CN115487082A - Antibacterial scrub cream and preparation method thereof - Google Patents
Antibacterial scrub cream and preparation method thereof Download PDFInfo
- Publication number
- CN115487082A CN115487082A CN202211174605.3A CN202211174605A CN115487082A CN 115487082 A CN115487082 A CN 115487082A CN 202211174605 A CN202211174605 A CN 202211174605A CN 115487082 A CN115487082 A CN 115487082A
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- Prior art keywords
- percent
- scrub cream
- antibacterial
- sugar
- antibacterial scrub
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- Cosmetics (AREA)
Abstract
The invention relates to an antibacterial scrub cream and a preparation method thereof, wherein the scrub cream comprises the following components in percentage by weight: 2-5% of lauric acid, 3-10% of stearic acid, 10-30% of glycerol, 0.1-3% of sodium hydroxide, 0.5-5% of ozokerite, 3-10% of fatty alcohol ether sodium sulfate, 10-45% of filler, 25-40% of granular salt, 1-10% of sugar, 0-3% of essence and 0-3% of pigment. The antibacterial scrub cream can effectively sterilize while exfoliating, is easy to disperse when meeting water, and has longer local scrub time; no preservative is added, so that the green and safe effects are achieved; the ointment is stable and can be stored for a long time without adding an emulsifier, and has a good market application prospect.
Description
Technical Field
The invention relates to a solid cosmetic, in particular to an antibacterial scrub cream and a preparation method thereof.
Background
The solid cosmetics are cosmetic products in a solid form in a broad sense, and the solid cosmetics are almost free of tax, so that the solid cosmetics are small in size, light in weight, convenient to transport and carry and more accord with the green and environment-friendly concept.
The scrub cream is an emulsified skin cleaning product containing uniform fine particles, is mainly used for removing dirt in deep layers of skin, and can peel aged scaly cutin by rubbing on the skin to remove dead skin. The scrub cream generally uses sugar or plant particles as a scrub agent, so that bacteria are easy to breed in products, and a preservative is usually added into the scrub cream and is harmful to human bodies whether natural or not.
Patent application CN113616559A discloses a scrub cream, which comprises the following raw materials: scrub agents, base oils, thickeners, and make-up removers; the scrub agent comprises solid sugar and solid alcohol, wherein the solid sugar comprises any one or a combination of at least two of fructose, maltose, glucose, sucrose, lactose, rhamnose, fucooligosaccharide and chitosan, and preferably comprises the combination of sucrose, fucooligosaccharide and rhamnose; the solid alcohol includes any one or a combination of at least two of sorbitol, xylitol, mannitol, maltitol, or erythritol, and is preferably a combination of mannitol, maltitol, and sorbitol. The solid sugar and the solid alcohol are contained, so that the system is easy to solidify to form paste, but the risk of easy bacterial growth and deterioration exists at the same time.
Disclosure of Invention
The invention aims to solve the problems of easy bacteria breeding and deterioration of the existing scrub cream and provides an antibacterial scrub cream. The invention reduces or avoids the use of substances such as saccharides, sugar alcohols and the like which are easy to cause bacterial reproduction, and the granular salt is used as the main grinding force, so that the cutin can be removed and the sterilization can be effectively carried out, thereby having the advantages of no preservative and environmental protection and safety.
However, the introduction of particulate salts makes the preparation of pastes difficult, as determined by the nature of the particulate salts, which do not have a paste morphology and tend to aggregate to form large areas of hard mass.
In order to overcome the problem that a system containing granular salt is difficult to form paste, the inventor tries to adopt dodecanoic acid and octadecanoic acid, wherein the dodecanoic acid and the octadecanoic acid can form hard solids after saponification reaction under an alkaline condition, and the dodecanoic acid and the octadecanoic acid form hard solids after granular salt and sugar are added, so that the use of the scrub cream is not facilitated for consumers, and the hardness requirement of the scrub cream is difficult to meet. Therefore, the inventors have further tried to add ozokerite, and found that the ozokerite and the saponified product are hardly miscible with each other, and the system can be formed into a loose paste, which can give a beautiful appearance and is suitable for consumers to use, thereby completing the present invention.
In the preparation process of the scrub cream, the key is to control the mixing of the water phase and the oil phase, the high-speed stirring is carried out at 30-35rpm, the reaction is kept for 90 minutes, the heat preservation is carried out at 85 +/-5 ℃, a good reaction effect can be realized, and the problems of uneven mixing and layering are avoided. And (3) when the mixed materials are defoamed and protected, adding ozokerite and sodium fatty alcohol polyether sulfate until the mixed materials are completely dissolved without impurities, keeping the temperature at 90 +/-5 ℃ for continuous reaction, and stirring at the speed of 15-20rpm, wherein the mixed materials have a dispersing property preliminarily after the reaction is finished. And finally, cooling, adding salt, sugar and a filling agent, uniformly stirring at the stirring speed of 15-20rpm, and forming loose paste. And adding essence and pigment according to the requirement of the product, and sending the mixture to an aging room for standing and defoaming.
