CN115281296A - Preparation method of honeysuckle and forsythia suspense leaf compound beverage - Google Patents
Preparation method of honeysuckle and forsythia suspense leaf compound beverage Download PDFInfo
- Publication number
- CN115281296A CN115281296A CN202210946145.5A CN202210946145A CN115281296A CN 115281296 A CN115281296 A CN 115281296A CN 202210946145 A CN202210946145 A CN 202210946145A CN 115281296 A CN115281296 A CN 115281296A
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- Prior art keywords
- honeysuckle
- water
- forsythia suspense
- beverage
- forsythia
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- 241000205585 Aquilegia canadensis Species 0.000 title claims abstract description 103
- 235000013361 beverage Nutrition 0.000 title claims abstract description 91
- 150000001875 compounds Chemical class 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 241000555682 Forsythia x intermedia Species 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 151
- 241000555712 Forsythia Species 0.000 claims abstract description 98
- 239000000341 volatile oil Substances 0.000 claims abstract description 59
- 239000003921 oil Substances 0.000 claims abstract description 52
- 238000004821 distillation Methods 0.000 claims abstract description 38
- 239000000284 extract Substances 0.000 claims abstract description 32
- 239000000463 material Substances 0.000 claims abstract description 28
- 239000002131 composite material Substances 0.000 claims abstract description 15
- 239000000706 filtrate Substances 0.000 claims description 47
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- 238000007865 diluting Methods 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 10
- 241000576429 Forsythia suspensa Species 0.000 claims description 9
- 230000000694 effects Effects 0.000 abstract description 19
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- KFFCKOBAHMGTMW-LGQRSHAYSA-N Forsythin Chemical compound C1=C(OC)C(OC)=CC=C1[C@H]1[C@@H](CO[C@@H]2C=3C=C(OC)C(O[C@H]4[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O4)O)=CC=3)[C@@H]2CO1 KFFCKOBAHMGTMW-LGQRSHAYSA-N 0.000 description 7
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
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- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 3
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 description 3
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- 125000003118 aryl group Chemical group 0.000 description 3
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 description 3
- 229940074393 chlorogenic acid Drugs 0.000 description 3
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 description 3
- 235000001368 chlorogenic acid Nutrition 0.000 description 3
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 230000036039 immunity Effects 0.000 description 3
- 230000001603 reducing effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- JMGZEFIQIZZSBH-UHFFFAOYSA-N Bioquercetin Natural products CC1OC(OCC(O)C2OC(OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5)C(O)C2O)C(O)C(O)C1O JMGZEFIQIZZSBH-UHFFFAOYSA-N 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 2
- DTOUWTJYUCZJQD-UJERWXFOSA-N Forsythiaside Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1OC[C@@H]1[C@@H](OC(=O)\C=C\C=2C=C(O)C(O)=CC=2)[C@H](O)[C@@H](O)[C@H](OCCC=2C=C(O)C(O)=CC=2)O1 DTOUWTJYUCZJQD-UJERWXFOSA-N 0.000 description 2
- 206010037660 Pyrexia Diseases 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
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- 230000036772 blood pressure Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- IVTMALDHFAHOGL-UHFFFAOYSA-N eriodictyol 7-O-rutinoside Natural products OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C=C3C(C(C(O)=C(O3)C=3C=C(O)C(O)=CC=3)=O)=C(O)C=2)O1 IVTMALDHFAHOGL-UHFFFAOYSA-N 0.000 description 2
- 206010022000 influenza Diseases 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 201000009240 nasopharyngitis Diseases 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- FDRQPMVGJOQVTL-UHFFFAOYSA-N quercetin rutinoside Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 FDRQPMVGJOQVTL-UHFFFAOYSA-N 0.000 description 2
- 235000005493 rutin Nutrition 0.000 description 2
