CN115429720B - Extremely simple lipstick and preparation method thereof - Google Patents

Extremely simple lipstick and preparation method thereof Download PDF

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Publication number
CN115429720B
CN115429720B CN202111180238.3A CN202111180238A CN115429720B CN 115429720 B CN115429720 B CN 115429720B CN 202111180238 A CN202111180238 A CN 202111180238A CN 115429720 B CN115429720 B CN 115429720B
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Prior art keywords
synthetic wax
lipstick
solid synthetic
solid
wax
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CN115429720A (en
Inventor
黄旭敏
李代荣
郎鹏
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Guangzhou Hua Chu Xian Biotech Co ltd
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Guangzhou Hua Chu Xian Biotech Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention relates to the technical field of IPC A61K8/00, in particular to a very simple lipstick and a preparation method thereof. The raw material of the very simple lipstick only contains synthetic wax. The extremely simple lipstick provided by the invention has the following advantages: the composition is extremely simple: the product contains only one component of the synthetic wax, and has simple components and good sensory experience; the mechanical strength is high: the synthetic wax with specific penetration and viscosity is selected to act, so that the anti-falling and folding-resisting performances of the lipstick are improved, and the service life of the lipstick is effectively prolonged; the use experience is good: the synthetic waxes with 3 forms are selected to act together, so that the problem that the mechanical strength and the use comfort of the lipstick are difficult to balance is solved, excellent use experience is provided for the lipstick, and the obtained lipstick is warm, smooth and has long-acting skin moisturizing and nourishing effects on lips; the temperature resistance is strong: the obtained lipstick has a melting point of more than 60 ℃, excellent high temperature resistance, difficult softening of paste, strong practicability and wide application prospect in the lipstick field.