The specific scheme is as follows:
the antibacterial scrub cream comprises the following components in percentage by weight:
2 to 5 percent of dodecanoic acid
Octadecanoic acid 3-10%
10-30% of glycerin
0.1 to 3 percent of sodium hydroxide
0.5 to 5 percent of ozokerite
3-10% of fatty alcohol ether sodium sulfate
10 to 45 percent of filling agent
25-40% of granular salt
1 to 10 percent of sugar
0 to 3 percent of essence
0-3% of pigment.
Further, the composition comprises the following components in percentage by weight:
3 to 4 percent of lauric acid
Octadecanoic acid 5-8%
15-25% of glycerin
0.5 to 2 percent of sodium hydroxide
1 to 3 percent of ozokerite
Fatty alcohol ether sodium sulfate 4-8%
12 to 30 percent of filling agent
30 to 40 percent of granular salt
Sugar 5-10%
0.5 to 1.5 percent of essence
0-2% of pigment.
Further, the composition comprises the following components in percentage by weight:
3 to 4 percent of lauric acid
Octadecanoic acid 5-8%
12-20% of glycerin
1 to 2 percent of sodium hydroxide
1 to 4 percent of ozokerite
3-8% of fatty alcohol ether sodium sulfate
15 to 28 percent of filling agent
32 to 38 percent of granular salt
Sugar 5-7%
0.5 to 1 percent of essence
0 to 0.5 percent of pigment.
Further, the filler is any one of carbomer, polyvinyl alcohol, gelatin, anhydrous sodium sulphate, sodium metasilicate powder or starch; the sugar is any one of glucose, fructose, arabinose, trehalose, D-ribose, agarose, raffinose, lactose or maltose.
Further, the particle size of the granular salt is 0.1-3mm, preferably 1-2mm.
Furthermore, the antibacterial scrub cream is in a loose paste shape, is smeared on skin and is kneaded, and the bacteria removal efficiency on the surface of the skin is more than or equal to 96%.
The invention also provides a preparation method of the antibacterial scrub cream, which comprises the following steps:
(1) Adding dodecanoic acid and octadecanoic acid into an oil pan, heating to 70-75 ℃, and stirring to obtain an oil phase;
(2) Adding glycerol and sodium hydroxide into a water phase pot, heating to 70-75 ℃, and stirring to form a transparent solution to obtain a water phase;
(3) Mixing the water phase and the oil phase, stirring and reacting for 50-120 minutes, and keeping the temperature at 85 +/-5 ℃; after defoaming the reaction product, adding ozokerite and sodium fatty alcohol polyether sulfate, stirring for reaction for 30-120 minutes, keeping the temperature at 90 +/-5 ℃, and then cooling;
(4) Adding granular salt, sugar and a filler into the cooled material, and uniformly stirring; and then adding essence and pigment, aging, standing and defoaming to obtain the antibacterial scrub cream.
Further, in the step (3), the temperature is reduced to 70-80 ℃.
And (4) further, adding essence and pigment when the temperature of the system is reduced to 55 +/-5 ℃ in the step (3).
The invention also protects the application of the antibacterial scrub cream in the field of solid cosmetics.
Has the beneficial effects that:
according to the invention, the scrub cream contains the granular salt, has the effect of removing cutin, and the granular salt also has the bactericidal property, so that the cream can be kept for a long time without adding a preservative.
In addition, the invention enables the system to form loose paste rather than hard solid through the action of ceresin, dodecanoic acid and octadecanoic acid, thereby meeting the hardness requirement of the scrub cream.
Furthermore, the invention also provides a preparation method of the scrub cream, wherein the key is to control the temperature and the reaction time after the oil phase and the water phase are mixed, so that the reaction is complete and the layering is avoided; defoaming is carried out after the reaction is finished, ceresin and sodium fatty alcohol polyether sulfate are added to complete the dissolution, and the ceresin and the sodium fatty alcohol polyether sulfate are difficult to be fully dissolved by early adding.
In a word, the antibacterial scrub cream provided by the invention meets the requirements of consumers, is safe and environment-friendly, has an outstanding cutin removing effect, meets the green and non-toxic requirements, and has a wide application prospect.
Drawings
In order to more clearly illustrate the technical solution of the present invention, the drawings will be briefly introduced, and it is apparent that the drawings in the following description relate only to some embodiments of the present invention and are not limiting to the present invention.
