CN115251397A - 一种稳定的乳状矿物质补充物 - Google Patents
一种稳定的乳状矿物质补充物 Download PDFInfo
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- CN115251397A CN115251397A CN202110706051.6A CN202110706051A CN115251397A CN 115251397 A CN115251397 A CN 115251397A CN 202110706051 A CN202110706051 A CN 202110706051A CN 115251397 A CN115251397 A CN 115251397A
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- mineral
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- glycerol
- citrate
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- 235000020786 mineral supplement Nutrition 0.000 title claims abstract description 98
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- 235000011187 glycerol Nutrition 0.000 claims abstract description 99
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 84
- 239000002562 thickening agent Substances 0.000 claims abstract description 75
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 72
- 239000011707 mineral Substances 0.000 claims abstract description 72
- 235000013336 milk Nutrition 0.000 claims abstract description 64
- 239000008267 milk Substances 0.000 claims abstract description 64
- 210000004080 milk Anatomy 0.000 claims abstract description 64
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- 239000001354 calcium citrate Substances 0.000 claims description 55
- 235000013337 tricalcium citrate Nutrition 0.000 claims description 55
- 229960005336 magnesium citrate Drugs 0.000 claims description 54
- 239000004337 magnesium citrate Substances 0.000 claims description 54
- 235000002538 magnesium citrate Nutrition 0.000 claims description 54
- PLSARIKBYIPYPF-UHFFFAOYSA-H trimagnesium dicitrate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O PLSARIKBYIPYPF-UHFFFAOYSA-H 0.000 claims description 54
- WGIWBXUNRXCYRA-UHFFFAOYSA-H trizinc;2-hydroxypropane-1,2,3-tricarboxylate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O WGIWBXUNRXCYRA-UHFFFAOYSA-H 0.000 claims description 53