Description

Extremely simple lipstick and preparation method thereof
Technical Field
The invention relates to the technical field of IPC A61K8/00, in particular to a very simple lipstick and a preparation method thereof.
Background
The existing lipstick is generally formed by mixing raw materials such as wax, grease, essence and the like, on one hand, the production process is complex, on the other hand, the compatibility among different components is difficult to control, and the obtained lipstick has poor mechanical strength and poor anti-falling and folding resistance. In order to improve the mechanical strength of the lipstick in the prior art, 2-3 solid synthetic waxes are usually added into the raw materials, but the solid synthetic waxes are dry, and have poor spreadability and moist property when being smeared on lips, so that comfortable sensory experience is difficult to provide for consumers when the lipstick is used; the existing lipstick has poor temperature resistance, is easy to soften at high temperature and has short service life, and the defects limit popularization and application of the lipstick.
Chinese patent CN107281031 discloses a long-acting moisturizing and nourishing lip balm for repairing damage and a preparation method thereof, and uses the combined action of vegetable oil, synthetic wax, synthetic fat, antioxidant and the like to obtain a lip balm capable of relieving chapping and peeling of lips; chinese patent CN109125138 discloses a moisturizing high-gloss lipstick and a preparation method thereof, wherein microcrystalline wax, polyethylene wax, synthetic wax and the like are used as thickening agents to act together with wild soybean oil, carrot root extract and the like to obtain the lipstick with high glossiness and good moisturizing degree. However, these prior arts are complicated in composition and do not solve the above-mentioned problems.
Under the background, the invention develops a very simple lipstick, the back mark component of the very simple lipstick only comprises 1 INCI raw material (synthetic wax), and a plurality of synthetic waxes are compounded in the specific implementation process, so that the technical problems that the lipstick in the prior art is complex in component, and the mechanical strength and the use experience are difficult to balance are solved.
Disclosure of Invention
The invention provides the extremely simple lipstick, solves the technical problems of complex components, easy softening and breaking and the like of the lipstick in the prior art, and realizes the lipstick with extremely simple components and excellent use experience.
In order to solve the above problems, a first aspect of the present invention provides a very simple lipstick. In a first aspect, the present invention provides a lip balm comprising synthetic wax as a raw material.
In some preferred embodiments, the synthetic wax is specifically a mixture of a solid synthetic wax, a semi-solid synthetic wax, and a liquid synthetic wax.
In some preferred embodiments, the solid synthetic wax, the semi-solid synthetic wax and the liquid synthetic wax are present in a weight ratio of (0.1 to 60): (0.5-35): (20-90).
Further preferably, the weight ratio of the solid synthetic wax, the semisolid synthetic wax and the liquid synthetic wax is (0.4 to 50): (1-30): (30-85).
Still more preferably, the weight ratio of the solid synthetic wax, the semi-solid synthetic wax and the liquid synthetic wax is 16.3:15.2:68.5.
in some preferred embodiments, the solid synthetic wax has a penetration of 10 to 40dmm and a viscosity of 1 to 12cps.
In some preferred embodiments, the solid synthetic waxes include a first solid synthetic wax, a second solid synthetic wax, and a third solid synthetic wax.
In order to improve the toughness and the anti-falling property of the lipstick and simultaneously maintain better smearing performance, the weight ratio of the first solid synthetic wax to the second solid synthetic wax to the third solid synthetic wax is (0.1-10): (0.1-10): (0.1-15); preferably 2.6:2.6:4.5. The invention discovers that the specific solid synthetic waxes with the following penetration and viscosity are adopted to perform combined action, so that the lipstick material can be endowed with stronger molecular cohesion and stronger mechanical property; however, the improvement of the mechanical property of the lipstick is often accompanied by drier use feeling, and the lipstick is not easy to smear; according to the invention, a large number of experiments prove that on the basis of 3 solid synthetic waxes, the sensory experience of the lipstick can be optimized by simultaneously matching with the effect of the fourth solid synthetic wax with the gel point of 40-55 ℃ and the penetration of 40-80dmm, so that the toughness and the folding resistance of the lipstick are improved, and the lipstick has dry, non-sticky and easy-to-paint experience.
In some preferred embodiments, the first solid synthetic wax has a penetration of 20 to 35dmm and a viscosity of 6 to 10cps.
In some preferred embodiments, the second solid synthetic wax has a penetration of 15 to 30dmm and a viscosity of 4 to 6cps.
In some preferred embodiments, the third solid synthetic wax has a penetration of 10 to 20dmm and a viscosity of 2 to 5cps.
Note that: the penetration test temperature was 25 ℃; the test temperature for viscosity was 99 ℃.
Preferably, the first solid synthetic wax has a penetration of 25dmm and a viscosity of 8.0cps; specifically PERFORMALENE M90 WAX, available from Bekkes corporation (Baker Hughes) of America.
Preferably, the second solid synthetic wax has a penetration of 25dmm and a viscosity of 4.5cps; specifically, PERFORMANENE M80 WAX; from Bekkes corporation (Baker Hughes) of America.
Preferably, the penetration of the third solid synthetic wax is 20dmm and the viscosity is 4.0cps; specifically, PERFORMANEE M70 WAX; from Bekkes corporation (Baker Hughes) of America.
In some preferred embodiments, the solid synthetic wax further comprises a fourth solid synthetic wax; the weight ratio of the fourth solid synthetic wax to the first solid synthetic wax is (3-8): (1-3); preferably 6.6:2.6.
