CN115227631A - Anhydrous essence composition and preparation method and application thereof - Google Patents
Anhydrous essence composition and preparation method and application thereof Download PDFInfo
- Publication number
- CN115227631A CN115227631A CN202210810700.1A CN202210810700A CN115227631A CN 115227631 A CN115227631 A CN 115227631A CN 202210810700 A CN202210810700 A CN 202210810700A CN 115227631 A CN115227631 A CN 115227631A
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- CN
- China
- Prior art keywords
- anhydrous
- essence composition
- parts
- essence
- solvent
- Prior art date
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- Pending
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- 239000000203 mixture Substances 0.000 title claims abstract description 70
- 238000002360 preparation method Methods 0.000 title abstract description 19
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 48
- 230000003020 moisturizing effect Effects 0.000 claims abstract description 34
- 239000002562 thickening agent Substances 0.000 claims abstract description 34
- 239000002904 solvent Substances 0.000 claims abstract description 30
- 239000003974 emollient agent Substances 0.000 claims abstract description 29
- 239000003755 preservative agent Substances 0.000 claims abstract description 22
- 230000002335 preservative effect Effects 0.000 claims abstract description 21
- 239000003906 humectant Substances 0.000 claims abstract description 12
- 150000001875 compounds Chemical class 0.000 claims abstract description 11
- 239000000443 aerosol Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 3
- 239000002131 composite material Substances 0.000 claims description 38
- 239000000047 product Substances 0.000 claims description 34
- 238000003756 stirring Methods 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 238000006243 chemical reaction Methods 0.000 claims description 16
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 15
- 239000000284 extract Substances 0.000 claims description 15
- 238000000855 fermentation Methods 0.000 claims description 15
- 230000004151 fermentation Effects 0.000 claims description 15
- 239000011259 mixed solution Substances 0.000 claims description 14
- 239000013557 residual solvent Substances 0.000 claims description 14
- 239000003009 skin protective agent Substances 0.000 claims description 13
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims description 12
- 244000144927 Aloe barbadensis Species 0.000 claims description 11
- 235000002961 Aloe barbadensis Nutrition 0.000 claims description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 11
- 235000011399 aloe vera Nutrition 0.000 claims description 11
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 11
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 claims description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 229920001577 copolymer Polymers 0.000 claims description 9
- 150000002148 esters Chemical class 0.000 claims description 9
- 241000186660 Lactobacillus Species 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- 229940039696 lactobacillus Drugs 0.000 claims description 8
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 8
- -1 polydimethylsiloxane Polymers 0.000 claims description 8
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims description 7
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims description 7
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 claims description 7
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 7
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 7
- 229940057910 shea butter Drugs 0.000 claims description 7
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 6
- 229960000458 allantoin Drugs 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 235000011187 glycerol Nutrition 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 5
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 5
- 229960000735 docosanol Drugs 0.000 claims description 5
- 229960005323 phenoxyethanol Drugs 0.000 claims description 5
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 5
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 5
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims description 4
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims description 4
- QFOHBWFCKVYLES-UHFFFAOYSA-N Butylparaben Chemical compound CCCCOC(=O)C1=CC=C(O)C=C1 QFOHBWFCKVYLES-UHFFFAOYSA-N 0.000 claims description 4
- YDNKGFDKKRUKPY-JHOUSYSJSA-N C16 ceramide Natural products CCCCCCCCCCCCCCCC(=O)N[C@@H](CO)[C@H](O)C=CCCCCCCCCCCCCC YDNKGFDKKRUKPY-JHOUSYSJSA-N 0.000 claims description 4
- 244000068988 Glycine max Species 0.000 claims description 4
- 235000010469 Glycine max Nutrition 0.000 claims description 4
- 239000004909 Moisturizer Substances 0.000 claims description 4
- CRJGESKKUOMBCT-VQTJNVASSA-N N-acetylsphinganine Chemical compound CCCCCCCCCCCCCCC[C@@H](O)[C@H](CO)NC(C)=O CRJGESKKUOMBCT-VQTJNVASSA-N 0.000 claims description 4
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims description 4
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 4