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
本发明提供一种稳定的乳状矿物质补充物，包含矿物质、甘油、增稠剂和水；防止乳状矿物质补充物低温结晶，防止乳状矿物质补充物低温处理后分层，防止乳状矿物质补充物微生物繁殖，防止乳状矿物质补充物表面变干。
Description
技术领域
本发明涉及一种矿物质补充物，特别涉及一种稳定的乳状矿物质补充物。
背景技术
对于矿物质补充物，液态矿物质补充剂更加适口，且能够适合于任何年龄段的人群，尤其是婴幼儿和儿童，不需要咀嚼，并且无卡住咽喉、气管的风险。液态矿物质补充剂产品多数含白砂糖，糖尿病患者和需要控制糖分摄入的人群不适用；几乎都添加防腐剂；更显著的是，因矿物质的溶解性问题，如柠檬酸钙、碳酸钙、柠檬酸镁、碳酸镁、柠檬酸锌等，液态矿物质补充剂几乎都做成乳状的非牛顿流体，以承载住不溶性矿物质盐的微粒。而乳状液体在低温条件下体系内含的水份冷冻结晶使乳化结构被破坏导致物料分层，产品稳定性和观感下降，影响后续的产品使用，还会以为体积变化导致外包装变形，影响产品的外观感受。
此外，开封后物料失水会导致产品的浓度增加，或者表面物料变干。
发明内容
本发明的目的在于针对现有技术的不足之处，提供一种稳定的乳状矿物质补充物，包含矿物质、多元醇、增稠剂和水，所述多元醇包括甘油、丙二醇的一种或两种组合。
进一步的，矿物质包括钙盐、镁盐、锌盐、铁盐中的一种或者两种以上的组合。
进一步的，所述矿物质含有不溶性或者微溶性的矿物质。
进一步的，钙盐可以是任何已知用于口服营养产品中的不溶性钙盐，包括柠檬酸钙、碳酸钙、苏糖酸钙、磷酸氢钙、焦磷酸钙、磷酸三钙的一种或两种以上的组合。
进一步的，镁盐可以是任何已知用于口服营养产品中的不溶性镁盐，镁盐包括柠檬酸镁、碳酸镁、苏糖酸镁、磷酸氢镁、焦磷酸镁、磷酸镁的一种或两种以上的组合。
进一步的，锌盐可以是任何已知用于口服营养产品中的不溶性锌盐，进一步的，锌盐包括柠檬酸锌、碳酸锌、苏糖酸锌、磷酸氢锌、焦磷酸铁、磷酸铁的一种或两种以上的组合。
进一步的，铁盐可以是任何已知用于口服营养产品中的不溶性铁盐，进一步的，铁盐包括柠檬酸铁、柠檬酸铁铵、苏糖酸铁、焦磷酸锌、磷酸铁、硫酸亚铁，琥珀酸亚铁、富马酸亚铁，甘氨酸亚铁的一种或两种以上的组合。
进一步的，关于矿物质的粒径，矿物质D90≤10μm；进一步的，矿物质D95≤10μm，进一步的，矿物质D97≤10μm。或矿物质D97≤50μm，进一步的，矿物质D97≤30μm，进一步的，矿物质D97≤30μm，进一步的，矿物质D97≤10μm。
进一步的，增稠剂包括黄原胶、瓜尔胶、角叉菜胶、结冷胶、阿拉伯胶、茄替胶、刺梧桐胶、黄蓍胶、琼脂、帚叉藻聚糖、刺槐豆胶、果胶、低甲氧基果胶、明胶、微晶纤维素、CMC(羧甲基纤维素钠)、甲基纤维素、羟丙基甲基纤维素、羟丙基纤维素、DATEM(甘油单酯和甘油二酯的二乙酰酒石酸酯)、葡聚糖、CITREM(甘油单酯和甘油二酯的柠檬酸酯)、具有增稠作用的变形淀粉一种或两种以上的组合。
进一步的，所述多元醇包括甘油，甘油的用量为0.5％-50％，进一步的，甘油的用量为1％-45％，进一步的，甘油的用量为5％-40％，进一步的，甘油的用量为10％-35％，进一步的，甘油的用量为20％-30％，进一步的，甘油的用量为21％-29％，进一步的，甘油的用量为26％。
进一步的，增稠剂用量为0.01-10％，进一步的，增稠剂用量为0.05-5％，进一步的，增稠剂用量为0.1-1％，进一步的，增稠剂用量为0.15-0.5％。
进一步的，增稠剂的粘度大于100cp，进一步的，增稠剂的粘度大于200cp，进一步的，增稠剂的粘度大于300cp，进一步的，增稠剂的粘度大于400cp，进一步的，增稠剂的粘度大于500cp，进一步的，增稠剂的粘度大于600cp。
进一步的，补充物含有甜味剂，包括麦芽糖糊精、葡萄糖聚合物、玉米糖浆、蔗糖、葡萄糖、果糖、乳糖、蜂蜜、糖醇(例如，麦芽糖醇、赤藓糖醇、山梨糖醇、木糖醇)、人造甜味剂(例如，蔗糖素(sucralose)、乙酰氨基磺酸钾、甜菊糖的一种或两种以上的组合。优选的，甜味剂选择为赤藻糖醇、山梨糖醇、甜菊糖中的一种或两种以上的组合。
进一步的，补充物中含有香精，包括水果香精和奶味香精，进一步优选为橙子香精和酸奶香精。
进一步的，补充物中含有维生素及其衍生物和/或前体，包括维生素A、B族中的一种或两种以上的组合、C、D、E、K、U，β-胡萝卜素，优选为维生素D和/或维生素K，进一步优选为维生素D3和/或维生素K2。维生素D3的用量在所在国家、地区的要求范围之内，优选为0.000784％。
