CN110812283A - Anti-inflammation sterilization makeup removing cream and preparation method thereof - Google Patents
Anti-inflammation sterilization makeup removing cream and preparation method thereof Download PDFInfo
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- CN110812283A CN110812283A CN201911299772.9A CN201911299772A CN110812283A CN 110812283 A CN110812283 A CN 110812283A CN 201911299772 A CN201911299772 A CN 201911299772A CN 110812283 A CN110812283 A CN 110812283A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention relates to an anti-inflammatory and bactericidal makeup removing cream which is prepared from the following raw materials in parts by weight: phase A component: 20-50 parts of caprylic/capric triglyceride, 5-30 parts of mineral oil, 10-30 parts of a styrene/butadiene copolymer mixed solution, 5-12 parts of oxidized polyethylene, 3-10 parts of microcrystalline wax, 1-7 parts of shea butter, 1-7 parts of coconut oil PEG-10 esters, 1-8 parts of paraffin, 0.2-2 parts of glyceryl monostearate and 0.2-3 parts of stearamide; phase B component: 5-10 parts of PEG-20 triisostearin and 0.01-0.5 part of Pinus densiflora oil; its preparing process is also disclosed. The invention has the advantages that: anti-inflammatory and bactericidal, refreshing and non-greasy, strong makeup removing capability, mildness and moistening.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to an anti-inflammatory bactericidal makeup removing cream and a preparation method thereof.
Background
More and more women choose to use long-lasting make-up-free products, such as 7-hour make-up-free BB cream, waterproof and sweat-resistant eyeliner, and the like. In order to achieve better waterproof and sweat-resistant effects, these products are added with a larger amount of film-forming agent, and therefore are not easy to remove. The purpose of makeup removal is not only to remove residual makeup, but also sweat, sebum secretion, and dirt from the atmosphere that adheres to the skin. The skin care product is difficult to completely remove only by using facial cleanser or makeup remover, so that the nutrient components in the skin care product used subsequently cannot be well absorbed by the skin, even acnes are generated, and the problems of pore blockage, acnes and the like are caused.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides an anti-inflammatory and bactericidal makeup remover which is anti-inflammatory and bactericidal, fresh, clean, not greasy, strong in makeup removing capability, mild and moist and a preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
an anti-inflammatory bactericidal makeup removing cream is prepared from the following raw materials in parts by weight:
phase A component: 20-50 parts of caprylic/capric triglyceride, 5-30 parts of mineral oil, 10-30 parts of a styrene/butadiene copolymer mixed solution, 5-12 parts of oxidized polyethylene, 3-10 parts of microcrystalline wax, 1-7 parts of shea butter, 1-7 parts of coconut oil PEG-10 esters, 1-8 parts of paraffin, 0.2-2 parts of glyceryl monostearate and 0.2-3 parts of stearamide;
phase B component: 5 to 10 parts of PEG-20 triisostearin and 0.01 to 0.5 part of Pinus densiflora oil.
Further, the anti-inflammatory and bactericidal makeup removing cream is prepared from the following raw materials in parts by weight:
phase A component: 25-45 parts of caprylic/capric triglyceride, 10-30 parts of mineral oil, 10-30 parts of a styrene/butadiene copolymer mixed solution, 6-12 parts of oxidized polyethylene, 4-8 parts of microcrystalline wax, 2-6 parts of shea butter, 2-6 parts of coconut oil PEG-10 esters, 2-7 parts of paraffin, 0.5-2 parts of glyceryl monostearate and 0.5-2 parts of stearamide;
phase B component: 6 to 10 parts of PEG-20 triisostearin and 0.01 to 0.2 part of Pinus densiflora oil.
Further, the volume concentration of the styrene/butadiene copolymer mixed solution is 4-8%.
The preparation method of the anti-inflammatory and bactericidal makeup removing cream comprises the following steps:
s1, pre-dissolving a styrene/butadiene copolymer by mineral oil to prepare a styrene/butadiene copolymer mixed solution with the volume concentration of 4-8%;
s2, mixing caprylic/capric triglyceride, mineral oil, a styrene/butadiene copolymer mixed solution, oxidized polyethylene, microcrystalline wax, shea butter, coconut oil PEG-10 esters, paraffin, glyceryl monostearate and stearamide according to a proportion, heating to 80-90 ℃, and stirring until the solid wax is completely dissolved; s3, cooling to 65-75 ℃, adding PEG-20 triisostearin and Pinus densiflora oil, cooling to 48-52 ℃, preserving heat, filling, continuously cooling to 30 ℃, and solidifying the material body into white fine paste.