FIG. 1 is a schematic process flow diagram provided in one embodiment 1 of the present invention.
Detailed Description
Preferred embodiments of the present invention will be described in more detail below. While the following describes preferred embodiments of the present invention, it should be understood that the present invention may be embodied in various forms and should not be limited by the embodiments set forth herein. Those skilled in the art will recognize that the specific techniques or conditions, not specified in the examples, are according to the techniques or conditions described in the literature of the art or according to the product specification. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products commercially available. In the following examples, "%" means weight percent, unless otherwise specified.
Examples 1 to 8
The antibacterial scrub cream is prepared by the following main steps in a process flow as shown in figure 1:
1. preparing before production, getting materials, preparing materials, cleaning a machine, checking whether a machine operates normally, preparing in the early production stage, and preparing components according to a table 1; wherein, anhydrous sodium sulphate is adopted as the filler in the examples 1 to 4, and starch is adopted as the filler in the examples 5 to 8. Examples 1-4 where the sugar is glucose and examples 5-8 where the sugar is fructose. The particle size of the adopted granular salt is 1-2mm.
2. Adding dodecanoic acid and octadecanoic acid into an oil pan, heating to 70-75 ℃, and stirring moderately;
3. adding glycerol and sodium hydroxide into a water phase pot, heating to 70-75 ℃ until the glycerol and the sodium hydroxide are completely dissolved and transparent, and stirring at the speed of 15-20rpm;
4. pumping water phase and oil phase, starting high-speed stirring at 30-35rpm, keeping reaction for 90 minutes, and keeping the temperature at 85 +/-5 ℃;
5. after defoaming, adding ozokerite and sodium fatty alcohol polyether sulfate until complete dissolution without impurities, keeping the temperature at 90 +/-5 ℃, stirring at the speed of 15-20rpm, and beginning to cool;
6. adding salt, sugar and filler, stirring uniformly at the stirring speed of 15-20rpm;
7. cooling to 55 + -5 deg.C, adding essence and pigment;
8. checking, namely checking according to requirements;
9. after the product is qualified, the product is sent to an aging room for standing and defoaming;
10. and (5) after standing, filling and packaging.
TABLE 1 Scale for raw materials (weight percent)
Comparative example 1
In addition to example 1, when ozokerite was replaced with the same weight of sodium fatty alcohol polyether sulfate, it was found that it was difficult to form a paste during the preparation, and a hard solid was finally obtained, which was bulky as a whole and could not be used as a scrub cream.
Comparative example 2
In addition to example 1, the granular salt was replaced with refined salt of the same weight, and the grain size of the refined salt was 0.15 to 0.45m.
Performance detection
1. Overall evaluation
The scrub cream prepared in the example was applied to hands, spread evenly for rubbing, and then washed with water, the use feeling was subjectively evaluated, using an evaluation standard of 10 points, 1 point being the worst, 10 points being the best, the higher the point being the better the effect, and 3 samples were evaluated after use, and the results were averaged as shown in table 2.
The scrub cream product prepared by the invention is easy to disperse when meeting water, and has longer local scrub time.
TABLE 2 Overall evaluation Table
| Sample (I) | Sense organ | Frosted feel | Richness of foam |
| Example 1 | 9.8 | 9.5 | 8 |
| Example 2 | 9.6 | 9.7 | 8.5 |
| Example 3 | 9.8 | 9.8 | 9 |
| Example 4 | 9.7 | 9.9 | 9.3 |
| Example 5 | 9.7 | 9.9 | 9.8 |
| Example 6 | 9.7 | 9.9 | 9.6 |
| Example 7 | 9.8 | 9.8 | 9.5 |
| Example 8 | 9.5 | 9.9 | 9.4 |
2. Antibacterial test
Selecting 10 volunteers, sampling 1 with cotton swab hands, washing with the scrub cream prepared in the example, sampling 2 near the sampling 1 with the cotton swab hands, detecting microorganisms according to a method of technical Specification for cosmetic safety 2015 edition, and comparing the microorganisms before and after to obtain a reduction amount; reduction of microorganisms% = number of microorganisms 1-number of microorganisms 2/number of microorganisms 1 x 100%, then take the average).
TABLE 3 antibacterial Property test results Table
The scrub cream is not added with an antibacterial agent and does not belong to a bactericidal product, but the test shows that the scrub cream can wash away microbial colonies from hands and effectively inhibit bacterial reproduction.
3. Exfoliating effect
10 volunteers selected the aged part of the horny layer of the elbow, and the scrub cream prepared in example was used once a day, and comparison was performed after three days, and the results are shown in Table 4.