- IKGXIBQEEMLURG-BKUODXTLSA-N rutin Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@@H]1OC[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-BKUODXTLSA-N 0.000 description 2
- ALABRVAAKCSLSC-UHFFFAOYSA-N rutin Natural products CC1OC(OCC2OC(O)C(O)C(O)C2O)C(O)C(O)C1OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5 ALABRVAAKCSLSC-UHFFFAOYSA-N 0.000 description 2
- 229960004555 rutoside Drugs 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000010025 steaming Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 241001655769 Androsace Species 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 240000006740 Cichorium endivia Species 0.000 description 1
- 241000711573 Coronaviridae Species 0.000 description 1
- DTOUWTJYUCZJQD-QJDQKFITSA-N Forsythiaside Natural products C[C@@H]1O[C@H](OC[C@H]2O[C@@H](OCCc3ccc(O)c(O)c3)[C@H](O)[C@@H](O)[C@@H]2OC(=O)C=Cc4ccc(O)c(O)c4)[C@H](O)[C@H](O)[C@H]1O DTOUWTJYUCZJQD-QJDQKFITSA-N 0.000 description 1
- 239000009636 Huang Qi Substances 0.000 description 1
- WJHSRFQBVYHKKL-UHFFFAOYSA-N Oroboside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC(O)=C2C(=O)C(C=3C=C(O)C(O)=CC=3)=COC2=C1 WJHSRFQBVYHKKL-UHFFFAOYSA-N 0.000 description 1
- 240000004534 Scutellaria baicalensis Species 0.000 description 1
- 235000017089 Scutellaria baicalensis Nutrition 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 1
- 229940038481 bee pollen Drugs 0.000 description 1
- 238000009924 canning Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000003733 chicria Nutrition 0.000 description 1
- 235000021557 concentrated beverage Nutrition 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- PEFNSGRTCBGNAN-QNDFHXLGSA-N luteolin 7-O-beta-D-glucoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC(O)=C2C(=O)C=C(C=3C=C(O)C(O)=CC=3)OC2=C1 PEFNSGRTCBGNAN-QNDFHXLGSA-N 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229940023492 oral liquid product Drugs 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
- A61K36/634—Forsythia
-
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/16—Drugs for disorders of the alimentary tract or the digestive system for liver or gallbladder disorders, e.g. hepatoprotective agents, cholagogues, litholytics
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- A61P11/06—Antiasthmatics
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- A61P11/14—Antitussive agents
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- A61P31/04—Antibacterial agents
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- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention belongs to the technical field of food processing, and particularly relates to a preparation method of a honeysuckle and forsythia suspense leaf compound beverage. According to the preparation method of the honeysuckle and forsythia suspense leaf composite beverage, the honeysuckle and the forsythia suspense leaf are combined in a compatibility mode and are continuously prepared into two kinds of beverage containing volatile oil and extract in one step, and the honeysuckle and forsythia suspense leaf composite beverage is expected to have a certain effect on improving sub-health. The honeysuckle and the forsythia suspense leaves are distilled by adding water, so that beneficial substances are fully released to obtain an oil phase and a water phase, and the oil phase and the water phase are respectively utilized, and the waste of volatile oil after distillation is avoided. The honeysuckle can fully release the beneficial substances of the honeysuckle through the distillation technology, and has the functions of resisting bacteria and diminishing inflammation, clearing away heat and toxic materials, treating heat-toxin bloody flux, carbuncle and furuncle, pharyngitis and various infectious diseases. The honeysuckle and the forsythia suspense are compatible and mutually reinforced, and are mutually matched and interdependent, so that the efficacy of 1+1 > 2 is realized, and the efficacy of clearing heat and removing toxicity is greatly enhanced.
Description
Technical Field
The invention belongs to the technical field of food processing, and particularly relates to a preparation method of a honeysuckle and forsythia suspense leaf compound beverage.