Further, in step S3, before the heat preservation filling, the obtained product is sampled and inspected, and after the inspection is qualified, the heat preservation filling is performed.
Further, in step S1, when pre-dissolving, mineral oil is poured into the container, and the styrene/butadiene copolymer is added while stirring, and the pre-dissolving is completed within 5-10 min.
Further, in step S2, the stirring speed is 60 to 200 rpm.
Further, in step S2, the stirring speed is gradually decreased until the stirring speed is decreased to 0.
Further, the stirring speed was reduced by 20 revolutions per minute.
Further, in step S3, the temperature reduction process is slow temperature reduction, and the temperature reduction speed is 0.2-0.4 ℃/min.
The invention has the following advantages:
the invention relates to a full-oil paste which meets the storage conditions of commodities (40 ℃ in summer and 10 ℃ in winter), wherein pinus pinaster oil, also called Australian tea tree oil, is added in a formula, and a large number of researches show that the tea tree oil has the effects of antisepsis, antibiosis, antivirus, fungus killing, inflammation diminishing and the like, the Australian tea tree is a plant of melaleuca in Myrtaceae, the research of tea tree science starts in 1920 s, and the tea tree oil is applied to Australian soldiers for treating skin injury during world war II. In all studies, tea tree oil has been shown to have disinfectant properties and to be effective in inhibiting many ubiquitous pathogenic cells and moulds. Modern times we can consider tea tree as a natural disinfectant, and it is very helpful to cure many diseases and wounds. Such as cuts, abrasions, bites by insects, acne, burns, vaginal infections, skin tinea, etc. It is also used to control bacteria and mold in air conditioning systems. The tea tree oil has twelve times stronger disinfection and antibiosis property than phenol which is the most commonly used disinfection and antibiosis agent, so that people can widely apply the tea tree oil to disinfection, sterilization and cleaning products of medicine, dentistry and home. Meanwhile, grease in the formula is mixed with wax to form a thick film, fingers are used for massaging the face in a circling mode, the waterproof product in pores can be removed, the added shea butter and coconut oil enable the skin to be moist after washing, and the surfactant with sufficient quantity also ensures that the makeup remover has excellent makeup removing capability.
Detailed Description
The invention is further described below with reference to examples, but the scope of the invention is not limited to the following.
[ example 1 ]:
an anti-inflammatory bactericidal makeup removing cream is prepared from the following raw materials in parts by weight:
phase A component: 20 parts of caprylic/capric triglyceride, 30 parts of mineral oil, 30 parts of 4% styrene/butadiene copolymer mixed solution, 5 parts of oxidized polyethylene, 10 parts of microcrystalline wax, 1 part of shea butter, 7 parts of coconut oil PEG-10 esters, 1 part of paraffin, 2 parts of glyceryl monostearate and 0.2 part of stearic amide;
phase B component: 10 parts of PEG-20 triisostearin and 0.01 part of pinus thin seed oil.
The preparation method of the anti-inflammatory and bactericidal makeup removing cream comprises the following steps:
s1, pre-dissolving the styrene/butadiene copolymer by mineral oil to prepare a styrene/butadiene copolymer mixed solution with the volume concentration of 4%, pouring the mineral oil into a container during pre-dissolving, adding the styrene/butadiene copolymer while stirring, and completing the pre-dissolving within 10 min;
s2, mixing caprylic/capric triglyceride, mineral oil, a styrene/butadiene copolymer mixed solution, oxidized polyethylene, microcrystalline wax, shea butter, coconut oil PEG-10 esters, paraffin, glyceryl monostearate and stearamide according to a proportion, heating to 90 ℃, and stirring until solid waxes are completely dissolved, wherein the stirring speed is 60rpm, the stirring speed is gradually reduced in the stirring process, and the stirring speed is reduced by 20 revolutions per minute until the stirring speed is reduced to 0;
s3, cooling to 65 ℃, adding PEG-20 triisostearin and Pinus Petasites oil, sampling and inspecting the obtained product when the temperature is reduced to 52 ℃, performing heat preservation filling after the inspection is qualified, performing heat preservation filling, continuously cooling to 30 ℃, slowly cooling in the cooling process, wherein the cooling speed is 0.2 ℃/min, and the material body is solidified into white fine paste.