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims description 4
- 229940059958 centella asiatica extract Drugs 0.000 claims description 4
- 229940106189 ceramide Drugs 0.000 claims description 4
- ZVEQCJWYRWKARO-UHFFFAOYSA-N ceramide Natural products CCCCCCCCCCCCCCC(O)C(=O)NC(CO)C(O)C=CCCC=C(C)CCCCCCCCC ZVEQCJWYRWKARO-UHFFFAOYSA-N 0.000 claims description 4
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 4
- 230000001333 moisturizer Effects 0.000 claims description 4
- VVGIYYKRAMHVLU-UHFFFAOYSA-N newbouldiamide Natural products CCCCCCCCCCCCCCCCCCCC(O)C(O)C(O)C(CO)NC(=O)CCCCCCCCCCCCCCCCC VVGIYYKRAMHVLU-UHFFFAOYSA-N 0.000 claims description 4
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 4
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical class CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 3
- 239000004475 Arginine Substances 0.000 claims description 3
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims description 3
- 241000519987 Scutellaria alpina Species 0.000 claims description 3
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 claims description 3
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims description 3
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 3
- 229960002216 methylparaben Drugs 0.000 claims description 3
- 229940101267 panthenol Drugs 0.000 claims description 3
- 235000020957 pantothenol Nutrition 0.000 claims description 3
- 239000011619 pantothenol Substances 0.000 claims description 3
- 229940095110 selaginella tamariscina extract Drugs 0.000 claims description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
- UOQHWNPVNXSDDO-UHFFFAOYSA-N 3-bromoimidazo[1,2-a]pyridine-6-carbonitrile Chemical compound C1=CC(C#N)=CN2C(Br)=CN=C21 UOQHWNPVNXSDDO-UHFFFAOYSA-N 0.000 claims description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 2
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 claims description 2
- 241000226556 Leontopodium alpinum Species 0.000 claims description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims description 2
- BBAFBDLICMHBNU-MFZOPHKMSA-N N-(2-hydroxyoctadecanoyl)-4-hydroxysphinganine Chemical compound CCCCCCCCCCCCCCCCC(O)C(=O)N[C@@H](CO)[C@H](O)[C@H](O)CCCCCCCCCCCCCC BBAFBDLICMHBNU-MFZOPHKMSA-N 0.000 claims description 2
- KZTJQXAANJHSCE-OIDHKYIRSA-N N-octodecanoylsphinganine Chemical compound CCCCCCCCCCCCCCCCCC(=O)N[C@@H](CO)[C@H](O)CCCCCCCCCCCCCCC KZTJQXAANJHSCE-OIDHKYIRSA-N 0.000 claims description 2
- ATGQXSBKTQANOH-UWVGARPKSA-N N-oleoylphytosphingosine Chemical compound CCCCCCCCCCCCCC[C@@H](O)[C@@H](O)[C@H](CO)NC(=O)CCCCCCC\C=C/CCCCCCCC ATGQXSBKTQANOH-UWVGARPKSA-N 0.000 claims description 2
- 241000235347 Schizosaccharomyces pombe Species 0.000 claims description 2
- GCDXVKZXCQGDHC-BLCQCPAESA-N [30-oxo-30-[[(2s,3s,4r)-1,3,4-trihydroxyoctadecan-2-yl]amino]triacontyl] (9z,12z)-octadeca-9,12-dienoate Chemical compound CCCCCCCCCCCCCC[C@@H](O)[C@@H](O)[C@H](CO)NC(=O)CCCCCCCCCCCCCCCCCCCCCCCCCCCCCOC(=O)CCCCCCC\C=C/C\C=C/CCCCC GCDXVKZXCQGDHC-BLCQCPAESA-N 0.000 claims description 2
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- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims description 2
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims description 2
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- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims description 2
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 7
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- 125000002511 behenyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 4
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- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 description 3
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 2
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- LDXJRKWFNNFDSA-UHFFFAOYSA-N 2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]ethanone Chemical compound C1CN(CC2=NNN=C21)CC(=O)N3CCN(CC3)C4=CN=C(N=C4)NCC5=CC(=CC=C5)OC(F)(F)F LDXJRKWFNNFDSA-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract
The invention discloses an anhydrous essence composition, a preparation method and an application thereof, wherein the anhydrous essence composition comprises the following components: 75-95 parts of solvent, 10-20 parts of humectant, 2-5 parts of emollient, 5-10 parts of compound emulsifier, 0.1-10 parts of skin protectant, 0.1-1 part of pH regulator, 0.1-3 parts of thickener and 0.1-2 parts of preservative. The anhydrous essence composition is prepared by adding the solvent with the moisturizing effect as the solvent and combining a plurality of active ingredients with specific compound emulsion, thickening agent and the like, has better skin moisturizing and soothing effects, and is high in stability; the method is applied to preparing the anhydrous essence composition aerosol, fills the vacancy of the anhydrous essence composition aerosol on the market, and has good market prospect.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an anhydrous essence composition as well as a preparation method and application thereof.