进一步的，补充物的含有酸味剂，包括苹果酸、乙酸、柠檬酸、富马酸、酒石酸中的一种或两种以上的组合，优选为柠檬酸。
进一步的，补充物含：矿物质盐1-100份，水1-100份，甘油1-100份，增稠剂0.01-10份；进一步的，补充物含：矿物质盐1-50份，水10-100份，甘油1-50份，增稠剂0.1-5份；进一步的，补充物含：矿物质盐5-20份，水30-80份，甘油8-30份，增稠剂0.1-1份；进一步的，补充物含：矿物质盐13份，水50份，甘油21份，增稠剂0.2份。
进一步的，补充物中不含有蛋白质，或者含有微量的蛋白质，或者含有少量的蛋白质。在一个实施方案中，蛋白质含量为0；在另一实施方案中，蛋白质的含量为小于0.01％、0.1％、0.5％、1％、2％、5％。本发明补充物中的乳状补充物的形态和感官性质，依赖于不溶性矿物质盐和增稠剂，以及甘油的添加，并不依赖于蛋白，更不依赖于乳蛋白。本发明的方案不同于CN104981170A与其同族的报道，本发明的方案并非必然使用在牛乳等乳制品中，而主要为制备成乳状，进而提供矿物质补充。
所述一种稳定的乳状矿物质补充物，为稳定的非牛顿流体。稳定的乳状矿物质补充物避免了经过低温冷冻后物料性质变化导致的物料不均一；稳定的乳状矿物质减轻了传统矿物质补充乳剂产品开封后因失水导致的表面物料变干问题。
传统的乳状矿物质体系中含有增稠剂和不溶性矿物质盐，常温下增稠剂承载着不溶性矿物质盐，不会发生分层和物料不均一的情况。对于乳状的增稠剂和不溶性矿物质盐的体系，低温环境下，增稠剂、水和不溶性矿物质盐变得不稳定，尤其是水分一旦结晶，增稠剂脱离使得体系无法起到不溶性矿物质的承载作用。
在传统的含有增稠剂的乳状矿物质体系中添加多元醇，例如甘油，甘油具有持水性，并且能够充分溶胀体系中的增稠剂，使得承载体系更加稳定，避免了在低温条件下内含的水份冷冻结晶会使乳化结构被破坏导致物料分层的情况，产品稳定性和观感得到提升。并且结晶后体积变化，会使得外包装变形，如塑料包装瓶体变形，即使当结晶在常温下融化后，外包装瓶体的变形无法复原，尤其是塑料包装瓶体变形几乎无法复原。
传统矿物质补充乳剂产品，通常为瓶装，一次取用一勺或若干勺，传统矿物质补充乳剂产品开封后因失水导致的表面物料变干问题，而甘油具有吸湿性和持水性，能够明显改善产品开封后因失水导致的表面物料变干的情形。
所述一种稳定的乳状矿物质补充物，可以不添加防腐剂，或者添加更小剂量的防腐剂，也能够达到防腐的效果。
多元醇，例如甘油，能够提高产品的渗透压，不利于产品的微生物繁殖；另一方面，甘油能够提供一定的甜度，减少了乳状矿物质补充物中甜味剂的使用，尤其是如果糖、葡萄糖、蔗糖的使用，微生物缺少碳源，使得产品不利于微生物繁殖。需要说明的是，甘油的添加并不排斥甜味剂的使用，尤其是不排斥赤藻糖醇、山梨糖醇、甜菊糖等人工甜味剂或提取的甜味剂的使用。
本发明提供一种防止乳状矿物质补充物低温结晶的方法，在含有不溶性矿物质盐和增稠剂的体系中，添加多元醇，例如甘油，。
本发明提供一种防止乳状矿物质补充物低温处理后分层的方法，在含有不溶性矿物质盐和增稠剂的体系中，添加多元醇，例如甘油，。
本发明提供一种防止乳状矿物质补充物微生物繁殖的方法，在含有不溶性矿物质盐和增稠剂的体系中，添加多元醇，例如甘油，。
本发明提供一种防止乳状矿物质补充物表面变干的方法，在含有不溶性矿物质盐和增稠剂的体系中，添加多元醇，例如甘油，。
本发明提供一种多元醇，例如甘油，在含有不溶性矿物质盐和增稠剂的乳状矿物质补充物中的用途，防止乳状矿物质补充物低温结晶，和/或防止乳状矿物质补充物低温处理后分层，和/或防止乳状矿物质补充物微生物繁殖，和/或防止乳状矿物质补充物表面变干。
本发明提供一种乳状矿物质补充物的制备方法，加水前，将多元醇，例如甘油，与增稠剂混合。
进一步的，增稠剂与矿物质盐和/或甜味剂和/或其他添加剂(如香精)混合，然后与多元醇，例如甘油，混合。
进一步的，增稠剂与一部分矿物质盐和/或甜味剂和/或其他添加剂(如香精)混合，然后与甘油充分混合。
干物质，尤其是增稠剂，之间的空隙由多元醇填满，避免直接接触水后表面形成胶，内核还是粉末后结块，更进一步降低了乳状矿物质补充物低温处理后分层的风险。
进一步的，酸味剂与不溶性矿物质盐在水环境中混合后，再与体系中其他成分混合。
术语解释
本文所用“不溶性盐”、“不溶性矿物质”、“不溶性矿物质盐”具有可以相互替换使用，在未标明的情况下，指是的人体所需矿物质盐，该盐为不溶性的。
本文所用的“不溶性盐”是指在室温下基本不溶于水的盐，并且特别是指在室温下小于1wt.％或小于0.5wt.％或小于0.1wt.％溶于水的盐。
