of product-fat content before use of product)/fat content before use of product } × 100%, and the test results are shown in the following table.
As can be seen from examples 1 to 4 and comparative examples 1 to 5; after the product is used, the scalp grease removal effect is remarkable, the removal rate is gradually increased, and meanwhile, the long-acting oil control capacity and the clear scalp capacity of the product are greatly improved;
as seen from comparative examples 1-5, the oil change rate of the product is remarkably deteriorated without adding the chitosan dissolution modifier and without adding the hydroxyapatite modification synergist, and meanwhile, the oil tends to be deteriorated when the preparation methods of the chitosan dissolution modifier are different, and the effect of the product is most remarkable only when the chitosan dissolution modifier prepared by the method is adopted.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (10)
1. The natural herbal composition with the effects of preventing hair loss and fixing hair is characterized by comprising the following raw materials in parts by weight:
5-10 parts of nettle, 3-5 parts of kudzu root, 2-4 parts of cacumen biotae, 1-3 parts of polygonum multiflorum, 1-3 parts of glossy privet fruit, 1-3 parts of angelica, 1-2 parts of ginseng, 1-2 parts of sophora flavescens, 1-2 parts of fructus forsythiae, 1-2 parts of cordyceps sinensis, 10-20 parts of chitosan dissolution modifier, 20-30 parts of deionized water and 2-6 parts of hydroxyapatite modification synergist.
2. The natural herbal composition with hair loss prevention and hair strengthening effects as claimed in claim 1, wherein the composition comprises the following raw materials in parts by weight:
7.5 parts of nettle, 4 parts of kudzu root, 3 parts of cacumen biotae, 2 parts of fleece-flower root, 2 parts of glossy privet fruit, 2 parts of angelica, 1.5 parts of ginseng, 1.5 parts of sophora flavescens, 1.5 parts of fructus forsythiae, 1.5 parts of cordyceps sinensis, 15 parts of chitosan dissolution modifier, 25 parts of deionized water and 4 parts of hydroxyapatite modification synergist.
3. The natural herbal composition with the effects of preventing hair loss and strengthening hair as claimed in claim 1, wherein the chitosan penetration modifier is prepared by the following steps:
s01: adding 5-10 parts of chitosan into 20-25 parts of deionized water, then adding 1-5 parts of rice fermentation liquor, and uniformly stirring;
s02: adding nano rectorite into hydrochloric acid solution according to the weight ratio of 1:5, then adding sodium alginate accounting for 5-10% of the total amount of the nano rectorite and sodium dodecyl sulfate accounting for 1-5%, stirring uniformly, washing with water, and drying to obtain modified nano rectorite;
s03: and then adding 5-10% of modified nano rectorite into the S01 product, and uniformly stirring to obtain the chitosan dissolution modifier.
4. The natural herbal composition with hair loss prevention and hair strengthening effects as claimed in claim 3, wherein the mass fraction of the hydrochloric acid solution is 3-6%.
5. The natural herbal composition with hair loss prevention and hair strengthening effects as claimed in claim 3, wherein the rice fermentation broth is prepared by the following steps: washing rice, draining, adding 4-6 times of deionized water, steaming, adding 10-15 times of deionized water, sealing, fermenting, and collecting fermentation broth to obtain rice fermentation broth.
6. The natural herbal composition with hair loss prevention and hair solidification effects as claimed in claim 5, wherein the fermentation temperature is 32-35 ℃ and the fermentation time is 2-5h.
7. The natural herbal composition with the effects of preventing hair loss and strengthening hair as claimed in claim 1, wherein the preparation method of the hydroxyapatite modified synergistic agent comprises the following steps: feeding hydroxyapatite into 5-10 times of deionized water, then adding 5-10% of lanthanum sulfate and 1-4% of silane coupling agent, uniformly stirring, then adding 2-5% of sodium alkylsulfonate, fully stirring, washing with water, and drying to obtain the hydroxyapatite modified synergistic agent.
8. The natural herbal composition with hair loss prevention and hair solidification effects as claimed in claim 7, wherein the silane coupling agent is a coupling agent KH560.
9. A preparation method of a natural herbal composition with the effects of preventing hair loss and fixing hair is characterized by comprising the following steps: sequentially adding the raw materials into a stirrer, stirring at 1000-1500r/min for 10-20min, and stirring to obtain natural herbal composition.
10. Use of a natural herbal composition for hair loss prevention and hair solidification according to any one of claims 1 to 8 in hair washing.
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