Background
In recent years, with the rapid increase of Chinese economy, cosmetic consumers in China rise rapidly, and consumers are more and more willing to use skin care products to maintain the skin health of themselves and keep a good skin state. The product homogeneity among various brands of cosmetics is increasingly obvious and lacks of identification, and consumers expect more personalized customized products. In recent years, people work in air-conditioned rooms or dry environments for a long time, the problem of skin water shortage is increasingly serious, the skin of people is enabled to be dry, the skin aging speed is accelerated, the past grease skin care cannot meet the requirements of modern people on moisturizing and moisturizing cosmetics, more and more people like moisturizing agents with better moisturizing and soothing performances, and meanwhile, along with the improvement of science and technology, the requirements of people on products are simpler and more convenient. With the continuous development of people on the cognition of cosmetics, the method quickly and effectively solves the problem of personal skin and improves the skin state, and becomes the mainstream trend of the product demand of consumers. However, most of solvents of the essence products on the market are water, and the water can only reach the horny layer in the facial skin and cannot be absorbed, so that the moisturizing and relieving performance is reduced, and the anhydrous essence products are more and more popular.
Chinese patent document CN111346036A discloses an anhydrous facial mask containing aloe vera leaf water and a preparation method thereof in 2020, 6 months and 30 days, wherein the anhydrous facial mask is prepared by using the aloe vera leaf water instead of water as a solvent, has good effects of moisture retention, soothing and repairing, and the like, and indicates that anhydrous products start to continuously land in domestic markets to become circulation products; chinese patent document CN112472614A discloses anhydrous hyaluronic acid essence and a preparation method thereof in 2021, 3 months and 12 days, the bifidus yeast fermentation product filtrate replaces water, and sodium hyaluronate with common molecular weight, hydrolyzed sodium hyaluronate and low molecular weight are mixed for use, so that the anhydrous hyaluronic acid essence has a good moisturizing effect; chinese patent document CN113559023A discloses an anhydrous yeast essence filtrate and a preparation method thereof in 29/10.1.A rose hydrosol is used for replacing water to dissolve various active ingredients in a yeast schizolysis solution, a yeast extract and a yeast fermentation product filtrate extract, so that the moisture content of skin is effectively improved; however, the anhydrous essence product has single active ingredients, the moisturizing and relieving effects are not good, and in the field of cosmetics, the cosmetic composition is very sensitive to the aspects of texture, system stability and the like, and many products in the market have poor stability in severe environments such as low temperature and high temperature, and the active ingredients can be precipitated out along with the lapse of time, so that people continuously pursue an anhydrous essence product which has better moisturizing and relieving effects, is more convenient to use and more remarkable in effect, can adapt to various complex environments and is stable in existence along with the gradual deterioration of natural environments.
Meanwhile, as the cosmetic market products are various in types, the updating iteration speed is high, and the differentiation innovation becomes more important, the brand loyalty of users can be effectively improved by developing the cosmetics with brand-new formulations, the eyeballs of the consumers are attracted, and the purchasing power of the consumers on the products is improved. The existing moisturizing essence is generally in a liquid state, has a short shelf life and is inconvenient to carry, and some moisturizing essence powders such as freeze-dried powder-containing products are also available, but the powders are too light when the products are opened, are easy to hang on the wall of a cosmetic bottle and are mostly stored in a binary chamber, and a matched special moisture-proof packaging design is needed, usually the whole bottle is added for use, and active substances have a short shelf life and are used up in a limited time; at present, freeze-dried silk balls or collagen balls are also used as moisturizing essence in the market, but the moisturizing essence needs to be packaged by independent glass ampoules, is not easy to open and has higher cost.
Disclosure of Invention
The anhydrous essence composition is rich in active ingredients, can exert better skin moisturizing and soothing effects, and is convenient to use and high in stability.
The invention provides an anhydrous essence composition which is characterized by comprising the following components: 75-95 parts of solvent, 10-20 parts of humectant, 2-5 parts of emollient, 5-10 parts of compound emulsifier, 0.1-10 parts of skin protectant, 0.1-1 part of pH regulator, 0.1-3 parts of thickener and 0.1-2 parts of preservative by weight.