[ example 2 ]:
an anti-inflammatory bactericidal makeup removing cream is prepared from the following raw materials in parts by weight:
phase A component: 35 parts of caprylic/capric triglyceride, 20 parts of mineral oil, 20 parts of 6% styrene/butadiene copolymer mixed solution, 8 parts of oxidized polyethylene, 7 parts of microcrystalline wax, 4 parts of shea butter, 4 parts of coconut oil PEG-10 esters, 6 parts of paraffin, 1.1 parts of glyceryl monostearate and 1.6 parts of stearic amide;
phase B component: 7.5 parts of PEG-20 triisostearin and 0.3 part of Pinus piniperi oil.
The preparation method of the anti-inflammatory and bactericidal makeup removing cream comprises the following steps:
s1, pre-dissolving the styrene/butadiene copolymer by mineral oil to prepare a styrene/butadiene copolymer mixed solution with the volume concentration of 6%, pouring the mineral oil into a container during pre-dissolving, adding the styrene/butadiene copolymer while stirring, and completing the pre-dissolving within 8 min;
s2, mixing caprylic/capric triglyceride, mineral oil, a styrene/butadiene copolymer mixed solution, oxidized polyethylene, microcrystalline wax, shea butter, coconut oil PEG-10 esters, paraffin, glyceryl monostearate and stearamide according to a proportion, heating to 85 ℃, and stirring until solid waxes are completely dissolved, wherein the stirring speed is 130rpm, and in the stirring process, the stirring speed is gradually reduced, and is reduced by 20 revolutions per minute until the stirring speed is reduced to 0;
s3, cooling to 70 ℃, adding PEG-20 triisostearin and Pinus Petasites oil, sampling and inspecting the obtained product when the temperature is reduced to 50 ℃, performing heat preservation filling after the inspection is qualified, performing heat preservation filling, continuously cooling to 30 ℃, slowly cooling in the cooling process, wherein the cooling speed is 0.3 ℃/min, and the material body is solidified into white fine paste.
[ example 3 ]:
an anti-inflammatory bactericidal makeup removing cream is prepared from the following raw materials in parts by weight:
phase A component: 50 parts of caprylic/capric triglyceride, 25 parts of mineral oil, 20 parts of 6% styrene/butadiene copolymer mixed solution, 5 parts of oxidized polyethylene, 10 parts of microcrystalline wax, 1 part of shea butter, 7 parts of coconut oil PEG-10 esters, 5 parts of paraffin, 1.2 parts of glyceryl monostearate and 2 parts of stearic amide;
phase B component: 7 parts of PEG-20 triisostearin and 0.32 part of pinus pinaster oil.
The preparation method of the anti-inflammatory and bactericidal makeup removing cream comprises the following steps:
s1, pre-dissolving the styrene/butadiene copolymer by mineral oil to prepare a styrene/butadiene copolymer mixed solution with the volume concentration of 4-8%, pouring the mineral oil into a container during pre-dissolving, adding the styrene/butadiene copolymer while stirring, and completing the pre-dissolving within 9 min;
s2, mixing caprylic/capric triglyceride, mineral oil, a styrene/butadiene copolymer mixed solution, oxidized polyethylene, microcrystalline wax, shea butter, coconut oil PEG-10 esters, paraffin, glyceryl monostearate and stearamide according to a proportion, heating to 88 ℃, and stirring until solid waxes are completely dissolved, wherein the stirring speed is 160rpm, the stirring speed is gradually reduced in the stirring process, and the stirring speed is reduced by 20 revolutions per minute until the stirring speed is reduced to 0;
s3, cooling to 72 ℃, adding PEG-20 triisostearin and Pinus Petasites oil, sampling and inspecting the obtained product when the temperature is reduced to 51 ℃, performing heat preservation filling after the inspection is qualified, performing heat preservation filling, continuously cooling to 30 ℃, slowly cooling in the cooling process, wherein the cooling speed is 0.3 ℃/min, and the material body is solidified into white fine paste.