本文所用的“增稠剂”是指形成负载体系，能够使得乳状补充物能够增稠稳定的原料。
本文所用的术语“婴儿配方”，在未标明的情况下，是指液体婴儿配方和小儿配方，其中婴儿配方意在用于最多约1岁的婴儿，幼儿配方意在用于从约1岁至约12岁的儿童。
除非另外规定，如本文所用的所有百分数、份数和比例以总组合物的重量计。除非另外规定，所有这种重量在其关于所列成分时是基于活性水平，并因此不包括市售物质中可能包括的溶剂或副产物。
本文所用的“产品”，所用的“补充物”，在未标明的情况下，是指，含有不溶性/微溶性矿物质，甘油和增稠剂的体系，形成的补充剂产品。
附图说明
图1为将实施例1的样品A和样品B置于冷冻环境的情形。
图2为将实施例1的样品A和样品B从冷冻环境中取出的情形。
图3为测量实施例1冷冻后样品A粘度的情形。
图4为测量实施例1冷冻后样品B粘度的情形。
图5为不同混匀方式的对照情形。
具体实施方式
为了便于本领域技术人员的理解，下面结合实施例对本发明作进一步的说明，实施方式提及的内容并非对本发明的限定。
实施例1
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份。
实施例2
一种稳定的乳状矿物质补充物，包含柠檬酸钙10份、黄原胶0.2份、甘油21份和水56份。
实施例3
一种稳定的乳状矿物质补充物，包含柠檬酸镁10份、黄原胶0.2份、甘油21份和水56份。
实施例4
一种稳定的乳状矿物质补充物，包含柠檬酸锌10份、黄原胶0.2份、甘油21份和水56份。
实施例5
一种稳定的乳状矿物质补充物，包含焦磷酸铁10份、黄原胶0.2份、甘油21份和水56份。
实施例6
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、黄原胶0.2份、甘油21份和水56份。
实施例7
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份、山梨糖醇9份和水56份。
实施例8
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份、果糖24份和水56份。
实施例9
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份、山梨糖醇9份、维生素D3为0.0008份和水56份。
实施例10
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份、山梨糖醇9份、维生素D3为0.0008份、橙子香精0.07份、酸奶香精0.01份、柠檬酸0.5份和水56份。
实施例11
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、柠檬酸镁5份、柠檬酸锌2份、黄原胶0.3份、甘油27份和水45份。
实施例12
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、黄原胶0.3份、甘油27份和水45份。
实施例13
一种稳定的乳状矿物质补充物，包含柠檬酸镁5份、黄原胶0.3份、甘油27份和水45份。
实施例14
一种稳定的乳状矿物质补充物，包含柠檬酸锌2份、黄原胶0.3份、甘油27份和水45份。
实施例15
一种稳定的乳状矿物质补充物，包含焦磷酸铁2份、黄原胶0.3份、甘油27份和水45份。
实施例16
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、柠檬酸锌2份、黄原胶0.3份、甘油27份和水45份。
实施例17
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、柠檬酸镁5份、黄原胶0.3份、甘油27份和水45份。
实施例18
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、柠檬酸镁5份、柠檬酸锌2份、黄原胶0.3份、甘油27份、山梨糖醇9份和水45份。
实施例19
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、柠檬酸镁5份、柠檬酸锌2份、黄原胶0.3份、甘油27份、山梨糖醇9份、维生素D3为0.001份和水45份。
实施例20
一种稳定的乳状矿物质补充物，包含柠檬酸钙8份、柠檬酸镁5份、柠檬酸锌2份、黄原胶0.3份、甘油27份、山梨糖醇9份、维生素D3为0.001份、香精0.08份和水45份。