Background
Honeysuckle is a common heat-clearing and detoxifying medicinal material, and the modern medical table shows that: flos Lonicerae contains chlorogenic acid, luteoloside and volatile oil, has antibacterial, antiviral, immunity improving, skin caring and weight reducing effects, and can be used in medicine and food fields. The dry product can be used for drinking after soaking in water, is a substance with homology of medicine and food, and has a beverage and an oral liquid product. The honeysuckle volatile oil is volatile and difficult to extract. Usually, chlorogenic acid extract of honeysuckle is used, and a large amount of volatile oil is abandoned. In recent patent (application No. CN201510433386.X), concentrated beverage is prepared from flos Lonicerae, and folium forsythiae extract is not added, and flos Lonicerae volatile oil is not reasonably utilized. A flos Lonicerae beverage (application number: CN 201310677213.3) is prepared by adding flos Lonicerae, radix astragali, fructus Lycii, fructus Jujubae, alismatis rhizoma, white sugar, and citric acid, but folium forsythiae is not added, and flos Lonicerae volatile oil is not utilized reasonably. A honeysuckle plant beverage formula and a preparation method thereof (application number: CN 201654879.1) the formula contains honeysuckle and chrysanthemum, but does not contain weeping forsythia leaves, and the volatile oil of the honeysuckle is not reasonably utilized. A honeysuckle beverage is prepared from (by weight parts) flos Lonicerae 20-30, fructus Lycii 15-20, flos Chrysanthemi 10-15, bee pollen 15-20, and herba Pileae Scriptae 10-15, but does not contain folium forsythiae and has no reasonable use of flos Lonicerae volatile oil.
The forsythia fruits are common bulk medicinal materials for clearing heat and removing toxicity, and the volatile oil content measurement is definitely increased by the new edition 2020 of Chinese pharmacopoeia forsythia quality standard and is used as an important index for controlling the quality of forsythia. In recent years, the development of forsythia fruit resources is wide, and forsythia leaf resources are wasted greatly. In recent patent, a forsythia suspense leaf beverage (application (patent) No. CN 201310677213.3) relates to a beverage containing a forsythia suspense leaf extract and a traditional Chinese medicine mixed extracting solution of endive, umbellate rock jasmine and scutellaria baicalensis, but honeysuckle is not contained, and the volatile oil of forsythia suspense leaves is not reasonably utilized. In the preparation method of the forsythia suspense beverage (application (patent) No. CN 201611175739.1), raw materials are prepared according to 0.4-0.6 kg of dry forsythia suspense leaf decoction pieces, 0.12-0.16 kg of citric acid, 0.72-0.96 kg of sodium citrate, 4-5 kg of rock candy or 5-6.26 kg of xylitol and 40-50 ml of green tea essence used in every 100L of the beverage, wherein honeysuckle is not contained, and the volatile oil of the forsythia suspense leaf is not reasonably utilized.
In the current various literature data, the preparation method of the honeysuckle beverage does not contain weeping forsythia leaves; the method for preparing the beverage by using the forsythia suspense leaves does not contain honeysuckle. And the volatile oil of honeysuckle and forsythia leaves is not reasonably utilized. The extract is prepared by steaming with hot water, directly canning, or precipitating and filtering the steaming solution, and drying to obtain powdered extract. In the hot water cooking process, a large amount of honeysuckle or forsythia suspense leaf volatile oil is directly discharged through steam and discarded, and the resource of the honeysuckle or forsythia suspense leaf volatile oil is not reasonably utilized, so that the resource is seriously wasted. At present, a method for preparing a beverage by combining honeysuckle and forsythia suspense leaves together in a compatible manner is not available, and a report that the honeysuckle and forsythia suspense leaf beverage is prepared by using both an extract and volatile oil is not available.
Disclosure of Invention
The invention aims to provide a preparation method of a honeysuckle and forsythia suspense leaf composite beverage, which is characterized in that forsythia suspense leaves are used for replacing forsythia suspense (fruit) and honeysuckle for the first time to form compatibility application, and two beverages containing volatile oil and extract are continuously prepared at one time, and the preparation method is expected to have a certain effect on improving sub-health.
The second purpose of the invention is to provide a honeysuckle and forsythia suspense leaf extract composite beverage. Because the mixed extract beverage contains active ingredients such as phillyrin, forsythoside A, rutin, chlorogenic acid and the like, the beverage has a certain effect on improving sub-health, well solves the accessibility of the traditional Chinese medicine, and has important significance on promoting the culture of the traditional Chinese medicine and promoting the health of the whole population.
The third purpose of the invention is to provide a honeysuckle and forsythia suspense leaf volatile oil compound beverage. Because the beverage contains the volatile oil of the honeysuckle and the forsythia suspense leaves, the serious waste of volatile oil resources is avoided, and the volatile oil has strong aromatic smell and medicinal value.
