CN115176957A - Preparation method of efficient liquid mildew inhibitor capable of prolonging storage life of feed - Google Patents
Preparation method of efficient liquid mildew inhibitor capable of prolonging storage life of feed Download PDFInfo
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- CN115176957A CN115176957A CN202210832673.8A CN202210832673A CN115176957A CN 115176957 A CN115176957 A CN 115176957A CN 202210832673 A CN202210832673 A CN 202210832673A CN 115176957 A CN115176957 A CN 115176957A
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- 239000007788 liquid Substances 0.000 title claims abstract description 48
- 238000003860 storage Methods 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000003112 inhibitor Substances 0.000 title claims description 15
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 63
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims abstract description 42
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000000284 extract Substances 0.000 claims abstract description 41
- 239000011259 mixed solution Substances 0.000 claims abstract description 41
- 241000411851 herbal medicine Species 0.000 claims abstract description 40
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims abstract description 34
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 25
- 238000002156 mixing Methods 0.000 claims abstract description 25
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims abstract description 22
- 230000003449 preventive effect Effects 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000001530 fumaric acid Substances 0.000 claims abstract description 21
- 235000019260 propionic acid Nutrition 0.000 claims abstract description 21
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims abstract description 21
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims abstract description 21
- 241000205585 Aquilegia canadensis Species 0.000 claims abstract description 18
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 18
- 240000006688 Telosma cordata Species 0.000 claims abstract description 18
- 235000017352 Telosma cordata Nutrition 0.000 claims abstract description 18
- 244000112814 pipewort Species 0.000 claims abstract description 18
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims abstract description 17
- 235000019253 formic acid Nutrition 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 17
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 241001529821 Agastache Species 0.000 claims abstract description 4
- 241001162994 Rugosus Species 0.000 claims abstract description 4
- 244000223014 Syzygium aromaticum Species 0.000 claims description 17
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- 238000006243 chemical reaction Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- -1 alkylbenzene sulfonate Chemical class 0.000 claims description 10
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 9
- 238000007873 sieving Methods 0.000 claims description 5
- 150000003863 ammonium salts Chemical class 0.000 claims description 4
- 230000000855 fungicidal effect Effects 0.000 claims description 4
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- 229910052783 alkali metal Inorganic materials 0.000 claims description 3
- 229920000136 polysorbate Polymers 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 2
- 240000002948 Ophiopogon intermedius Species 0.000 claims 2
- 244000248557 Ophiopogon japonicus Species 0.000 abstract description 16
- 230000000694 effects Effects 0.000 abstract description 16
- 239000003795 chemical substances by application Substances 0.000 abstract description 8
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
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- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
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- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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Abstract
The invention relates to the technical field of feed liquid mildew preventive, and discloses a preparation method of a high-efficiency liquid mildew preventive capable of prolonging the storage life of feed, which comprises the following steps: s1: preparing raw materials, 10-20 parts of formic acid, 15-18 parts of propionic acid, 5-10 parts of propionate, 5-6 parts of citric acid, 6-8 parts of fumaric acid, 11-15 parts of Chinese herbal medicine extract, 10-16 parts of emulsifier and a plurality of parts of water; s2: stirring and mixing, namely heating and mixing formic acid, propionic acid, propionate, citric acid and fumaric acid to obtain a mixed solution A; s3: adding Chinese herbal medicine extract. According to the invention, the anti-mildew effect of the feed is improved by adding the Chinese herbal medicine extract which takes the clove, the Chinese violet, the agastache rugosus, the ophiopogon root, the pipewort and the honeysuckle stem as raw materials into the liquid anti-mildew agent, so that the purpose of prolonging the storage life of the feed is achieved, the anti-mildew agent can also sterilize and disinfect, enhance the resistance of animals, promote metabolism and digestion, and the like, is beneficial to the growth of the animals, and has good palatability.
Description
Technical Field
The invention relates to the technical field of liquid feed mildew inhibitors, in particular to a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of feed.
Background
The rapid development of the feed industry in China leads feed products to be commonly used in the breeding industry, and plays an important role in saving the feeding cost, improving the production (growth) performance of livestock and poultry and increasing the economic benefit of breeding. However, the feed is very vulnerable to mold contamination and mildew during storage, transportation, sale and use.
