CN115252492A - Moisturizing composition and application thereof, moisturizing mask composition aerosol and preparation method - Google Patents
Moisturizing composition and application thereof, moisturizing mask composition aerosol and preparation method Download PDFInfo
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- CN115252492A CN115252492A CN202210879731.2A CN202210879731A CN115252492A CN 115252492 A CN115252492 A CN 115252492A CN 202210879731 A CN202210879731 A CN 202210879731A CN 115252492 A CN115252492 A CN 115252492A
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- moisturizing
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- mixture
- skin
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- 239000000203 mixture Substances 0.000 title claims abstract description 148
- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 105
- 239000000443 aerosol Substances 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000001856 aerosol method Methods 0.000 title description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 49
- 244000144927 Aloe barbadensis Species 0.000 claims abstract description 24
- 235000002961 Aloe barbadensis Nutrition 0.000 claims abstract description 24
- 235000011399 aloe vera Nutrition 0.000 claims abstract description 24
- 239000000284 extract Substances 0.000 claims abstract description 24
- 239000003755 preservative agent Substances 0.000 claims abstract description 23
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims abstract description 22
- 229920002674 hyaluronan Polymers 0.000 claims abstract description 22
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- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims abstract description 16
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- 229960003237 betaine Drugs 0.000 claims abstract description 16
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- 235000014001 Prunus serrulata Nutrition 0.000 claims abstract description 15
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 15
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229930003270 Vitamin B Natural products 0.000 claims abstract description 9
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- 238000003756 stirring Methods 0.000 claims description 30
- 230000001815 facial effect Effects 0.000 claims description 19
- 229930003779 Vitamin B12 Natural products 0.000 claims description 12
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 claims description 12
- 239000011715 vitamin B12 Substances 0.000 claims description 12
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- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical group OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 7
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- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
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- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 2
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- WTVHAMTYZJGJLJ-UHFFFAOYSA-N (+)-(4S,8R)-8-epi-beta-bisabolol Natural products CC(C)=CCCC(C)C1(O)CCC(C)=CC1 WTVHAMTYZJGJLJ-UHFFFAOYSA-N 0.000 description 1
- RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 description 1
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 1
- OCKGFTQIICXDQW-ZEQRLZLVSA-N 5-[(1r)-1-hydroxy-2-[4-[(2r)-2-hydroxy-2-(4-methyl-1-oxo-3h-2-benzofuran-5-yl)ethyl]piperazin-1-yl]ethyl]-4-methyl-3h-2-benzofuran-1-one Chemical compound C1=C2C(=O)OCC2=C(C)C([C@@H](O)CN2CCN(CC2)C[C@H](O)C2=CC=C3C(=O)OCC3=C2C)=C1 OCKGFTQIICXDQW-ZEQRLZLVSA-N 0.000 description 1
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- 240000008067 Cucumis sativus Species 0.000 description 1
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- 206010012289 Dementia Diseases 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 235000009220 Prunus speciosa Nutrition 0.000 description 1
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- RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
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- 229940036350 bisabolol Drugs 0.000 description 1
- HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 description 1
- 230000019522 cellular metabolic process Effects 0.000 description 1
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- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of skin care products, and particularly relates to a moisturizing composition, application thereof, a moisturizing mask composition aerosol and a preparation method thereof. The moisturizing composition comprises the following components in parts by weight: 10-30 parts of oriental cherry flower extract, 1-3 parts of 4D hyaluronic acid, 5-8 parts of Caesalpinia spinosa gum and 6-10 parts of vitamin B. The invention discloses a moisturizing mask composition aerosol, which comprises the following components in percentage by mass: 78.3-91.23% of aloe vera leaf water, 1.0-3.0% of rosa damascena flower water, 1-2% of a moisturizing composition, 2.0-4.0% of betaine, 0.22-0.5% of PPG-13-decyltetradecanol polyether-24, 0.4-1.0% of caprylic/capric triglyceride, 4.0-6.0% of polyglycerol-6, 0.05-0.2% of a preservative, and 0.1-5.0% of a propellant. The invention has convenient use and good moisturizing and skin moistening effects.
Description
Technical Field
The invention belongs to the technical field of skin care products, and particularly relates to a moisturizing composition and application thereof, a moisturizing mask composition aerosol and a preparation method of the moisturizing mask composition aerosol.