The invention is realized by the following technical scheme:
in a first aspect, the invention provides a preparation method of a honeysuckle and forsythia suspense leaf compound beverage,
mixing honeysuckle and forsythia suspense leaves according to the mass ratio of 1.5-2 to obtain a base material, adding water into the base material, and distilling at 70-100 ℃ to obtain a water phase and an oil phase;
filtering the water phase to obtain filter residue and filtrate, and diluting the filtrate with water to obtain extract composite beverage;
diluting the oil phase with water to obtain volatile oil compound beverage.
In a second aspect, the invention provides a honeysuckle and forsythia suspense leaf extract composite beverage prepared by the preparation method.
In a third aspect, the invention provides a honeysuckle and forsythia suspense leaf volatile oil compound beverage prepared by the preparation method.
Compared with the prior art, the invention at least has the following technical effects:
the invention makes full use of the compatibility and combination of honeysuckle and forsythia suspense leaves. The compatibility of the honeysuckle and the forsythia (fruit) is inherited and innovated, and the forsythia (fruit) is replaced by forsythia leaves for the first time to form compatibility application. And two beverages of an oil phase containing the volatile oil and a filtered water phase containing the extract are continuously prepared at one time, and are expected to have certain effects on preventing diseases. The honeysuckle and the forsythia suspense leaves are distilled to recycle the oil phase, so that the volatile oil phase is reasonably utilized, and the volatile oil substances of the honeysuckle and the forsythia suspense leaves have the effects of sterilization, bacteriostasis and the like. The water phase of the honeysuckle and the forsythia suspense leaves is fully utilized. The forsythia suspense leaves can fully utilize the active substance phillyrin of the forsythia suspense leaves through a distillation technology, the phillyrin can resist virus attack, and the forsythia suspense leaves contain active ingredients such as phillyrin, forsythiaside A, rutin, volatile oil and the like and have good biological consistency. Moreover, experiments show that the content of phillyrin in the forsythia suspense leaves is far higher than that of forsythia suspense fruits, and no toxic or side effect exists. The honeysuckle can fully release the beneficial substances of the honeysuckle through the distillation technology, and has the functions of resisting bacteria and diminishing inflammation, clearing away heat and toxic materials, treating heat-toxin bloody flux, carbuncle and furuncle, pharyngitis and various infectious diseases. The honeysuckle and the forsythia suspense are compatible and mutually reinforced, and are mutually matched and interdependent, so that the effect of 1+1 is more than 2, and the effect of clearing heat and removing toxicity is greatly enhanced.
The invention provides a honeysuckle and forsythia suspense leaf extract compound beverage prepared by the preparation method. Because the honeysuckle and the forsythia suspense leaves contained in the beverage have certain effects on improving sub-health, the accessibility of the traditional Chinese medicine is well solved, and the beverage has important significance on promoting the culture of the traditional Chinese medicine and promoting the health of the whole people.
The invention provides a honeysuckle and forsythia suspense leaf volatile oil compound beverage prepared by the preparation method. Because the beverage contains the volatile oil of the honeysuckle and the forsythia suspense leaves, the serious waste of volatile oil resources is avoided, the volatile oil has strong aromatic smell and medicinal value, and the beverage contains the volatile oil component which can increase the functional effect of the beverage. The honeysuckle volatile oil has the functions of resisting bacteria, resisting virus, relieving fever, relieving cough and relieving asthma, and also has the functions of reducing blood pressure, delaying senility, protecting liver, improving the immunity of the organism and the like. The volatile oil of folium forsythiae has antibacterial, antiviral, heat and toxic materials clearing away, and common cold and influenza treating effects.
Detailed Description
Embodiments of the present invention will be described in detail with reference to the following examples, but those skilled in the art will understand that the following examples are merely illustrative of the present invention and should not be construed as limiting the scope of the present invention, and that the specific conditions not specified in the examples are carried out according to conventional conditions or conditions suggested by the manufacturer, and that the reagents or equipment used are not specified by the manufacturer, and are all conventional products available through commercial purchase.