Further, the solvent is one or more of aloe vera leaf water, a secondary fission yeast fermentation product filtrate, a lactobacillus/soybean fermentation product extract and a lactobacillus fermentation product.
Further, the humectant is one or more of glycerin, butylene glycol, panthenol, sodium hyaluronate, trehalose, betaine, allantoin, hydrogenated lecithin, ceramide NP, ceramide NS/ceramide NG, ceramide AS, ceramide EOP, and ceramide AP.
Further, the emollient is one or more of shea butter, ethylhexyl palmitate, polydimethylsiloxane and polyglycerol-6; the skin protectant is one or more of Scutellaria alpina flower/leaf/stem extract, centella asiatica extract, hibiscus alpina flower/leaf extract, and Selaginella tamariscina extract.
Further, the compound emulsifier is obtained by mixing cetearyl alcohol and disodium cetearyl sulfosuccinate according to a mass ratio of 3; the thickening agent is acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer.
Furthermore, the mass ratio of the composite emulsifier to the thickener is (3-50) to 1.
Further, the pH regulator is one or more of potassium hydroxide, sodium hydroxide, TEA, citric acid, lactobionic acid and arginine.
Further, the preservative is one or more of phenoxyethanol, methyl hydroxybenzoate, ethylparaben, propylparaben, butylparaben and p-hydroxyacetophenone.
The invention also provides a preparation method of the anhydrous essence composition, which is characterized by comprising the following steps of:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier into a reaction kettle, heating to 73-83 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
The invention also provides an application of the anhydrous essence composition in preparation of an anhydrous essence composition aerosol.
The anhydrous essence composition is prepared by using aloe vera leaf water, the secondary cracking yeast fermentation product filtrate, the lactobacillus/soybean fermentation product extract and the lactobacillus fermentation product as the solvent instead of water, the content of active ingredients is rich, the active ingredients can replace water as the solvent, and the active ingredients have the functions of moisturizing and relieving, so that the moisturizing and relieving effects are further enhanced.
The invention contains active ingredients such as a humectant, an emollient, a skin protective agent and the like, the problem of unstable emulsion system easily exists when the active ingredients are complex, and the phenomenon of non-uniformity occurs. Because the nonionic emulsifier and the anionic emulsifier are mixed according to the mass ratio of 3 to 7 under a certain total amount of the composite emulsifier, the increase of the amount of the anionic emulsifier is beneficial to improving the storage stability of the emulsion, and because a stable anionic charge protective layer is formed on the surface of the emulsion, particles repel each other, and the thermal and mechanical stability is improved; meanwhile, the using amount of the composite emulsifier is controlled to be 5-10%, and then a thickener acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer is added, because the using amount of the composite emulsifier has great influence on the stability and thickening capability of the emulsion, the number of micelles formed in the system is increased along with the increase of the using amount of the composite emulsifier, the initiation and reaction speed is accelerated, the conversion rate of monomers is increased, the stability in the polymerization process is improved, the particle size is reduced, the interaction force among particles is increased, the resistance of particle flow is also increased, the viscosity of the system is also increased, when the using amount of the composite emulsifier is too high, the formed particle size is too small, the surface energy is too large, the agglomeration tendency among emulsion particles is increased, the reaction becomes unstable, the phenomenon of sudden aggregation is easy to occur, and the stability of the emulsion is reduced; the inventor proves that the amount of the composite emulsifier is controlled to be 5-10% best, the mass ratio of the composite emulsifier to the thickening agent is controlled to be (3-50): 1, and various active substances in the system can be ensured to exist stably, so that the moisturizing and relieving effects are improved.
Compared with the prior art, the invention has the beneficial effects that:
1. the anhydrous essence composition provided by the invention has rich active ingredients, and through reasonable compatibility, the components can generate synergistic interaction, so that the prepared anhydrous essence composition has good moisturizing and relieving effects, and does not generate stimulation to skin;
2. the anhydrous essence composition disclosed by the invention is rich in active ingredients, a nonionic emulsifier cetearyl stearyl alcohol and an anionic emulsifier cetearyl disodium sulfosuccinate are mixed according to a certain proportion to serve as a composite emulsifier, an acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer is added to serve as a thickening agent, the mass ratio of the composite emulsifier to the thickening agent is controlled to be (3-50): 1, the system stability and thickening capacity can be promoted, and precipitation is not easy to occur;
3. the solvent of the anhydrous essence composition prepared by the invention is one or more of aloe vera leaf water with a moisturizing effect, secondary cracking yeast fermentation product filtrate, lactobacillus/soybean fermentation product extract and lactobacillus fermentation product, so that the effects of moisturizing and relieving repair are increased.