Background
With the continuous development of scientific level and the increasing improvement of living standard of people, people have not only satisfied the requirement of cleaning products for higher living quality, but also gradually come into the choice of people for skin care cosmetic products. The mask is a product in skin care products, and the principle of the mask is that the mask is temporarily isolated from the outside air by a short time when the mask is covered on the face, pores on the surface of the skin can be opened while the temperature of the skin is increased, so that the sweat gland secretion and metabolism can be promoted, the oxygen content of the skin can be increased, the skin can remove products of epidermal cell metabolism and accumulated grease substances, and the moisture in the mask can permeate into the cuticle of the epidermis to soften the skin and make the skin naturally bright and elastic. The mask has the following excellent effects: (1) The moist mask is applied to the face, the substances in the mask tightly wrap the skin, so that the skin is isolated from the outside air, on one hand, the moisture slowly permeates into the horny layer of the epidermis, and on the other hand, the moisture in the mask is prevented from losing quickly, cells of the horny layer can be drunk enough in a moist environment, the collagen of deep cells absorbs the moisture, and the skin is soft and has elasticity. Meanwhile, the skin surface is 'covered with a quilt', and the skin is warmed, so that the capillary vessels are slowly expanded, the blood microcirculation in the deep layer of the skin is accelerated, the activity of cells in each layer of the epidermis is enhanced, and the old state of fatigue is eliminated. (2) In the process of making the mask, the skin is isolated from the outside air, the temperature on the surface of the skin is raised, pores are expanded, and the secretion of sweat glands is promoted, so that the mask is beneficial to removing outside dust, chemical pollutants and microorganisms infected in the pores, and is also beneficial to removing waste generated by metabolism of epidermal cells and excessive accumulated grease substances. Subsequently, when the mask is formed into a film, the adhesive components of the mask can completely remove dirt, chemical pollutants, wastes, grease and other toxic substances harmful to the health of the skin on the surface of the skin and in pores. (3) The mask is applied to the face and slowly dries to form a film, which slowly tightens the skin, increases tension, and provides a good stimulus to the skin to stretch out wrinkles. Small wrinkles are not visible, large deep wrinkles appear small and complete, and the whole face looks young. (4) The moist mask is applied to the face and left for a period of time, which facilitates the penetration of nutritional or functional substances into the deep layers of the skin. Meanwhile, the expansion of the capillary vessels and the increase of blood microcirculation can greatly promote the absorption and utilization of nutritional or functional substances in the mask by cells.
With the continuous improvement of the living standard of people and the continuous development of the daily cosmetics market, the facial mask is popular among consumers of different ages. The facial mask has various types, such as mud-shaped facial mask, facial patch, jelly-shaped facial mask, no-clean facial mask, tear-off facial mask and the like. For example, chinese patent application CN107951794A discloses a method for preparing a pure natural facial mask, which mainly uses a silk non-woven fabric as a substrate, natural materials such as honey, egg white, bletilla striata, cucumber extracts and the like as facial mask essence, and the facial mask essence is uniformly distributed on the silk non-woven fabric in a fiber state by a centrifugal spinning technology, and then cut according to a facial mask model to prepare the facial mask. Chinese patent application CN107913200A discloses a dead sea mud magnet moistening mask, which comprises the following raw materials, by mass, 40-60 parts of mask iron powder, 8-12 parts of a thickening agent, 5-8 parts of isononanoic acid isodecyl ester, 14-21 parts of hydrogenated cocoglyceride, 8-12 parts of silicone oil, 4.8-8 parts of organic hectorite, 0.2-0.35 part of titanium dioxide, 0.8-1.5 parts of polymethylsilsesquioxane, 0.4-0.55 part of kobazak and 0.08-0.12 part of bisabolol. Although the above mask has a good effect, the above mask is inconvenient to use.
Modern life is more and more flexible, and has certain appeal to the convenience of cosmetics, and the traditional surface-mounted facial mask or smearing facial mask cannot meet the requirements. Aiming at the problems of the existing facial masks, a spraying facial mask product which has the functions of moisturizing and fitting the face and has the spraying convenience is needed to be developed.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a moisturizing composition, application thereof, a moisturizing mask composition aerosol and a preparation method thereof. The moisturizing mask composition aerosol prepared by the invention is convenient to use and has excellent moisturizing and skin moistening effects.