In some preferred embodiments, the fourth solid synthetic wax has a gel point of 40-55deg.C, a penetration of 40-80dmm, and an oil content of 3 wt.% or less.
Further preferably, the fourth solid synthetic wax has a gel point of 48 ℃, a penetration of 62dmm, and an oil content of 1.4wt%; specifically SW46, available from Shanghai Rong Zhi materials technologies, inc.
Note that: the gel point test method is ASTM D938; the penetration test method is ASTM D1321; the oil content was tested by ASTM D721; the drop melting point test method is ASTM D127.
In order to optimize the compatibility of the synthetic wax, it is preferable that the semi-solid synthetic wax has a drop melting point of 30 to 40 ℃ and a gel point of 28 to 40 ℃. The invention discovers that the addition of the synthetic wax with the specification can endow the synthetic wax with the advantages of smoothness and softness and easy melting during application; meanwhile, the obtained synthetic wax can be dissolved in a short time, so that the problems that raw materials are not easy to soften at high temperature and are difficult to dry and melt when the lipstick is prepared are solved.
Further preferably, the semi-solid synthetic wax has a drop melting point of 38.3 ℃ and a gel point of 32 ℃; and in particular SW3254, from Shanghai Rong Zhi materials technology Co., ltd.
In order to enhance the comfort, spreadability and moisturization of the synthetic wax composition, it is preferable that the relative density of the liquid synthetic wax is 0.8 to 0.9g/cm 3 (16 ℃) a kinematic viscosity of 500-1200cSt. According to the invention, when the liquid synthetic wax is added and the addition amount is controlled to be 30-85wt% of the total weight of the system, a waterproof film with firm adhesiveness can be formed on the surface of the lip, so that the effects of water locking, moistening and moisturizing are provided for the lip, and the use experience of the lipstick is further optimized; more importantly, the synthetic wax with the specification is compounded, the obtained lipstick has lasting use effect, the moisturizing and skin care effects can be up to more than 8 hours, and the lipstick with excellent use feeling is obtained under a very simple formula system, and has high cost performance and strong practicability. The successful research and development of the lipstick solves the problems that the existing lipstick is not easy to soften at high temperature, and the mechanical strength and the use experience feel are difficult to balance, and has the advantages of strong toughness, falling resistance, folding resistance, warmth, smoothness, easy application and the like.
Further preferably, the liquid synthetic wax has a relative density of 0.86.+ -. 0.01g/cm3 (16 ℃ C.) and a kinematic viscosity of 800.+ -. 200cSt (32 ℃ C.). Specifically PERFORMA V825, available from Bekkes corporation (Baker Hughes) of America.
In some preferred embodiments, the lip balm has a melting point of 50-70 ℃.
In a second aspect, the present invention provides a method for preparing a lip balm, comprising: adding the synthetic wax raw materials into a stirring device according to the formula amount, uniformly stirring at 90-115 ℃, preserving heat for 10-20min, discharging, and cooling to obtain the finished product.
In some preferred embodiments, the stirring speed is 350-600r/min.
Further preferably, the stirring speed is 400-500r/min.
The beneficial effects are that:
the extremely simple lipstick provided by the invention has the following advantages:
(1) The composition is extremely simple: the product contains only one component of the synthetic wax, and has simple components and good sensory experience;
(2) The mechanical strength is high: the synthetic wax with specific penetration and viscosity is selected to act, so that the anti-falling and folding-resisting performances of the lipstick are improved, and the service life of the lipstick is effectively prolonged;
(3) The use experience is good: the synthetic wax with 3 forms is selected to act together, so that the problem that the mechanical strength and the use comfort of the lipstick are difficult to balance is solved, the excellent use experience of the lipstick is provided while the toughness of the lipstick is optimized, the obtained lipstick is warm and smooth and easy to smear, and has long-acting skin moisturizing, moisturizing and nourishing effects on lips;
(4) The temperature resistance is strong: the obtained lipstick has a melting point of more than 60 ℃, excellent high temperature resistance, difficult softening of paste, strong practicability and wide application prospect in the lipstick field.
Detailed Description
Example 1.
The present embodiment provides a very simple lipstick, wherein the synthetic wax is specifically a mixture of solid synthetic wax, semi-solid synthetic wax and liquid synthetic wax.
The solid synthetic wax and the semisolid synthetic wax respectively account for 16.3 weight percent, 15.2 weight percent and the liquid synthetic wax accounts for the balance of the total weight of the lipstick.
The solid synthetic waxes include a first solid synthetic wax, a second solid synthetic wax, a third solid synthetic wax, and a fourth solid synthetic wax.
The weight ratio of the first solid synthetic wax to the second solid synthetic wax to the third solid synthetic wax to the fourth solid synthetic wax is 2.6:2.6:4.5:6.6.
note that: the penetration test temperature was 25 ℃; the test temperature for viscosity was 99 ℃.
The first solid synthetic wax has a penetration of 25dmm and a viscosity of 8.0cps; specifically PERFORMALENE M90 WAX, available from Bekkes corporation (Baker Hughes) of America.
The penetration of the second solid synthetic wax is 25dmm and the viscosity is 4.5cps; specifically, PERFORMANENE M80 WAX; from Bekkes corporation (Baker Hughes) of America.
The penetration of the third solid synthetic wax is 20dmm and the viscosity is 4.0cps; specifically, PERFORMANEE M70 WAX; from Bekkes corporation (Baker Hughes) of America.