TABLE 4 exfoliating effect table
| Sample (I) | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 | Comparative example 2 |
| Improving effect | Obviously improve | Obviously improve | Obviously improve | Obviously improve | Obviously improve | Obviously improve | Obviously improve | Without improvement |
The preferred embodiments of the present invention have been described in detail, however, the present invention is not limited to the specific details of the above embodiments, and various simple modifications may be made to the technical solution of the present invention within the technical idea of the present invention, and these simple modifications are within the protective scope of the present invention.
It should be noted that the various features described in the above embodiments may be combined in any suitable manner without departing from the scope of the invention. The invention is not described in detail in order to avoid unnecessary repetition.
In addition, any combination of the various embodiments of the present invention is also possible, and the same should be considered as the disclosure of the present invention as long as it does not depart from the spirit of the present invention.
Claims (10)
1. An antibacterial scrub cream is characterized in that: the composite material comprises the following components in percentage by weight:
2 to 5 percent of dodecanoic acid
Octadecanoic acid 3-10%
10-30% of glycerin
0.1 to 3 percent of sodium hydroxide
0.5 to 5 percent of ozokerite
3-10% of fatty alcohol ether sodium sulfate
10 to 45 percent of filling agent
25-40% of granular salt
1 to 10 percent of sugar
0 to 3 percent of essence
0 to 3 percent of pigment.
2. The antibacterial scrub cream as set forth in claim 1, wherein: the composition comprises the following components in percentage by weight:
3 to 4 percent of dodecanoic acid
Octadecanoic acid 5-8%
15-25% of glycerin
0.5 to 2 percent of sodium hydroxide
1 to 3 percent of ozokerite
Fatty alcohol ether sodium sulfate 4-8%
12 to 30 percent of filling agent
30 to 40 percent of granular salt
Sugar 5-10%
0.5 to 1.5 percent of essence
0 to 2 percent of pigment.
3. The antibacterial scrub cream of claim 1, wherein: the composition comprises the following components in percentage by weight:
3 to 4 percent of dodecanoic acid
Octadecanoic acid 5-8%
12-20% of glycerin
1 to 2 percent of sodium hydroxide
1 to 4 percent of ozokerite
3-8% of fatty alcohol ether sodium sulfate
15 to 28 percent of filling agent
32 to 38 percent of granular salt
Sugar 5-7%
0.5 to 1 percent of essence
0 to 0.5 percent of pigment.
4. An antibacterial scrub cream according to any one of claims 1 to 3, characterized in that: the filler is any one of carbomer, polyvinyl alcohol, gelatin, anhydrous sodium sulphate, acer palmatum powder or starch; the sugar is any one of glucose, fructose, arabinose, trehalose, D-ribose, agarose, raffinose, lactose or maltose.
5. An antibacterial scrub cream according to any one of claims 1 to 3, wherein: the particle size of the granular salt is 0.1-3mm, preferably 1-2mm.
6. An antibacterial scrub cream according to any one of claims 1 to 3, characterized in that: the antibacterial scrub cream is in a loose paste shape, is smeared on skin and is kneaded, and the bacteria removal efficiency on the surface of the skin is more than or equal to 96%.
7. The method of making an antibacterial scrub cream according to any one of claims 1 to 6, wherein the method comprises the steps of: the method comprises the following steps:
(1) Adding dodecanoic acid and octadecanoic acid into an oil pan, heating to 70-75 ℃, and stirring to obtain an oil phase;
(2) Adding glycerol and sodium hydroxide into a water phase pot, heating to 70-75 ℃, and stirring to form a transparent solution to obtain a water phase;
(3) Mixing the water phase and the oil phase, stirring and reacting for 50-120 minutes, and keeping the temperature at 85 +/-5 ℃; after defoaming the reaction product, adding ozokerite and sodium fatty alcohol polyether sulfate, stirring for reaction for 30-120 minutes, keeping the temperature at 90 +/-5 ℃, and then cooling;
(4) Adding granular salt, sugar and a filler into the cooled material, and uniformly stirring; and then adding essence and pigment, aging, standing and defoaming to obtain the antibacterial scrub cream.
8. The method for preparing the antibacterial scrub cream according to claim 7, wherein the method comprises the following steps: and (4) cooling in the step (3) to 70-80 ℃.
9. The method for preparing the antibacterial scrub cream according to claim 8, wherein the method comprises the following steps: and (3) adding essence and pigment when the temperature of the system is reduced to 55 +/-5 ℃.
10. Use of the antibacterial scrub cream according to any one of claims 1 to 6 in the field of solid cosmetics.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211174605.3A CN115487082A (en) | 2022-09-26 | 2022-09-26 | Antibacterial scrub cream and preparation method thereof |
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| CN202211174605.3A CN115487082A (en) | 2022-09-26 | 2022-09-26 | Antibacterial scrub cream and preparation method thereof |
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Application publication date: 20221220 |