The technical scheme of the invention is as follows:
the moisturizing composition comprises the following components in parts by weight:
10-30 parts of oriental cherry flower extract, 1-3 parts of 4D hyaluronic acid, 5-8 parts of Caesalpinia spinosa gum and 126-10 parts of vitamin B.
Further, the moisturizing composition comprises the following components in parts by weight:
20 parts of oriental cherry flower extract, 2 parts of 4D hyaluronic acid, 6 parts of Caesalpinia spinosa gum and 10 parts of vitamin B.
The invention also aims to provide application of the moisturizing composition in preparing a moisturizing mask skin care product.
The moisturizing mask composition aerosol comprises the following components in percentage by mass:
78.3-91.23% of aloe vera leaf water, 1.0-3.0% of rosa damascena flower water, 1-2% of a moisturizing composition, 2.0-4.0% of betaine, 0.22-0.5% of PPG-13-decyltetradecanol polyether, 0.4-1.0% of caprylic/capric triglyceride, 4.0-6.0% of polyglycerol, 0.05-0.2% of a preservative and 0.1-5.0% of a propellant.
Further, the moisturizing mask composition aerosol comprises the following components in percentage by mass:
85.1% of aloe vera leaf water, 2.0% of rosa damascena flower water, 1.5% of a moisturizing composition, 3.0% of betaine, 0.3% of PPG-13-decyltetradecanol polyether-24, 0.6% of caprylic/capric triglyceride, 5.0% of polyglycerol-6, 0.1% of a preservative and 2.4% of a propellant.
Further, the preservative is phenoxyethanol.
Further, the propellant is nitrogen.
The moisturizing mask composition aerosol is prepared from ALOE vera leaf water (ALOE BARBADENSIS leaf water), ROSA DAMASCENA flower water (ROSA DAMASCENA flower water), a moisturizing composition, betaine, PPG-13-decyltetradecanol polyether-24 and other raw materials. The moisturizing composition is prepared by compounding a cherry blossom extract, 4D hyaluronic acid, caesalpinia spinosa gum and vitamin B12, the cherry blossom extract in the moisturizing composition contains elements of cherry leaf flavone, has a good effect on skin care, can strengthen mucous membranes, promote sugar metabolism in vivo, is beneficial to skin tightness, can shrink pores and keep skin elasticity; the hyaluronic acid can provide moisture retention and skin nourishing effects for the skin in multiple directions; the vitamin B12 is helpful for promoting the regeneration of skin cells and well improving the rough state of the skin; the Caesalpinia spinosa Kuntze gum can improve the stability of the product, and can generate a moisture-keeping synergistic effect with a cherry blossom extract (PRUNUS SPECIOSA) flower extract), 4D hyaluronic acid and a vitamin B12 substance, so that the moisture-keeping effect is more durable.
The invention also provides a preparation method of the moisturizing mask composition aerosol, which comprises the following steps:
s1, sequentially weighing 9/10 (volume ratio) of aloe vera leaf water, rosa damascena flower water, oriental cherry flower extract, betaine and 4D hyaluronic acid, uniformly mixing, heating to 80-85 ℃, and keeping the temperature and stirring for 20-30min to obtain a mixture A;
s2, sequentially weighing PPG-13-decyltetradecanol polyether-24 and caprylic/capric triglyceride, mixing, placing in a water bath at 45-50 ℃, and uniformly stirring to obtain a mixture B;
s3, adding the rest amount of aloe vera leaf water into vitamin B12, and stirring until the mixture is uniformly dissolved to obtain a mixture C;
s4, cooling the mixture A obtained in the step S1 to 40-45 ℃, adding the uniformly mixed mixture B obtained in the step S2, and stirring for 4-8min to obtain a mixture D;
s5, adding the Caesalpinia spinosa gel, the preservative and the polyglycerol-6 into the mixture D obtained in the step S4, and stirring for 15-25min to obtain a mixture E;
s6, adding the pre-dissolved mixture C obtained in the step S3 into the mixture E obtained in the step S5, stirring for 10-15min, filtering through filter cloth of 200 meshes, and discharging to obtain the moisturizing facial mask composition;
and S7, filling the moisturizing mask composition obtained in the step S6, filling propellant, and sealing to obtain the moisturizing mask composition.