Detailed Description
The technical solutions of the present invention will be described in detail and fully with reference to the following embodiments, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without inventive step based on the embodiments of the present invention, are within the scope of protection of the present invention.
The reagents used in the invention are all common reagents and can be purchased from conventional reagent production and sale companies.
Example 1 Anhydrous serum composition of the invention and preparation thereof
The formula is as follows: 90kg of solvent, 10kg of humectant, 5kg of emollient, 8.5kg of compound emulsifier, 5kg of skin protectant, 0.3kg of pH regulator, 0.7kg of thickening agent and 0.5kg of preservative;
the skin care product comprises 90kg of aloe vera leaf water as a solvent, 5kg of glycerin and 5kg of allantoin as moisturizers, 2kg of ethylhexyl palmitate, 1.5kg of polydimethylsiloxane and 1.5kg of shea butter, 2.55kg of cetostearyl alcohol and 5.95g of disodium cetostearyl sulfosuccinate as composite emulsifiers, 3kg of scutellaria alpina flower/leaf/stem extract, 1kg of leontopodium alpinum flower/leaf extract and 1kg of centella asiatica extract as skin protectants, 0.3kg of potassium hydroxide as a pH regulator, 0.7kg of acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer as a thickening agent and 0.5kg of phenoxyethanol as a preservative;
the preparation process comprises the following steps:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier into a reaction kettle, heating to 73 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
Example 2 Anhydrous serum composition of the invention and preparation thereof
The formula is as follows: 85kg of solvent, 20kg of humectant, 2.2kg of emollient, 6kg of compound emulsifier, 4kg of skin protectant, 0.6kg of pH regulator, 1.3kg of thickening agent and 0.9kg of preservative;
the solvent is 85kg of aloe vera leaf water, the moisturizer is 5kg of trehalose, 5kg of glycerol and 10kg of allantoin, the emollient is 1kg of ethylhexyl palmitate, 1kg of polydimethylsiloxane and 0.2kg of shea butter, and the composite emulsifier is obtained by mixing 1.8kg of cetearyl alcohol and 4.2kg of disodium cetearyl sulfosuccinate; the skin protective agent is 2kg of a Hibiscus manihot flower/leaf extract and 2kg of a centella asiatica extract, the pH regulator is 0.6kg of arginine, the thickening agent is 1.3kg of acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer, and the preservative is 0.9kg of methylparaben;
the preparation process comprises the following steps:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier into a reaction kettle, heating to 75 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
Example 3 Anhydrous essence composition of the invention and preparation thereof
The formula is as follows: 95kg of solvent, 17kg of humectant, 2kg of emollient, 5kg of compound emulsifier, 0.1kg of skin protectant, 0.7kg of pH regulator, 0.1kg of thickening agent and 0.1kg of preservative;
the solvent is 95kg of aloe vera leaf water, and the emollient is 5kg of ethylhexyl palmitate, 5kg of polydimethylsiloxane and 7kg of shea butter; the skin protective agent is 0.1kg of alpine leontopodium herb flower/leaf extract, the pH regulator is 0.7kg of potassium hydroxide, the thickening agent is 0.1kg of acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer, and the preservative agent is 0.1kg of methylparaben;
the preparation process comprises the following steps:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier into a reaction kettle, heating to 77 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
Example 4 Anhydrous serum composition of the invention and preparation thereof
The formula is as follows: 82.4kg of solvent, 12kg of humectant, 5kg of emollient, 7kg of compound emulsifier, 10kg of skin protectant, 0.1kg of pH regulator, 2kg of thickener and 1.5kg of preservative;
the skin care product is characterized in that the solvent is 82.4kg of aloe vera leaf water, the moisturizer is 4kg of sodium hyaluronate, 6kg of glycerol and 2kg of allantoin, the emollients are 2kg of ethylhexyl palmitate, 1kg of polydimethylsiloxane and 2kg of shea butter, the composite emulsifier is obtained by mixing 2.1kg of cetostearyl alcohol and 4.9kg of disodium cetostearyl sulfosuccinate, the skin protective agent is 10kg of a leontopodium japonicum flower/leaf extract, the pH regulator is 0.1kg of potassium hydroxide, the thickener is 2kg of an acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer, and the preservative is 1.5kg of phenoxyethanol;