Example 4:
an anti-inflammatory bactericidal makeup removing cream is prepared from the following raw materials in parts by weight:
phase A component: 50 parts of caprylic/capric triglyceride, 5 parts of mineral oil, 10 parts of 8% styrene/butadiene copolymer mixed solution, 12 parts of oxidized polyethylene, 3 parts of microcrystalline wax, 7 parts of shea butter, 1 part of coconut oil PEG-10 esters, 8 parts of paraffin, 0.2 part of glyceryl monostearate and 3 parts of stearic amide;
phase B component: 5 parts of PEG-20 triisostearin and 0.5 part of pinus pinaster oil.
The preparation method of the anti-inflammatory and bactericidal makeup removing cream comprises the following steps:
s1, pre-dissolving the styrene/butadiene copolymer by mineral oil to prepare a styrene/butadiene copolymer mixed solution with the volume concentration of 8%, pouring the mineral oil into a container during pre-dissolving, adding the styrene/butadiene copolymer while stirring, and completing the pre-dissolving within 5 min;
s2, mixing caprylic/capric triglyceride, mineral oil, a styrene/butadiene copolymer mixed solution, oxidized polyethylene, microcrystalline wax, shea butter, coconut oil PEG-10 esters, paraffin, glyceryl monostearate and stearamide according to a proportion, heating to 80 ℃, and stirring until solid waxes are completely dissolved, wherein the stirring speed is 200rpm, the stirring speed is gradually reduced in the stirring process, and the stirring speed is reduced by 20 revolutions per minute until the stirring speed is reduced to 0;
s3, cooling to 75 ℃, adding PEG-20 triisostearin and Pinus Petasites oil, cooling to 48 ℃, sampling and inspecting the obtained product, performing heat preservation filling after the product is qualified, performing heat preservation filling, continuously cooling to 30 ℃, slowly cooling in the cooling process, wherein the cooling speed is 0.4 ℃/min, and the material body is solidified into white fine paste.
The stability tests were carried out for examples 1 to 4, the specific results being shown in the following table:
| example 1 | Example 2 | Example 3 | Example 4 | |
| Heat resistance (48 ℃ C. 24h) | Become thin | Qualified | Qualified | Oil discharge |
| Cold resistance (-15 ℃ C. 24h) | Qualified | Qualified | Become thin | Become thin |
Therefore, example 2 is a preferred embodiment.
Some performance index tests were performed on the test products as follows:
1. appearance: refining the paste;
2. heat resistance stability study (48 ℃ 24 h): qualified;
3. cold stability test (-15 ℃ 24 h): qualified;
evaluation of acne removal efficacy
100 skin lesion test volunteers were selected and tested with the makeup removing cream prepared in example 2, and the judgment standard of curative effect was generally classified according to "clinical research guidelines for dermatological disease of Ministry of health" (GB15797-2002 "hygienic standards for disposable hygienic articles").
The effect is shown: regression of skin lesions > 60%
The face condition was observed after 5 days, 10 days, 20 days and 30 days of use, and the experimental data are as follows:
| time of day | Significant effect/%) |
| 5 days | 30 |
| 10 days | 55 |
| 20 days | 70 |
| 30 days | 85 |
As seen from the table above, the obvious efficiency is as high as 85%, which shows that the makeup removing cream has obvious curative effect on diminishing inflammation and sterilizing.
Evaluation of cleansing ability
The cleansing cream (abbreviated as "a") prepared in example 2 and two cleansing creams B, C commonly used on the market were evaluated from three aspects of cleansing power, rinsing time and skin feel after washing, 100 volunteers were selected, three cleansing creams were used respectively, and the one with the best use effect was selected, and the use effect is shown in the following table:
| item | A | B | C |
| Strong cleaning force | 90/person | 7/person | 3/person |
| The flushing time is fast | 85/person | 10/person | 5/person |
| Skin moistening after washing | 88/person | 6/person | 6/person |
The data in the table show that the makeup removing cream is superior to two makeup removing creams commonly used in the market, and has the characteristics of strong cleaning force, quick rinsing time, mildness and moistening
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. An anti-inflammatory bactericidal makeup removing cream is characterized in that: the feed is prepared from the following raw materials in parts by weight:
phase A component: 20-50 parts of caprylic/capric triglyceride, 5-30 parts of mineral oil, 10-30 parts of a styrene/butadiene copolymer mixed solution, 5-12 parts of oxidized polyethylene, 3-10 parts of microcrystalline wax, 1-7 parts of shea butter, 1-7 parts of coconut oil PEG-10 esters, 1-8 parts of paraffin, 0.2-2 parts of glyceryl monostearate and 0.2-3 parts of stearamide;
phase B component: 5 to 10 parts of PEG-20 triisostearin and 0.01 to 0.5 part of Pinus densiflora oil.