Compared with the prior art, the invention has the following advantages:
(1) The invention adds cherry blossom extract, 4D hyaluronic acid, caesalpinia spinosa gum and vitamin B12 as raw materials
The cherry blossom extract contains the elements of the cherry leaf flavone, has good effect on skin care, can strengthen mucous membrane, promote in-vivo sugar metabolism, help skin to tighten, can shrink pores and keep skin elasticity; the hyaluronic acid can provide moisture retention and skin nourishing effects for the skin in multiple directions; the vitamin B12 is helpful for promoting the regeneration of skin cells and well improving the rough state of the skin; the Caesalpinia spinosa gum can improve the stability of the product, and can generate a moisturizing synergistic effect with the cherry blossom extract, the 4D hyaluronic acid and the vitamin B12 substance, so that the moisturizing effect is more durable.
(2) The invention has the advantages of convenient use of spraying and the effects of moisturizing the skin of the mask.
(3) The binary bag valve aerosol has good atomization effect and fine mist diameter; in addition, the content is isolated from the outside air, a natural physical barrier is provided for long-term preservation of products and prevention of oxidative degradation of active matters, the use of preservatives or antioxidants in the formula can be reduced or avoided, and skin allergy is relieved.
Detailed Description
The present invention is further described in the following description of the specific embodiments, which is not intended to limit the invention, but various modifications and improvements can be made by those skilled in the art according to the basic idea of the invention, within the scope of the invention, as long as they do not depart from the basic idea of the invention.
The raw materials used in the invention are all conventional commercial ingredients in the cosmetic industry. Such as oriental cherry flower extract (Zhenghe (Guangzhou) Biotechnology Co., ltd.), 4D hyaluronic acid (Shandong Anhua biomedical Co., ltd.), aloe Barbadensis leaf Water (Yunnan Wan Green Bio-medicine Co., ltd.), rosa damascena flower Water (Guangzhou Hanhui chemical technology Co., ltd.), PPG-13-decyltetradecanol polyether-24 (Deyuan China high-tech Co., ltd.).
Example 1A moisturizing composition
The moisturizing composition comprises the following components in parts by weight:
10 parts of oriental cherry flower extract, 1 part of 4D hyaluronic acid, 5 parts of tara gum and 6 parts of vitamin B.
Example 2A moisturizing composition
The moisturizing composition comprises the following components in parts by weight:
30 parts of oriental cherry flower extract, 3 parts of 4D hyaluronic acid, 8 parts of tara gum and 12 parts of vitamin B.
Example 3A moisturizing composition
The moisturizing composition comprises the following components in parts by weight:
20 parts of oriental cherry flower extract, 2 parts of 4D hyaluronic acid, 6 parts of Caesalpinia spinosa gum and 10 parts of vitamin B.
Example 4 Aerosol moisturizing mask composition
The moisturizing mask composition aerosol comprises the following components in percentage by mass:
91.23% of aloe vera leaf water, 1.0% of rosa damascena flower water, 1% of the moisturizing composition of example 1, 2.0% of betaine, 0.22% of PPG-13-decyltetradecanol polyether-24, 0.4% of caprylic/capric triglyceride, 4.0% of polyglycerol, 0.05% of preservative, 0.1% of propellant; the preservative is phenoxyethanol; the propellant is nitrogen.
The preparation method of the moisturizing mask composition aerosol comprises the following steps:
s1, sequentially weighing 9/10 of aloe vera leaf water, rosa damascena flower water, oriental cherry flower extract, betaine and 4D hyaluronic acid, uniformly mixing, heating to 80 ℃, and keeping the temperature and stirring for 20min to obtain a mixture A;
s2, sequentially weighing PPG-13-decyltetradecanol polyether-24 and caprylic/capric triglyceride, mixing, placing in a water bath at 45 ℃, and uniformly stirring to obtain a mixture B;
s3, adding the rest amount of aloe vera leaf water into vitamin B12, and stirring until the aloe vera leaf water is dissolved uniformly to obtain a mixture C;
s4, cooling the mixture A obtained in the step S1 to 40 ℃, adding the uniformly mixed mixture B obtained in the step S2, and stirring for 4min to obtain a mixture D;
s5, adding the Caesalpinia spinosa gel, the preservative and the polyglycerol-6 into the mixture D obtained in the step S4, and stirring for 15min to obtain a mixture E;
s6, adding the pre-dissolved mixture C obtained in the step S3 into the mixture E obtained in the step S5, stirring for 10min, and filtering and discharging through 200-mesh filter cloth to obtain the moisturizing mask composition;
and S7, filling the moisturizing mask composition obtained in the step S6, filling propellant and sealing to obtain the moisturizing mask.