the preparation process comprises the following steps:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier into a reaction kettle, heating to 79 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
Example 5 Anhydrous serum composition of the invention and preparation thereof
The formula is as follows: 75kg of solvent, 19kg of humectant, 4kg of emollient, 10kg of compound emulsifier, 6kg of skin protectant, 1kg of pH regulator, 3kg of thickener and 2kg of preservative;
the skin care product comprises a solvent, a humectant, a skin protecting agent and a thickening agent, wherein the solvent comprises 70kg of aloe vera leaf water and 5kg of a schizosaccharomyces fermentation product filtrate, the humectant comprises 5kg of glycerol, 5kg of trehalose, 5kg of allantoin, 1kg of hydrogenated lecithin and 3kg of panthenol, the emollient is 1kg of ethylhexyl palmitate, 1kg of polydimethylsiloxane, 1kg of shea butter, 0.5kg of polyglycerol-6 and 0.5kg of polydimethylsiloxane, the composite emulsifier is obtained by mixing 3kg of cetostearyl alcohol and 7kg of disodium cetostearyl sulfosuccinate, the skin protecting agent comprises 3kg of a flower/leaf extract of Hibiscus ferox and 3kg of a selaginella tamariscina extract, the pH adjusting agent is 1kg of sodium hydroxide, the thickening agent is 3kg of an acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer, and the preservative is 2kg of phenoxyethanol;
the preparation process comprises the following steps:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier into a reaction kettle, heating to 83 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
Comparative example 1
The comparative example is different from the example 1 in that the weight of the composite emulsifier is unchanged, but the composite emulsifier is obtained by mixing cetearyl alcohol and disodium cetearyl sulfosuccinate according to the mass ratio of 4.
Comparative example 2
The comparative example is different from example 1 in that the weight sum of the composite emulsifier and the thickener is unchanged, but the weight part of the composite emulsifier is only 4 percent, namely 4.8kg of the composite emulsifier and 4.4kg of the thickener, and the rest materials, parameters, steps and the like are completely the same.
Comparative example 3
The comparative example is different from example 1 in that the weight sum of the composite emulsifier and the thickening agent is unchanged, but the mass ratio of the composite emulsifier to the thickening agent is 1.
Test example one, moisture retention effect test of anhydrous essence composition
(1) Test samples: anhydrous essence compositions prepared in examples 1 to 5 and comparative examples 1 to 3;
(2) Test subjects: 80 female volunteers between 25 and 35 years of age were selected and randomly divided into 8 groups of 10 persons each, and volunteers required: the skin is healthy, has no history of skin diseases, and has almost the same moisture content;
(3) The test method comprises the following steps: in an indoor environment at 25 ℃ and with a relative humidity of 50%, testing samples are used on the whole face of a volunteer every day, other cosmetics are not used, the skin moisture content is tested on the 0 th day, the 14 th day and the 28 th day respectively by a skin moisture detector, and the average value measured by 10 volunteers is taken as a final result;
(4) The results of the tests are given in the following table:
TABLE 1 moisturizing effect test of essence compositions
As can be seen from the data in Table 1, the anhydrous essence compositions prepared in the examples 1 to 5 have good skin moisture content after 28 days after acting on the cheek skin, and have a remarkable moisturizing effect, wherein the moisture content is as high as 38.86%; wherein, the moisturizing effect of the embodiment 1 is the best, and is the best embodiment of the invention; the essence compositions prepared in comparative examples 1 to 3, however, did not have high skin moisture content and did not have good moisturizing effect after being applied to cheek skin for 28 days.