实施例21
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、瓜尔胶0.2份、甘油21份和水56份。
实施例22
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、卡拉胶0.2份、甘油21份和水56份。
实施例23
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、结冷胶0.3份、甘油21份和水56份。
实施例24
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、羧甲基淀粉钠0.05份、甘油21份和水56份。
实施例25
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、羧甲基纤维素钠(CMC)0.04份、甘油21份和水56份。
实施例26
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、决明胶0.08份、甘油21份和水56份。
实施例27
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、田菁胶0.08份、甘油21份和水56份。
实施例28
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、果胶0.08份、甘油21份和水56份。
实施例29
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、阿拉伯胶0.08份、甘油21份和水56份。
实施例30
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、海藻酸钠0.09份、甘油21份和水56份。
实施例31
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油2份、柠檬酸0.5份和水50份。
实施例32
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油4份和水50份。
实施例33
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油10份和水50份。
实施例34
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油20份和水50份。
实施例35
一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油50份和水50份。
实施例36
一种乳状矿物质补充物的制备方法，包括步骤：加水前，将甘油与增稠剂混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份。
实施例37
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与矿物质混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份。
实施例38
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与部分矿物质混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份。
实施例39
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与山梨糖醇混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份、山梨糖醇9份。
实施例40
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与部分山梨糖醇混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份、山梨糖醇9份。
实施例41
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与部分矿物质、部分山梨糖醇混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份。
实施例42