Example 5A moisturizing mask composition Aerosol
The moisturizing mask composition aerosol comprises the following components in percentage by mass:
78.3% of aloe vera leaf water, 3.0% of rosa damascena flower water, 2% of the moisturizing composition of example 2, 4.0% of betaine, 0.5% of PPG-13-decyltetradecanol polyether-24, 1.0% of caprylic/capric triglyceride, 6.0% of polyglycerol-6, 0.2% of preservative, 5.0% of propellant; the preservative is phenoxyethanol; the propellant is nitrogen.
The preparation method of the moisturizing mask composition aerosol comprises the following steps:
s1, sequentially weighing 9/10 of aloe vera leaf water, damascena flower water, cherry flower extract, betaine and 4D hyaluronic acid, uniformly mixing, heating to 85 ℃, and keeping the temperature and stirring for 30min to obtain a mixture A;
s2, sequentially weighing PPG-13-decyl tetradecanol polyether-24 and caprylic/capric triglyceride, mixing, placing in a water bath at 50 ℃, and uniformly stirring to obtain a mixture B;
s3, adding the rest amount of aloe vera leaf water into vitamin B12, and stirring until the mixture is uniformly dissolved to obtain a mixture C;
s4, cooling the mixture A obtained in the step S1 to 45 ℃, adding the uniformly mixed mixture B obtained in the step S2, and stirring for 8min to obtain a mixture D;
s5, adding the Caesalpinia spinosa gel, the preservative and the polyglycerol-6 into the mixture D obtained in the step S4, and stirring for 25min to obtain a mixture E;
s6, adding the pre-dissolved mixture C obtained in the step S3 into the mixture E obtained in the step S5, stirring for 15min, filtering through 200-mesh filter cloth, and discharging to obtain the moisturizing mask composition;
and S7, filling the moisturizing mask composition obtained in the step S6, filling propellant, and sealing to obtain the moisturizing mask composition.
Example 6A moisturizing mask composition Aerosol
The moisturizing mask composition aerosol comprises the following components in percentage by mass:
85.1% of aloe vera leaf water, 2.0% of rosa damascena flower water, 1.5% of the moisturizing composition of example 3, 3.0% of betaine, 0.3% of PPG-13-decyltetradecanol polyether-24, 0.6% of caprylic/capric triglyceride, 5.0% of polyglycerol, 0.1% of preservative, 2.4% of propellant; the preservative is phenoxyethanol; the propellant is nitrogen.
The preparation method of the moisturizing mask composition aerosol comprises the following steps:
s1, sequentially weighing 9/10 of aloe vera leaf water, rosa damascena flower water, oriental cherry flower extract, betaine and 4D hyaluronic acid, uniformly mixing, heating to 85 ℃, and keeping the temperature and stirring for 30min to obtain a mixture A;
s2, sequentially weighing PPG-13-decyltetradecanol polyether-24 and caprylic/capric triglyceride, mixing, placing in a water bath at 50 ℃, and uniformly stirring to obtain a mixture B;
s3, adding the rest amount of aloe vera leaf water into vitamin B12, and stirring until the mixture is uniformly dissolved to obtain a mixture C;
s4, cooling the mixture A obtained in the step S1 to 40 ℃, adding the uniformly mixed mixture B obtained in the step S2, and stirring for 5min to obtain a mixture D;
s5, adding the Caesalpinia spinosa gel, the preservative and the polyglycerol-6 into the mixture D obtained in the step S4, and stirring for 20min to obtain a mixture E;
s6, adding the pre-dissolved mixture C obtained in the step S3 into the mixture E obtained in the step S5, stirring for 12min, filtering through a filter cloth of 200 meshes, and discharging to obtain the moisturizing mask composition;
and S7, filling the moisturizing mask composition obtained in the step S6, filling propellant, and sealing to obtain the moisturizing mask composition.
Comparative example 1 a moisturizing composition
The moisturizing composition comprises the following components in parts by weight:
20 parts of oriental cherry flower extract, 2 parts of 4D hyaluronic acid and 10 parts of vitamin B.