The technical scheme of the invention is as follows:
in a first aspect, the invention provides a preparation method of a honeysuckle and forsythia suspense leaf compound beverage,
mixing honeysuckle and forsythia suspense leaves according to the mass ratio of 1.5-2 to obtain a base material, adding water into the base material, and distilling at 70-100 ℃ to obtain a water phase and an oil phase;
filtering the water phase to obtain filter residue and filtrate, and diluting the filtrate with water to obtain extract composite beverage;
diluting the oil phase with water to obtain volatile oil compound beverage.
Mixing honeysuckle and forsythia suspense leaves according to the mass ratio of 1 to 05-2, adding water for distillation, fully utilizing the compatibility and combination of the honeysuckle and the forsythia suspense leaves, and continuously preparing two beverages of an oil phase containing volatile oil and a water phase filtrate containing extract at one time, wherein the two beverages are expected to have a certain effect on preventing diseases. The honeysuckle and the forsythia suspense leaves are distilled to recycle the oil phase, so that the volatile oil phase is reasonably utilized, and the volatile oil substances of the honeysuckle and the forsythia suspense leaves have the effects of sterilization, bacteriostasis and the like. The water phase of the honeysuckle and the forsythia suspense leaves is fully utilized. The forsythia suspense leaves can fully utilize the active substance phillyrin of the forsythia suspense leaves through a distillation technology, the phillyrin can resist the attack of new coronavirus, and the invention has positive era significance in the post epidemic situation era. The honeysuckle can fully release the beneficial substances of the honeysuckle through the distillation technology, and has the functions of resisting bacteria and diminishing inflammation, clearing away heat and toxic materials, treating heat-toxin bloody flux, carbuncle and furuncle, pharyngitis and various infectious diseases. The honeysuckle and the forsythia suspense are compatible and mutually reinforced, and are mutually matched and interdependent, so that the effect of 1+1 is more than 2, and the effect of clearing heat and removing toxicity is greatly enhanced.
Further, in a preferred embodiment of the present invention, the distillation further comprises adding water to the obtained residue, and distilling for 2-4 times. The method aims to further utilize the effective components of the raw materials, fully utilize the beneficial substances of the raw materials and avoid the waste of the beneficial components in the raw materials.
Furthermore, in the preferred embodiment of the invention, the filter residue is distilled by adding water, and the mass ratio of the added water is 10-30 times of that of the filter residue. The method aims to extract the beneficial components of the raw materials to the maximum extent by adding water.
Further, in the preferred embodiment of the present invention, the distillation time of the residue is 20min to 60min. The method aims to find the optimal balance point between the full utilization of the beneficial components of the raw materials and the energy consumption cost, the energy consumption cost is increased when the time is too long, and the beneficial components of the raw materials cannot be fully utilized when the time is too short.
Further, in the preferred embodiment of the present invention, the above-mentioned base material is distilled with water, and the mass ratio of the water added is 20-60 times of that of the base material. The purpose is to continuously extract the beneficial components of the raw materials to the maximum extent by adding water.
Further, in a preferred embodiment of the present invention, the distillation time of the base material is 30min to 90min. The aim is to continuously and fully utilize the beneficial components of the raw materials and energy consumption cost to find an optimal balance point, the energy consumption cost is increased when the time is too long, and the beneficial components of the raw materials cannot be fully utilized when the time is too short.
Further, in a preferred embodiment of the invention, the extract composite beverage or the volatile oil composite beverage is boiled and sterilized, sterilized for 5min to 20min, cooled and filled. The aim is to kill the mixed bacteria in the beverage and prolong the shelf life of the product by boiling and sterilizing. And because the sterilization is carried out by boiling, a substance of a preservative is not required to be introduced, and the harm to the health of a human body is avoided.
Further, in a preferred embodiment of the present invention, the mass ratio of the filtrate or oil phase to water is 1 to 10. The proportion is carried out according to the proportion, and the aim is to increase the extraction utilization rate of the beneficial components of the raw materials to the maximum extent.
Further, in a preferred embodiment of the present invention, the honeysuckle and the forsythia suspense leaves are both dried. The purpose is to facilitate the transportation and storage of raw materials and ensure the excellence of the raw materials.