The gel point of the fourth solid synthetic wax is 48 ℃, the penetration is 62dmm, and the oil content is 1.4wt%; specifically SW46, available from Shanghai Rong Zhi materials technologies, inc.
Note that: the gel point test method is ASTM D938; the penetration test method is ASTM D1321; the oil content was tested by ASTM D721; the drop melting point test method is ASTM D127.
The drop melting point of the semisolid synthetic wax is 38.3 ℃ and the gel point is 32 ℃; and in particular SW3254, from Shanghai Rong Zhi materials technology Co., ltd.
The relative density of the liquid synthetic wax is 0.86+/-0.01 g/cm 3 (16 ℃) a kinematic viscosity of 800.+ -. 200cSt (32 ℃); specifically PERFORMA V825, available from Bekkes corporation (Baker Hughes) of America.
In a second aspect, the present embodiment provides a method for preparing the very simple lipstick, where the steps for preparing the very simple lipstick include: adding the synthetic wax raw materials into a stirring device according to the formula amount, uniformly stirring at 105 ℃, preserving heat for 15min, discharging the materials into a stainless steel container, and cooling to obtain a finished product.
The stirring speed is 450r/min.
Example 2.
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax comprises 10.3wt% of the total weight of the lipstick.
The weight ratio of the first solid synthetic wax, the second solid synthetic wax, the third solid synthetic wax and the fourth solid synthetic wax is 0.1:10:0.1:0.1.
example 3.
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax comprises 25.2wt% of the total weight of the lipstick.
The weight ratio of the first solid synthetic wax to the second solid synthetic wax to the third solid synthetic wax to the fourth solid synthetic wax is 10:0.1:0.1:15.
example 4.
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax and the semisolid synthetic wax respectively account for 16.8 weight percent and 1 weight percent of the total weight of the lipstick.
The weight ratio of the first solid synthetic wax, the second solid synthetic wax, the third solid synthetic wax and the fourth solid synthetic wax is 0.1:0.1:10:6.6.
Example 5
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax and the semisolid synthetic wax respectively account for 17.1 weight percent and 30 weight percent of the total weight of the lipstick.
The weight ratio of the first solid synthetic wax, the second solid synthetic wax, the third solid synthetic wax and the fourth solid synthetic wax is 0.5:2:8:6.6.
Example 6.
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax and the liquid synthetic wax respectively account for 22 weight percent and 30 weight percent of the total weight of the lipstick, and the semisolid synthetic wax is filled in the balance.
The weight ratio of the first solid synthetic wax to the second solid synthetic wax to the third solid synthetic wax to the fourth solid synthetic wax is 4:1:2:15.
Example 7.
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax and the liquid synthetic wax respectively account for 9.1 weight percent and 85 weight percent of the total weight of the lipstick, and the semisolid synthetic wax is filled in the balance.
The weight ratio of the first solid synthetic wax to the second solid synthetic wax to the third solid synthetic wax to the fourth solid synthetic wax is 3:4:2: :0.1.
Example 8.
This example provides a very simple lipstick, the specific embodiment of which is the same as example 1; the difference is that: the solid synthetic wax and the liquid synthetic wax respectively account for 15.1 weight percent and 65 weight percent of the total weight of the lipstick, and the semisolid synthetic wax is filled in the balance.
The weight ratio of the first solid synthetic wax to the second solid synthetic wax to the third solid synthetic wax to the fourth solid synthetic wax is 3:0.1:2:10.
Comparative example 1.
This comparative example provides a very simple lipstick, the embodiment is the same as example 1; the difference is that: the first solid synthetic wax was absent, and the solid synthetic wax accounted for 13.7wt% of the total weight of the lipstick.
Comparative example 2.
This comparative example provides a very simple lipstick, the embodiment is the same as example 1; the difference is that: the second solid synthetic wax was absent, the solid synthetic wax comprising 13.7wt% of the total weight of the lipstick.
Comparative example 3.
This comparative example provides a very simple lipstick, the embodiment is the same as example 1; the difference is that: the third solid synthetic wax was absent, the solid synthetic wax comprising 11.8wt% of the total weight of the lipstick.
Performance test method
1. Sensory evaluation
Sensory evaluation tests were performed by 33 evaluators (each group of example/comparative example 3). Each sample was applied to the lips, and the evaluators tried once a day, and scored after 8 hours of use according to the following rating absolute evaluation after usual life; after 1 week of continuous use, the daily score results were summarized to calculate an average value, which is recorded in table 1.
Higher scores indicate better experience.
2. Melting point
The melting points of the lipsticks provided in examples and comparative examples were measured using a rice melting point apparatus, and 3 parallel samples were measured for each group of examples/comparative examples, and the average values thereof are recorded in table 2.
Performance test data
Table 1.
Comfort level Spreadability of Degree of moistening
Example 1 9.3 9.3 8.6
Example 2 8.6 8 8.2
Example 3 8 8.3 7.8
Example 4 7.8 8.6 8.4
Example 5 8.6 8.6 8.8
Example 6 8.3 8 8.6
Example 7 8.3 8.4 8.2
Example 8 8.5 8.4 8.4
Comparative example 1 6 7.6 6.2
Comparative example 2 5.2 6.4 7
Comparative example 3 6.2 7.4 6.8
Table 2.
Melting point (. Degree. C.)
Example 1 66.7
Example 2 62.3
Example 3 66.4
Example 4 58.6
Example 5 60.5
Example 6 66.2
Example 7 62.3
Example 8 55.8
Comparative example 1 52.2
Comparative example 2 54.7
Comparative example 3 56.8