Test example two, examination of soothing effect of essence composition
(1) Test samples: anhydrous essence compositions prepared in examples 1 to 5 and comparative examples 1 to 3;
(2) The test method comprises the following steps:
selecting 80 sensitive skin women with the water dispersion value of more than or equal to 10, wherein the women are aged 25-45 years, randomly dividing the women into 8 groups, smearing the anhydrous essence compositions prepared in the examples 1-5 and the comparative examples 1-3 on each group of 10 people in the morning, after using the anhydrous essence compositions for 4 hours, carrying out the evaluation record of the relieving effect on the sample, and recording the number of people with good, common and no effect on the relieving effect;
(3) And (3) test results:
TABLE 2, results of examining the soothing effect of the essence compositions
| Item | Good effect (human) | Effect in general (human) | No effect (human) |
| Example 1 | 9 | 1 | 0 |
| Example 2 | 8 | 1 | 1 |
| Example 3 | 8 | 1 | 1 |
| Example 4 | 7 | 2 | 1 |
| Example 5 | 8 | 1 | 1 |
| Comparative example 1 | 2 | 2 | 6 |
| Comparative example 2 | 3 | 2 | 5 |
| Comparative example 3 | 2 | 3 | 5 |
As can be seen from table 2, the anhydrous essence compositions prepared in examples 1 to 5 of the present invention have better soothing effect, wherein the soothing effect of example 1 is the best example of the present invention; the soothing effect of the essence compositions prepared in comparative examples 1 to 3 was poor.
Test example three, stability test of anhydrous essence composition
(1) Test samples: the essence compositions prepared in examples 1 to 5 and comparative examples 1 to 3 were each 1kg
(2) The test method comprises the following steps: the sample is placed in an environment of 42 ℃ to-12 ℃, and is recovered to the room temperature after being kept for 24 hours, and whether the phenomena of turbidity, layering and discoloration appear or not is observed.
(3) And (3) test results:
table 3, stability test results of essence compositions
As can be seen from the data in Table 3, the anhydrous essence compositions prepared in the embodiments 1-5 of the invention have no phenomena of turbidity, layered discoloration after being subjected to the environment of 42 ℃ and 12 ℃ for 24 hours, and have good stability; in the essence compositions prepared in comparative examples 1 to 3, the ratio of the non-ionic emulsifier cetearyl stearyl alcohol to the anionic emulsifier cetearyl disodium sulfosuccinate in the composite emulsifier is changed or the amount of the composite emulsifier is changed, so that the stability of the active substances in the anhydrous essence composition is deteriorated, and the anhydrous essence composition is easily turbid and discolored by layering after a period of time in a high-temperature and low-temperature environment.
Test example four, examination of Using Performance of Anhydrous essence composition Aerosol
(1) Test samples: the anhydrous essence compositions prepared in examples 1-5 and comparative examples 1-3 were prepared into anhydrous essence composition aerosol
(2) The test method comprises the following steps: 80 female subjects with skin health aged 20-40 years are selected, randomly divided into 8 groups, 10 persons are in each group, the anhydrous essence composition aerosol prepared in the examples 1-5 and the comparative examples 1-3 is respectively used for each group of subjects, the anhydrous essence composition aerosol is uniformly sprayed on the whole face twice a day in the morning and evening and is continuously used for 7 days, and various performances of the anhydrous essence composition are tested;
(3) And (3) test results:
TABLE 4 Performance testing
| Group of | Sense of smearing | Skin feel after use |
| Example 1 | Fine and smooth, and easy to be coated | Good moisture retention, no stickiness |
| Example 2 | Fine and smooth, and easy to be spread | Good moisture retention, no stickiness |
| Example 3 | Fine and smooth, and easy to be coated | Good moisture retention, no stickiness |
| Example 4 | Fine and smooth, and easy to be coated | Good moisture retention, no stickiness |
| Example 5 | Fine and smooth, and easy to be spread | Good moisture retention and no greasy |
| Comparative example 1 | Sticky and not easy to be smeared | Moderate moisture retention and stickiness |
| Comparative example 2 | Sticky and not easy to be smeared | Moistening middle energizer and sticky |
| Comparative example 3 | Sticky and not easy to be smeared | Moistening middle energizer and sticky |
As can be seen from table 4, when the anhydrous essence compositions prepared in examples 1 to 5 are prepared into an aerosol for use, the sprayed contents are finer and smoother, are easy to spread, do not stick to greasy, have a good moisturizing effect, and have a better skin use feeling; the anhydrous essence compositions prepared in comparative examples 1 to 3 are used as aerosol, and the sprayed contents are sticky, not easy to spread, sticky, moderate in moisturizing effect and not strong enough in skin use feeling.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is specific and detailed, but not to be construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present invention should be subject to the appended claims.
Claims (10)
1. An anhydrous essence composition is characterized by comprising the following components: 75-95 parts of solvent, 10-20 parts of humectant, 2-5 parts of emollient, 5-10 parts of compound emulsifier, 0.1-10 parts of skin protectant, 0.1-1 part of pH regulator, 0.1-3 parts of thickener and 0.1-2 parts of preservative by weight.