In a second aspect, the invention provides a honeysuckle and forsythia suspense leaf composite extract beverage prepared by the preparation method. Because the honeysuckle and the forsythia suspense leaves contained in the beverage have certain effects on preventing diseases, especially in the post epidemic situation era, the accessibility of the traditional Chinese medicine is well solved, and the beverage has important significance on promoting the culture of the traditional Chinese medicine and promoting the health of the whole people.
In a third aspect, the invention provides a honeysuckle and forsythia suspense leaf composite volatile oil beverage prepared by the preparation method. Because the beverage contains the volatile oil of the honeysuckle and the forsythia suspense leaves, the serious waste of volatile oil resources is avoided, the volatile oil has strong aromatic smell and medicinal value, and the functional effect of the beverage can be improved due to the volatile oil contained in the beverage. The honeysuckle volatile oil has the functions of resisting bacteria, resisting virus, relieving fever, relieving cough and relieving asthma, and also has the functions of reducing blood pressure, delaying senility, protecting liver, improving the immunity of the organism and the like. The volatile oil of folium forsythiae has antibacterial, antiviral, heat and toxic materials clearing away, and common cold and influenza treating effects.
The following describes in detail specific embodiments of the present invention. It should be understood that the detailed description and specific examples, while indicating the present invention, are given by way of illustration and explanation only, not limitation.
Example 1
The embodiment provides a preparation method of a honeysuckle and forsythia suspense leaf compound beverage, which comprises the following steps:
(1) Mixing the dried honeysuckle and the weeping forsythia leaves according to a mass ratio of 1;
(2) Adding water with the mass 20 times of the total mass of the base materials, heating and distilling; the distillation temperature is 70-74 deg.C, and the distillation time is 30-31 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) Diluting the obtained filtrate with water, wherein the addition amount of water is 100 times of the mass of the filtrate, and diluting with water to obtain compound beverage containing flos Lonicerae and folium forsythiae extract.
Diluting the obtained oil phase with water, wherein the amount of water added is 100 times of the weight of the oil phase, and diluting with water to obtain compound beverage containing flos Lonicerae and folium forsythiae volatile oil.
Example 2
The embodiment provides a preparation method of a honeysuckle and forsythia suspense leaf compound beverage, which comprises the following steps:
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to a mass ratio of 1;
(2) Adding water 60 times the total mass of the base materials, heating and distilling; the distillation temperature is 98-100 deg.C, and the distillation time is 87-90 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) Diluting the obtained filtrate with water, wherein the amount of water added is 1000 times of the mass of the filtrate, and diluting with water to obtain compound beverage containing flos Lonicerae and folium forsythiae extract.
Diluting the obtained oil phase with water, wherein the addition amount of water is 1000 times of the oil phase by mass, and diluting with water to obtain compound beverage containing flos Lonicerae and folium forsythiae volatile oil.
Example 3
The embodiment provides a preparation method of a honeysuckle and forsythia suspense leaf compound beverage, which comprises the following steps:
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to a mass ratio of 1;
(2) Adding water with the mass 40 times of the total mass of the base materials, heating and distilling; the distillation temperature is 80-84 deg.C, and the distillation time is 60-62 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) Diluting the filtrate with water, wherein the amount of water added is 500 times of the mass of the filtrate, and diluting with water to obtain compound beverage containing flos Lonicerae and folium forsythiae extract.
Diluting the obtained oil phase with water, wherein the addition amount of water is 500 times of the oil phase by mass, and diluting with water to obtain the compound beverage containing flos Lonicerae and folium forsythiae volatile oil.
Example 4
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to the mass ratio of 1;
(2) Adding water with the mass 25 times of the total mass of the base materials, heating and distilling; the distillation temperature is 98-100 deg.C, and the distillation time is 60-62 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) And (4) adding water into the filter residue obtained in the step (3), wherein the mass of the added water is 18 times that of the filter residue, continuously distilling for 32-36 min, recovering a water phase and an oil phase after distillation, and filtering the water phase to obtain filtrate and filter residue.