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与部分矿物质、部分山梨糖醇混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、丙二醇21份和水56份。
实施例43
一种乳状矿物质补充物的制备方法，包括步骤：加水前，增稠剂与部分矿物质、部分山梨糖醇混合，再将甘油于与混合物进行混合。增稠剂为黄原胶；矿物质包含柠檬酸钙、柠檬酸镁、柠檬酸锌，柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油10份、丙二醇11份和水56份。
试验例1
将实施例1作为样品A，一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份，对照组作为样品B，为一种乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、水77份，原料的粒径、生产厂家和制备步骤均相同，都是常规混合并均质。将样品A和样品B分别置于-30℃环境下24h静置。
观察样品A和样品B，由图2可以看出，样品A没有变化，样品B结晶并有所鼓胀。可见，添加甘油使得产品的稳定性更好，能够耐低温冷冻不结晶、不分层。
在实际的产品运输过程中，很少遇到-30℃环境，但会遇到长时间在零下的情形，尤其是在冬季，因此低温稳定性是产品性状稳定的关键因素之一。
试验例2
将实施例1作为样品A，一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份，对照组作为样品B，为一种乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、水77份，原料的粒径、生产厂家和制备步骤均相同，都是常规混合并均质，测量样品粘度，因样品为非牛顿流体，测量的条件选择为室温20℃，测量的转速为30rpm，旋转10秒时的粘度。将样品A和样品B分别置于-30℃环境下24h静置。取出后立即测量样品粘度，测量的外部条件为室温，测量的转速为30rpm，旋转10秒时的粘度。对于样品A，冷冻前：2056mPa*s，冷冻后：1884mPa*s；对于样品B，冷冻前：1620mPa*s，冷冻后：872mPa*s。样品A的粘度下降为原粘度的91.6％，样品B的粘度下降为原粘度的53.8％，可见不溶性矿物质盐、增稠剂和甘油形成的体系使得产品的稳定性更好，能够耐低温冷冻粘度变化很小，性状稳定，更不易分层。
试验例3
将实施例1作为样品A，一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份，对照组作为样品B，为一种乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、水77份，原料的粒径、生产厂家和制备步骤均相同，都是常规混合并均质。灌装成瓶的环境为10万级洁净空间。灌装后不进行热杀菌处理。
参考欧洲药典9.0th<5.1.3>防腐功效测试；表中对数下降值为Log10(初始菌数/复苏菌数)。
测试结果如下：
表1试验例3中样品A的防腐调整情况
表2试验例3中样品B的防腐调整情况
结合表1和表2，可以看出添加了甘油明显抑制了大肠埃希氏菌和铜绿假单胞菌的繁殖，在防腐挑战中能够显著提高产品的抗菌效果。
试验例4
将实施例1作为样品，一种稳定的乳状矿物质补充物，包含柠檬酸钙6份、柠檬酸镁4份、柠檬酸锌1份、黄原胶0.2份、甘油21份和水56份。加水前，将甘油与黄原胶混合，充分混匀，然后与其他原料混合均质，作为样品A。另取相同量的原料，直接混匀均质，作为样品B。样品A和样品B分别进行低温静置。
结果如图5，左侧为样品A，右侧为样品B，对照可以看出，样品A更加的均一，没有黄原胶块。因此，将甘油与加水前，将甘油与增稠剂混合。能够进一步的提高产品的稳定性，防止低温处理后的分层风险。
综上，由不溶性矿物质盐、增稠剂、多元醇组成的乳状矿物质补充物体系更加的稳定，防止乳状矿物质补充物低温结晶，和/或防止乳状矿物质补充物低温处理后分层，和/或防止乳状矿物质补充物微生物繁殖，和/或防止乳状矿物质补充物表面变干。
本技术领域技术人员可以理解，除非另外定义，这里使用的所有术语(包括技术术语和科学术语)，具有与本发明所属领域中的普通技术人员的一般理解相同的意义。还应该理解的是，诸如通用字典中定义的那些术语，应该被理解为具有与现有技术的上下文中的意义一致的意义，并且除非像这里一样被特定定义，否则不会用理想化或过于正式的含义来解释。