The difference from example 3 is that no tara gum was added.
Comparative example 2 a moisturizing composition
The moisturizing composition comprises the following components in parts by weight:
20 parts of oriental cherry flower extract, 2 parts of 4D hyaluronic acid and 6 parts of Caesalpinia spinosa gum.
The difference from example 3 is that vitamin B12 is not added.
Comparative example 3, moisturizing mask composition aerosol
The moisturizing mask composition aerosol comprises the following components in percentage by mass:
85.1% of aloe vera leaf water, 2.0% of rosa damascena flower water, 1.5% of the moisturizing composition of comparative example 1, 3.0% of betaine, 0.3% of PPG-13-decyltetradecanoyl polyether-24, 0.6% of caprylic/capric triglyceride, 5.0% of polyglycerol, 0.1% of preservative, and 2.4% of propellant; the preservative is phenoxyethanol; the propellant is nitrogen.
The preparation method of the moisturizing mask composition aerosol is similar to that of example 6.
Comparative example 4A moisturizing mask composition Aerosol
The moisturizing mask composition aerosol comprises the following components in percentage by mass:
85.1% of aloe vera leaf water, 2.0% of rosa damascena flower water, 1.5% of the moisturizing composition of comparative example 2, 3.0% of betaine, 0.3% of PPG-13-decyltetradecanoyl polyether-24, 0.6% of caprylic/capric triglyceride, 5.0% of polyglycerol, 0.1% of preservative, and 2.4% of propellant; the preservative is phenoxyethanol; the propellant is nitrogen.
The preparation method of the moisturizing mask composition aerosol is similar to that of example 6.
Test example I, irritation test
The following experiment was performed with reference to "4 skin irritation/corrosion test" in chapter six toxicology experimental methods, cosmetic safety technical specification 2015 edition.
(1) Acute skin irritation test
Selecting 30 adult, healthy and skin-intact white rabbits and males. 30 rabbits were equally divided into 5 groups, i.e., example 4 group, example 5 group, example 6 group, comparative example 3 group, and comparative example 4 group, and 6 rabbits each were tested using the moisturizing mask composition prepared in example 4, example 5, example 6, comparative example 3, and comparative example 4 as a test object. 24h before the test, the hairs on two sides of the spine of the back of the rabbit are cut off, the epidermis cannot be injured, and the hair removing range is 3cm multiplied by 3cm respectively on the left side and the right side. 0.5mL of the test substance was applied directly to the left skin, covered with two layers of gauze (2.5 cm. Times.2.5 cm) and a layer of cellophane, and secured with a non-irritating adhesive tape and bandage. The right skin served as control. The application time is 4h by adopting a sealing test. After the test is finished, the residual test substance is removed by warm water. Skin reactions at the smeared sites were carefully observed for 1, 24, 48 and 72h after removal of the test substances, skin reaction scores were made according to table 1, comprehensive evaluations were made with the mean values of the tested animal scores, and skin irritation intensity was determined according to table 2 based on the highest mean values of the scores at each observation time point of 24, 48 and 72 h.
(2) Multiple skin irritation test
Selecting 30 adult, healthy and skin-intact white rabbits and males. 30 rabbits were equally divided into 5 groups, i.e., example 4, example 5, example 6, comparative example 3, and comparative example 4, and 6 rabbits were divided into 6 groups, and the moisturizing mask compositions prepared in example 4, example 5, example 6, comparative example 3, and comparative example 4 were used as test substances at the time of the experiment. Before the test, the hairs on two sides of the spine of the rabbit are cut off, the hair removing range is 3cm multiplied by 3cm on the left side and the right side respectively, and the smearing area is 2.5cm multiplied by 2.5cm. 0.5mL of the test substance was applied to the left skin and the right skin was used as a control. The application is carried out 1 time per day for 14d. The hair should be cut and the residual test substance removed with water before each application from the next day. The results were observed after one hour and scored according to Table 1, with the control and test zones treated identically. Average integral per animal = ((∑ integral of erythema and edema)/number of test animals)/14 per day, and skin irritation intensity was determined as in table 2.