(5) And (4) adding water into the filtrate obtained in the steps (3) and (4) for dilution, wherein the adding amount of the water is 350 times of the mass of the filtrate, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf extract.
And (4) adding water into the oil phase obtained in the steps (3) and (4) for dilution, wherein the adding amount of the water is 350 times of the mass of the oil phase, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf volatile oil.
Example 5
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to the mass ratio of 1.5;
(2) Adding water with the mass 20 times of the total mass of the base materials, heating and distilling; the distillation temperature is 98-100 deg.C, and the distillation time is 89-90 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) And (4) adding water into the filter residue obtained in the step (3), wherein the mass of the added water is 30 times that of the filter residue, continuously distilling for 49-50 min, recovering a water phase and an oil phase after distillation, and filtering the water phase to obtain filtrate and filter residue.
(5) And (5) adding water into the filtrate obtained in the steps (3) and (4) for dilution, wherein the adding amount of the water is 800 times of the mass of the filtrate, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf extracts.
And (5) adding water into the oil phase obtained in the steps (3) and (4) for dilution, wherein the adding amount of the water is 800 times of the mass of the oil phase, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf volatile oil.
Example 6
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to a mass ratio of 1;
(2) Adding water 40 times of the total mass of the base materials, heating and distilling; the distillation temperature is 95-98 deg.C, and the distillation time is 60-63 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) And (4) adding water into the filter residue obtained in the step (3), wherein the mass of the added water is 25 times that of the filter residue, continuously distilling for 36-38 min, recovering a water phase and an oil phase after distillation, and filtering the water phase to obtain filtrate and filter residue.
(5) And (4) adding water into the filtrate obtained in the steps (3) and (4) for dilution, wherein the adding amount of the water is 600 times of the mass of the filtrate, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf extract.
And (5) adding water into the oil phase obtained in the steps (3) and (4) for dilution, wherein the adding amount of the water is 600 times of the mass of the oil phase, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf volatile oil.
Example 7
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to a mass ratio of 1;
(2) Adding water with the mass 20 times of the total mass of the base materials, heating and distilling; the distillation temperature is 70-72 deg.C, and the distillation time is 89-90 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) And (4) adding water into the filter residue obtained in the step (3), wherein the mass of the added water is 10 times that of the filter residue, continuously distilling for 50-53 min, recovering a water phase and an oil phase after distillation, and filtering the water phase to obtain filtrate and filter residue.
(5) And (4) adding water into the filter residue obtained in the step (4), and the other steps are the same as the step (4). An oil phase and a filtrate are obtained.
(6) And (5) adding water into the filter residue obtained in the step (5), wherein other steps are the same as those in the step (4) or (5). An oil phase and a filtrate are obtained.
(7) And (4) adding water into the filtrate obtained in the steps (3) to (6) for dilution, wherein the adding amount of the water is 100 times of the mass of the filtrate, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf extract.
And (4) adding water into the oil phase obtained in the steps (3) to (6) for dilution, wherein the adding amount of the water is 100 times of the mass of the oil phase, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf volatile oil.
Example 8
(1) Mixing the dried honeysuckle and the weeping forsythia leaves according to a mass ratio of 1;
(2) Adding water with the mass 20 times of the total mass of the base materials, heating and distilling; the distillation temperature is 70-71 deg.C, and the distillation time is 88-90 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) And (4) adding water into the filter residue obtained in the step (3), wherein the mass of the added water is 24 times that of the filter residue, continuously distilling for 29-30 min, recovering a water phase and an oil phase after distillation, and filtering the water phase to obtain filtrate and filter residue.
(5) And (5) adding water into the filter residue obtained in the step (4), and performing other steps as same as the step (4). An oil phase and a filtrate are obtained.
(6) And (5) adding water into the filtrate obtained in the steps (3) to (5) for dilution, wherein the adding amount of the water is 120 times of the mass of the filtrate, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf extracts.
And (5) adding water into the oil phase obtained in the steps (3) - (5) for dilution, wherein the adding amount of the water is 120 times of the mass of the oil phase, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf volatile oil.