2. The anti-inflammatory and bactericidal makeup removing cream according to claim 1, characterized in that: the feed is prepared from the following raw materials in parts by weight:
phase A component: 25-45 parts of caprylic/capric triglyceride, 10-30 parts of mineral oil, 10-30 parts of a styrene/butadiene copolymer mixed solution, 6-12 parts of oxidized polyethylene, 4-8 parts of microcrystalline wax, 2-6 parts of shea butter, 2-6 parts of coconut oil PEG-10 esters, 2-7 parts of paraffin, 0.5-2 parts of glyceryl monostearate and 0.5-2 parts of stearamide;
phase B component: 6 to 10 parts of PEG-20 triisostearin and 0.01 to 0.2 part of Pinus densiflora oil.
3. The anti-inflammatory and bactericidal makeup removing cream according to claim 1 or 2, characterized in that: the volume concentration of the styrene/butadiene copolymer mixed solution is 4-8%.
4. The method for preparing the anti-inflammatory and bactericidal makeup removing cream as claimed in any one of claims 1 to 3, wherein the method comprises the following steps: the method comprises the following steps:
s1, pre-dissolving a styrene/butadiene copolymer by mineral oil to prepare a styrene/butadiene copolymer mixed solution with the volume concentration of 4-8%;
s2, mixing caprylic/capric triglyceride, mineral oil, a styrene/butadiene copolymer mixed solution, oxidized polyethylene, microcrystalline wax, shea butter, coconut oil PEG-10 esters, paraffin, glyceryl monostearate and stearamide according to a proportion, heating to 80-90 ℃, and stirring until the solid wax is completely dissolved;
s3, cooling to 65-75 ℃, adding PEG-20 triisostearin and Pinus densiflora oil, cooling to 48-52 ℃, preserving heat, filling, continuously cooling to 30 ℃, and solidifying the material body into white fine paste.
5. The method for preparing the anti-inflammatory and bactericidal makeup removing cream according to claim 4 is characterized in that: in step S3, before heat preservation filling, sampling inspection is carried out on the obtained product, and heat preservation filling is carried out after the inspection is qualified.
6. The method for preparing the anti-inflammatory and bactericidal makeup removing cream according to claim 4 is characterized in that: in the step S1, when the mineral oil is pre-dissolved, the mineral oil is poured into a container, and the styrene/butadiene copolymer is added while stirring, and the pre-dissolving is completed within 5-10 min.
7. The method for preparing the anti-inflammatory and bactericidal makeup removing cream according to claim 4 is characterized in that: in step S2, the stirring speed is 60 to 200 rpm.
8. The method for preparing the anti-inflammatory and bactericidal makeup removing cream according to claim 7 is characterized in that: in step S2, the stirring speed is gradually decreased until the stirring speed is decreased to 0.
9. The method for preparing the anti-inflammatory and bactericidal makeup removing cream according to claim 8, which is characterized by comprising the following steps: the stirring speed was reduced by 20 revolutions per minute.
10. The method for preparing the anti-inflammatory and bactericidal makeup removing cream according to claim 8, which is characterized by comprising the following steps: in step S3, the temperature reduction process is slow temperature reduction, and the temperature reduction speed is 0.2-0.4 ℃/min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911299772.9A CN110812283A (en) | 2019-12-17 | 2019-12-17 | Anti-inflammation sterilization makeup removing cream and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911299772.9A CN110812283A (en) | 2019-12-17 | 2019-12-17 | Anti-inflammation sterilization makeup removing cream and preparation method thereof |
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| CN110812283A true CN110812283A (en) | 2020-02-21 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113398057A (en) * | 2020-12-22 | 2021-09-17 | 重庆中佳信健康管理有限公司 | Bacteriostatic agent and preparation method thereof |
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Application publication date: 20200221 |
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