2. The anhydrous essence composition according to claim 1, wherein the solvent is one or more of aloe vera leaf water, a secondary fission yeast fermentation product filtrate, a lactobacillus/soybean fermentation product extract and a lactobacillus fermentation product.
3. The anhydrous essence composition according to claim 1, wherein the moisturizer is one or more of glycerin, butylene glycol, panthenol, sodium hyaluronate, trehalose, betaine, allantoin, hydrogenated lecithin, ceramide NP, ceramide NS/ceramide NG, ceramide AS, ceramide EOP, and ceramide AP.
4. The anhydrous essence composition according to claim 1, wherein the emollient is one or more of shea butter, ethylhexyl palmitate, polydimethylsiloxane and polyglycerol-6; the skin protectant is one or more of Scutellaria alpina flower/leaf/stem extract, centella asiatica extract, leontopodium alpinum flower/leaf extract, and Selaginella tamariscina extract.
5. The anhydrous essence composition according to claim 1, wherein the compound emulsifier is prepared by mixing cetearyl alcohol and disodium cetearyl sulfosuccinate according to a mass ratio of 3; the thickening agent is acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer.
6. The anhydrous essence composition according to claim 1, wherein the mass ratio of the composite emulsifier to the thickener is (3-50): 1.
7. The anhydrous essence composition according to claim 1, wherein the pH regulator is one or more of potassium hydroxide, sodium hydroxide, TEA, citric acid, lactobionic acid and arginine.
8. The anhydrous essence composition according to claim 1, wherein the preservative is one or more of phenoxyethanol, methylparaben, ethylparaben, propylparaben, butylparaben and p-hydroxyacetophenone.
9. A method for preparing the anhydrous essence composition according to any one of claims 1 to 8, comprising the steps of:
s1, respectively putting a moisturizing agent, a skin protective agent, a thickening agent and a part of solvent into a container, and uniformly stirring to obtain a mixed solution;
s2, putting the residual solvent, the emollient and the composite emulsifier in a reaction kettle, heating to 73-83 ℃, homogenizing and stirring until the residual solvent, the emollient and the composite emulsifier are completely dissolved, and cooling;
and S3, when the temperature of the reaction kettle is reduced to 45 ℃, adding the preservative and the mixed solution obtained in the step S1, stirring uniformly, then adding the pH regulator, and shaking uniformly to obtain the anhydrous essence composition.
10. Use of anhydrous essence composition according to any one of claims 1-9 for preparing anhydrous essence composition aerosol.
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| CN115844805A (en) * | 2022-12-14 | 2023-03-28 | 广东馨柯生命科学有限公司 | Whitening essence with tyrosinase activity inhibited by secondary fermentation micromolecule hyaluronic acid Supferm HA and preparation method thereof |
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| CN112933034A (en) * | 2021-03-04 | 2021-06-11 | 广州市珍榜日用化工有限公司 | Eye repair and nursing composition capable of removing dark circles, essence emulsion and preparation method |
| CN114099375A (en) * | 2021-10-16 | 2022-03-01 | 广州市尊爱日用化妆品有限公司 | Soothing and repairing essence containing yeast bifida fermentation product and preparation method thereof |
| CN114533643A (en) * | 2022-01-21 | 2022-05-27 | 广州卡洛莱化妆品有限公司 | Moisture-preserving essence color bead isolation product |
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| CN110101651A (en) * | 2019-05-31 | 2019-08-09 | 广东盛美化妆品有限公司 | Yeast tunning lysis object is split containing two releive repair Essence and preparation method thereof |
| CN112933034A (en) * | 2021-03-04 | 2021-06-11 | 广州市珍榜日用化工有限公司 | Eye repair and nursing composition capable of removing dark circles, essence emulsion and preparation method |
| CN114099375A (en) * | 2021-10-16 | 2022-03-01 | 广州市尊爱日用化妆品有限公司 | Soothing and repairing essence containing yeast bifida fermentation product and preparation method thereof |
| CN114533643A (en) * | 2022-01-21 | 2022-05-27 | 广州卡洛莱化妆品有限公司 | Moisture-preserving essence color bead isolation product |
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| CN115844805A (en) * | 2022-12-14 | 2023-03-28 | 广东馨柯生命科学有限公司 | Whitening essence with tyrosinase activity inhibited by secondary fermentation micromolecule hyaluronic acid Supferm HA and preparation method thereof |
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