应当理解，以上借助优选实施例对本发明的技术方案进行的详细说明是示意性的而非限制性的。本领域的普通技术人员在阅读本发明说明书的基础上可以对各实施例所记载的技术方案进行修改，或者对其中部分技术特征进行等同替换；而这些修改或者替换，并不使相应技术方案的本质脱离本发明各实施例技术方案的精神和范围。
Claims (10)
1.一种稳定的乳状矿物质补充物，包含矿物质、多元醇、增稠剂和水；所述多元醇包括甘油、丙二醇的一种或两种组合。
2.根据权利要求1所述的补充物，其特征在于，矿物质包括钙盐、镁盐、锌盐、铁盐中的一种或者两种以上的组合。
3.根据权利要求1所述的补充物，其特征在于，所述矿物质含有不溶性或者微溶性的矿物质。
4.根据权利要求1所述的补充物，其特征在于，钙盐包括柠檬酸钙、碳酸钙、苏糖酸钙、磷酸氢钙、焦磷酸钙、磷酸三钙的一种或两种以上的组合；
和/或
镁盐包括柠檬酸镁、碳酸镁、苏糖酸镁、磷酸氢镁、焦磷酸镁、磷酸镁的一种或两种以上的组合；
和/或
锌盐包括柠檬酸锌、碳酸锌、苏糖酸锌、磷酸氢锌、焦磷酸铁、磷酸铁的一种或两种以上的组合；
和/或
铁盐包括柠檬酸铁、柠檬酸铁铵、苏糖酸铁、焦磷酸锌、磷酸铁、硫酸亚铁，琥珀酸亚铁、富马酸亚铁，甘氨酸亚铁的一种或两种以上的组合；
和/或
增稠剂包括黄原胶、瓜尔胶、角叉菜胶、结冷胶、阿拉伯胶、茄替胶、刺梧桐胶、黄蓍胶、琼脂、帚叉藻聚糖、刺槐豆胶、果胶、低甲氧基果胶、明胶、微晶纤维素、CMC、甲基纤维素、羟丙基甲基纤维素、羟丙基纤维素、DATEM、葡聚糖、CITREM、具有增稠作用的变性淀粉一种或两种以上的组合。
5.根据权利要求1所述的补充物，其特征在于，关于矿物质的粒径，矿物质D90≤10μm；进一步的，矿物质D95≤10μm，进一步的，矿物质D97≤10μm。或矿物质D97≤50μm，进一步的，矿物质D97≤30μm，进一步的，矿物质D97≤30μm，进一步的，矿物质D97≤10μm。
6.根据权利要求1所述的补充物，其特征在于，补充物含有甜味剂，包括麦芽糖糊精、葡萄糖聚合物、玉米糖浆、蔗糖、葡萄糖、果糖、乳糖、蜂蜜、糖醇、蔗糖素、乙酰氨基磺酸钾、甜菊糖的一种或两种以上的组合。优选的，甜味剂选择为赤藻糖醇、山梨糖醇、甜菊糖中的一种或两种以上的组合；
和/或
补充物的含有酸味剂，包括苹果酸、乙酸、柠檬酸、富马酸、酒石酸中的一种或两种以上的组合，优选为柠檬酸。
和/或
补充物中含有维生素及其衍生物和/或前体，包括维生素A、B族中的一种或两种以上的组合、C、D、E、K、U，β-胡萝卜素，优选为维生素D和/或维生素K，进一步优选为维生素D3和/或维生素K2。
7.根据权利要求1所述的补充物，其特征在于，所述多元醇为甘油，甘油的用量为0.5％-50％，进一步的，甘油的用量为1％-45％，进一步的，甘油的用量为5％-40％，进一步的，甘油的用量为10％-35％，进一步的，甘油的用量为20％-30％，进一步的，甘油的用量为21％-29％，进一步的，甘油的用量为26％；
和/或
增稠剂用量为0.01-10％，进一步的，增稠剂用量为0.05-5％，进一步的，增稠剂用量为0.1-1％，进一步的，增稠剂用量为0.15-0.5％；
和/或
增稠剂的粘度大于100cp，进一步的，增稠剂的粘度大于200cp，进一步的，增稠剂的粘度大于300cp，进一步的，增稠剂的粘度大于400cp，进一步的，增稠剂的粘度大于500cp，进一步的，增稠剂的粘度大于600cp；
和/或
补充物含：矿物质盐1-100份，水1-100份，甘油1-100份，增稠剂0.01-10份；进一步的，补充物含：矿物质盐1-50份，水10-100份，甘油1-50份，增稠剂0.1-5份；进一步的，补充物含：矿物质盐5-20份，水30-80份，甘油8-30份，增稠剂0.1-1份；进一步的，补充物含：矿物质盐13份，水50份，甘油21份，增稠剂0.2份。
8.一种多元醇在含有不溶性矿物质盐和增稠剂的乳状矿物质补充物中的用途，所述多元醇包括甘油、丙二醇的一种或两种组合，防止乳状矿物质补充物低温结晶，和/或防止乳状矿物质补充物低温处理后分层，和/或防止乳状矿物质补充物微生物繁殖，和/或防止乳状矿物质补充物表面变干。
9.一种乳状矿物质补充物的制备方法，其特征在于，加水前，将多元醇与增稠剂混合，所述多元醇包括甘油、丙二醇的一种或两种组合。
10.根据权利要求9的方法，其特征在于，增稠剂与矿物质盐和/或甜味剂和/或其他添加剂混合，然后与多元醇混合；所述多元醇包括甘油、丙二醇的一种或两种组合；进一步的，增稠剂与一部分矿物质盐和/或甜味剂和/或其他添加剂混合，然后与甘油充分混合。
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