Claims (3)

1. A very simple lipstick is characterized in that the raw materials only contain synthetic wax;
the synthetic wax is specifically solid synthetic wax, a mixture of semisolid synthetic wax and liquid synthetic wax;
the weight ratio of the solid synthetic wax, the semisolid synthetic wax and the liquid synthetic wax is (0.1-60): (0.5-35): (20-90);
the solid synthetic wax consists of a first solid synthetic wax, a second solid synthetic wax, a third solid synthetic wax and a fourth solid synthetic wax;
the weight ratio of the first solid synthetic wax, the second solid synthetic wax and the third solid synthetic wax is (0.1-10): (0.1-10): (0.1-15);
the first solid synthetic wax has a penetration of 25dmm and a viscosity of 8.0cps;
the penetration of the second solid synthetic wax is 25dmm and the viscosity is 4.5cps;
the penetration of the third solid synthetic wax is 20dmm and the viscosity is 4.0cps;
the gel point of the fourth solid synthetic wax is 48 ℃, the penetration is 62dmm, and the oil content is 1.4wt%;
the weight ratio of the fourth solid synthetic wax to the first solid synthetic wax is (3-8): (1-3);
the drop melting point of the semisolid synthetic wax is 30-40 ℃, and the gel point is 28-40 ℃;
the relative density of the liquid synthetic wax is 0.8-0.9g/cm 3 The kinematic viscosity is 500-1200cSt;
the melting point of the very simple lipstick is 50-70 ℃.
2. A method of preparing a lip balm according to claim 1, comprising the steps of: adding the synthetic wax raw materials into a stirring device according to the formula amount, uniformly stirring at 90-115 ℃, preserving heat for 10-20min, discharging, and cooling to obtain the finished product.
3. The method for preparing a very simple lipstick according to claim 2, wherein said stirring speed is 350-600r/min.
CN202111180238.3A 2021-10-11 2021-10-11 Extremely simple lipstick and preparation method thereof Active CN115429720B (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1378833A (en) * 2001-03-21 2002-11-13 株式会社资生堂 Solid cosmetic
US6503516B1 (en) * 1998-11-06 2003-01-07 L'oreal S.A. Make-up composition containing a blend of waxes
WO2008065739A1 (en) * 2006-11-28 2008-06-05 Shiseido Company, Ltd. Stick-type cosmetic preparation
CN101563060A (en) * 2006-12-20 2009-10-21 雅芳产品公司 High gloss gel-based lipstick
CN109939017A (en) * 2019-04-30 2019-06-28 广东三好科技有限公司 One kind pure oil lipstick product having repairing effect and preparation method thereof
WO2021081859A1 (en) * 2019-10-31 2021-05-06 L'oreal Solid anhydrous composition for caring for and/or making up keratin materials

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011028328A1 (en) * 2009-09-03 2011-03-10 Avon Products, Inc. Stabilized wax compositions and uses thereof
US10342756B2 (en) * 2016-06-13 2019-07-09 Carma Laboratories, Inc. Hydrating lip balm composition

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6503516B1 (en) * 1998-11-06 2003-01-07 L'oreal S.A. Make-up composition containing a blend of waxes
CN1378833A (en) * 2001-03-21 2002-11-13 株式会社资生堂 Solid cosmetic
WO2008065739A1 (en) * 2006-11-28 2008-06-05 Shiseido Company, Ltd. Stick-type cosmetic preparation
CN101563060A (en) * 2006-12-20 2009-10-21 雅芳产品公司 High gloss gel-based lipstick
CN109939017A (en) * 2019-04-30 2019-06-28 广东三好科技有限公司 One kind pure oil lipstick product having repairing effect and preparation method thereof
WO2021081859A1 (en) * 2019-10-31 2021-05-06 L'oreal Solid anhydrous composition for caring for and/or making up keratin materials

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