Example 9
(1) Mixing the dried honeysuckle and the forsythia suspense leaves according to a mass ratio of 1;
(2) Adding water 60 times the total mass of the base materials, heating and distilling; the distillation temperature is 99-100 deg.C, and the distillation time is 30-32 min.
(3) Distilling, recovering water phase and oil phase, and filtering water phase to obtain filtrate and residue.
(4) And (4) adding water into the filter residue obtained in the step (3), wherein the mass of the added water is 12 times that of the filter residue, continuously distilling for 45-46 min, recovering a water phase and an oil phase after distillation, and filtering the water phase to obtain filtrate and filter residue.
(5) And (4) adding water into the filter residue obtained in the step (4), and the other steps are the same as the step (4). An oil phase and a filtrate are obtained.
(6) And (5) adding water into the filter residue obtained in the step (5), and the other steps are the same as the step (4) or the step (5). An oil phase and a filtrate are obtained.
(7) And (4) adding water into the filtrate obtained in the steps (3) to (6) for dilution, wherein the adding amount of the water is 300 times of the mass of the filtrate, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf extract.
And (4) adding water into the oil phase obtained in the steps (3) to (6) for dilution, wherein the adding amount of the water is 300 times of the mass of the oil phase, and adding water for dilution to obtain the compound beverage containing the honeysuckle and the forsythia suspense leaf volatile oil.
The test results of the composite beverage of honeysuckle flower and forsythia suspense leaf volatile oil prepared in example 3 are shown in the following table
Nutrient composition table
The test results of the composite beverage of honeysuckle and forsythia suspense leaf extracts prepared in example 3 are shown in the following table
Total 3 pages, page 2 No: s22031192
Nutrient composition list information
The experimental research shows that the invention inherits the essence, is upright and innovative, has good sense and taste and is suitable for industrial production, and the product of the invention accords with the national drink execution standard.
Finally, it should be noted that: the above description is only a preferred embodiment of the present invention, and is not intended to limit the scope of the present invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. A preparation method of honeysuckle and forsythia suspense leaf compound beverage is characterized in that,
mixing honeysuckle and forsythia suspense leaves according to the mass ratio of 1.5-2 to obtain a base material, and adding water into the base material to distill at 70-100 ℃ to obtain a water phase and an oil phase;
filtering the water phase to obtain filter residue and filtrate, and diluting the filtrate with water to obtain an extract composite beverage;
diluting the oil phase with water to obtain volatile oil compound beverage.
2. The method for preparing the honeysuckle and forsythia suspensa leaf compound beverage according to claim 1, wherein the distillation further comprises adding water to the obtained filter residue and distilling for 2-4 times.
3. The preparation method of the honeysuckle and forsythia suspensa leaf compound beverage as claimed in claim 2, wherein water is added to the filter residue for distillation, and the mass ratio of the added water is 10-30 times that of the filter residue;
preferably, the distillation time of the filter residue is 20min-60min.
4. The preparation method of the honeysuckle and forsythia suspense leaf composite beverage according to claim 1, wherein the base material is distilled by adding water, and the mass ratio of the water added is 20-60 times of that of the base material.
5. The method for preparing a honeysuckle and forsythia suspensa leaf compound beverage according to claim 1, wherein the distillation time of the base material is 30-90 min.
6. The method for preparing the honeysuckle and forsythia suspensa leaf compound beverage according to claim 1, wherein the extract compound beverage or the volatile oil compound beverage is boiled and sterilized, sterilized for 5min to 20min, cooled and filled.
7. The preparation method of the honeysuckle and forsythia suspensa leaf compound beverage as claimed in claim 6, wherein the mass ratio of the filtrate to water is 1-10;
preferably, the mass ratio of the oil phase to the water is 1-10.
8. The method for preparing a compound beverage of honeysuckle and forsythia suspense leaves according to claims 1 to 7, wherein the honeysuckle and the forsythia suspense leaves are both dry.
9. The honeysuckle and forsythia suspense leaf extract compound beverage prepared by the preparation method of any one of claims 1 to 8.
10. The honeysuckle flower and forsythia suspense leaf volatile oil compound beverage prepared by the preparation method of any one of claims 1 to 8.
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