Table 1: skin irritation response scoring criteria
| Skin reactions | Integration |
| Erythema and char formation | / |
| No erythema | 0 |
| Mild erythema (barely visible) | 1 |
| Obvious erythema | 2 |
| Moderate-severe erythema | 3 |
| Severe erythema (purplish red) to mild dementia | 4 |
| Edema formation | / |
| Without edema | 0 |
| Mild edema (barely visible) | 1 |
| Mild edema (clear outline of skin bulge) | 2 |
| Moderate edema (skin hump about lmm) | 3 |
| Severe edema (skin doming over 1mm, extended range) | 4 |
| Highest integral | 8 |
TABLE 2 skin irritation Strength grading Standard
| Integral mean value | Strength of |
| 0～＜0.5 | Has no irritation |
| 0.5～＜2.0 | Light irritation |
| 2.0～＜6.0 | Middle irritation |
| 6.0～8.0 | Strong irritation |
Acute skin irritation tests showed that no erythema (score 0) nor edema (score 0) was observed by observing the skin reaction of rabbits at 1, 24, 48 and 72 hours after the removal of the test substance. The observation scores at 4 time points of 1, 24, 48 and 72h were all 0 points according to the skin irritation response score standard, and the total of the integrals was also 0 points. As can be seen from the skin irritation intensity grading criteria, the moisturizing mask composition of the present invention is non-irritating. Therefore, the moisturizing facial mask composition is mild and non-irritant.
After multiple skin irritation tests, no erythema (score of 0) and no edema (score of 0) were observed on the skin in all rabbits. The total integral of the skin irritation test after two weeks was 0 point. Therefore, multiple skin irritation tests show that the moisturizing mask composition is mild, free of irritation and high in safety.
Test example two, evaluation of safety
The moisturizing mask compositions prepared in examples 4, 5, 6, 3, and 4 were subjected to a safety test as a test substance with reference to "2-person patch test" in chapter seven method of testing human safety in technical specification for cosmetic safety 2015 edition. 30 eligible subjects were selected for testing, all subjects had healthy skin with no history of skin allergy. Selecting a qualified spot tester, and putting the tested object into the spot tester with the dosage of 0.025g. The spot test device with the tested object is applied to the curved side of the forearm of the tested object by using a non-irritating adhesive tape, and is lightly pressed by hands to be uniformly applied to the skin for 24 hours. And (5) removing the test substance spot tester for 30min, and observing skin reaction after the indentation disappears. If the result is negative, the reaction result is recorded after 24h and 48h of the patch test. The test result shows that all the subjects have no skin adverse reaction, and the tested object is judged to have no skin adverse reaction to the human body. The results show that the moisturizing mask composition has high safety.
Test example III test of moisturizing Effect
Selecting 36 qualified subjects to participate in the test, wherein the male is 20-35 years old and 18 persons; women 20-35 years of age 18, all subjects had healthy skin with no history of skin allergy. 36 subjects were randomly divided into 3 groups, i.e., example 6 group, comparative example 3 group, and comparative example 4 group, and the moisturizing mask composition aerosols prepared in example 6, comparative example 3, and comparative example 4 were used, respectively. The moisture content of the forehead, the left face, the right face and the chin of the subject were measured respectively by using a skin moisture tester, and the average value was taken as the average moisture of the skin before use. After a subject cleans the face, the moisturizing mask composition aerosol is directly and uniformly sprayed on the skin, the skin moisture content of the forehead, the left face, the right face and the chin of the subject at the same positions is tested by a skin moisture tester, and the average value is taken as the average moisture of the skin after use. The test was repeated after 8 h. The test results are shown in table 3.
Table 3: moisturizing effect test results of moisturizing mask composition aerosol
As can be seen from table 3, the average skin moisture of the subjects remained at a high level after 8 hours using the aerosol moisturizing mask composition of example 6 of the present invention, while the average skin moisture of the subjects decreased significantly after 8 hours using the aerosol moisturizing mask compositions of comparative examples 3 and 4. Therefore, the components of the aerosol of the moisturizing mask composition have the moisturizing synergistic effect, so that the moisturizing effect is more durable.
Claims (8)
1. The moisturizing composition is characterized by comprising the following components in parts by mass:
10-30 parts of oriental cherry flower extract, 1-3 parts of 4D hyaluronic acid, 5-8 parts of Caesalpinia spinosa gum and 6-10 parts of vitamin B.
2. The moisturizing composition of claim 1, comprising the following components in parts by mass: 20 parts of oriental cherry flower extract, 2 parts of 4D hyaluronic acid, 6 parts of Caesalpinia spinosa gum and 10 parts of vitamin B.
3. Use of the moisturizing composition of claim 1 or 2 in the preparation of a moisturizing mask skin care product.
4. The aerosol of the moisturizing mask composition is characterized by comprising the following components in percentage by mass:
78.3-91.23% of aloe vera leaf water, 1.0-3.0% of rosa damascena flower water, 1-2% of the moisturizing composition of claim 1 or 2, 2.0-4.0% of betaine, 0.22-0.5% of PPG-13-decyltetradecanol polyether-24, 0.4-1.0% of caprylic/capric triglyceride, 4.0-6.0% of polyglycerol-6, 0.05-0.2% of preservative, 0.1-5.0% of propellant.
5. The moisturizing mask composition aerosol as claimed in claim 4, which is characterized by comprising the following components in percentage by mass:
85.1% of aloe vera leaf water, 2.0% of rosa damascena flower water, 1.5% of the moisturizing composition of claim 1 or 2, 3.0% of betaine, 24.3% of PPG-13-decyltetradecanol polyether, 0.6% of caprylic/capric triglyceride, 6.0% of polyglycerol, 0.1% of a preservative, 2.4% of a propellant.
6. The aerosol pack composition according to claim 4 or 5, wherein the preservative is phenoxyethanol.
7. The aerosol pack composition according to claim 4 or 5, wherein the propellant is nitrogen.
8. A method of preparing an aerosol moisturizing mask composition according to any of claims 4-7 comprising the steps of:
s1, sequentially weighing 9/10 of aloe vera leaf water, rosa damascena flower water, oriental cherry flower extract, betaine and 4D hyaluronic acid, uniformly mixing, heating to 80-85 ℃, and keeping the temperature and stirring for 20-30min to obtain a mixture A;
s2, sequentially weighing PPG-13-decyltetradecanol polyether-24 and caprylic/capric triglyceride, mixing, placing in a water bath at 45-50 ℃, and uniformly stirring to obtain a mixture B;
s3, adding the rest amount of aloe vera leaf water into vitamin B12, and stirring until the mixture is uniformly dissolved to obtain a mixture C;
s4, cooling the mixture A obtained in the step S1 to 40-45 ℃, adding the uniformly mixed mixture B obtained in the step S2, and stirring for 4-8min to obtain a mixture D;
s5, adding the Caesalpinia spinosa gel, the preservative and the polyglycerol-6 into the mixture D obtained in the step S4, and stirring for 15-25min to obtain a mixture E;
s6, adding the pre-dissolved mixture C obtained in the step S3 into the mixture E obtained in the step S5, stirring for 10-15min, filtering through filter cloth of 200 meshes, and discharging to obtain the moisturizing facial mask composition;
and S7, filling the moisturizing mask composition obtained in the step S6, filling propellant, and sealing to obtain the moisturizing mask composition.
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| CN111249175A (en) * | 2020-03-13 | 2020-06-09 | 中山市天图精细化工有限公司 | Carbonic acid moisturizing essence composition aerosol and preparation method thereof |
| CN111450033A (en) * | 2020-04-29 | 2020-07-28 | 刘科勇 | Moisture-keeping nourishing facial mask containing birch juice and its preparation method |
| CN113230188A (en) * | 2021-06-30 | 2021-08-10 | 南京林业大学 | A herba Lycopodii pine needle polysaccharide facial mask with moisturizing and antioxidant effects, and its preparation method |
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2022
- 2022-07-25 CN CN202210879731.2A patent/CN115252492A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111249175A (en) * | 2020-03-13 | 2020-06-09 | 中山市天图精细化工有限公司 | Carbonic acid moisturizing essence composition aerosol and preparation method thereof |
| CN111450033A (en) * | 2020-04-29 | 2020-07-28 | 刘科勇 | Moisture-keeping nourishing facial mask containing birch juice and its preparation method |
| CN113230188A (en) * | 2021-06-30 | 2021-08-10 | 南京林业大学 | A herba Lycopodii pine needle polysaccharide facial mask with moisturizing and antioxidant effects, and its preparation method |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117898987A (en) * | 2024-01-23 | 2024-04-19 | 广州艾柔生物科技有限公司 | Moisturizing aerosol and preparation method thereof |
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