In the prior art, feed is generally mildewed by a liquid mildewproof agent, but the existing liquid mildewproof agent in the market has poor mildewproof effect, shortens the storage life of the feed, and cannot meet the requirements of people, so that the preparation method of the high-efficiency liquid mildewproof agent capable of prolonging the storage life of the feed is provided.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of a feed, and mainly solves the problems that the existing liquid mildew inhibitor in the current market has poor mildew-proof effect, shortens the storage life of the feed and cannot meet the requirements of people.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of feed comprises the following steps:
s1: preparing raw materials, 10-20 parts of formic acid, 15-18 parts of propionic acid, 5-10 parts of propionate, 5-6 parts of citric acid, 6-8 parts of fumaric acid, 11-15 parts of Chinese herbal medicine extract, 10-16 parts of emulsifier and a plurality of parts of water;
s2: stirring and mixing, namely heating and mixing formic acid, propionic acid, propionate, citric acid and fumaric acid to obtain a mixed solution A;
s3: adding Chinese herbal medicine extract, adding the Chinese herbal medicine extract into the mixed solution A, and then heating and mixing to obtain mixed solution B;
s4: adding an emulsifier, adding the emulsifier and water into the mixed solution B, and then stirring and mixing to obtain a liquid mildew preventive;
s5: and (4) metering and packaging, namely metering and packaging the liquid mildew preventive to obtain a finished product.
On the basis of the scheme, the Chinese herbal medicine extract raw materials in the S1 are clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem.
As a still further scheme of the present invention, the preparation method of the herbal extract in S1 comprises: firstly, clove, chinese violet, agastache rugosus, dwarf lilyturf tuber, pipewort and honeysuckle stem are crushed, after the crushing is finished, a sieve with 50-80 meshes is selected for sieving, the screened particles are crushed again until the particles are completely powdery to obtain crushed materials, then the crushed materials and water are heated and boiled for 30-40min according to the ratio of 1.
Further, the emulsifier in S1 is one or more of alkylphenol polyoxyethylene, tween and alkylbenzene sulfonate.
On the basis of the scheme, the propionate in the S1 is any one or more of ammonium salt or alkali metal salt.
In the step S2, firstly, 15-18 parts of propionic acid is added into a reaction kettle, the mixture is heated by a steam jacket for 25-35min and stirred at 50-60 r/min, and then 10-20 parts of formic acid, 5-10 parts of propionate, 5-6 parts of citric acid and 6-8 parts of fumaric acid are added into the reaction kettle for reaction for 20-30min, so that mixed solution A is obtained.
Further, in the step S3, the Chinese herbal medicine extract prepared in the step S1 is added into the mixed solution A for three times, the temperature is controlled to be 50-60 ℃, and the mixture is stirred and mixed at the speed of 20-35 r/min to obtain a mixed solution B.
On the basis of the scheme, in the step S4, an emulsifying machine and water are added into the mixed liquid B, and stirring and mixing are carried out at the speed of 30-40 r/min, so that the liquid mildew preventive is obtained.
(III) advantageous effects
Compared with the prior art, the invention provides the preparation method of the high-efficiency liquid mildew preventive capable of prolonging the storage life of the feed, and the preparation method has the following beneficial effects:
1. according to the invention, the anti-mildew effect of the feed is improved by adding the Chinese herbal medicine extract which takes the clove, the Chinese violet, the agastache rugosus, the ophiopogon root, the pipewort and the honeysuckle stem as raw materials into the liquid anti-mildew agent, so that the purpose of prolonging the storage life of the feed is achieved, the anti-mildew agent can also sterilize and disinfect, enhance the resistance of animals, promote metabolism and digestion, and the like, is beneficial to the growth of the animals, and has good palatability.
2. According to the invention, propionic acid, citric acid and fumaric acid are free acids, so that high osmotic pressure can be caused outside the cell wall of the mould to dehydrate the inside of the mould cell, thus the mould-proof effect is achieved, the pH in the mould cell can be disturbed, nutrition is prevented from being transported into the cell, the cell metabolic reaction is prevented, the asexual propagation of the mould is inhibited, and the mould-proof effect is improved.
3. According to the invention, one or more of alkylphenol polyoxyethylene, tween and alkylbenzene sulfonate are selected as the emulsifier, so that the using effect of the liquid mildew inhibitor can be improved, and the mildew-proof effect of the liquid mildew inhibitor can be further improved.
4. According to the invention, the raw materials of the Chinese herbal medicine extract are fully crushed, then water and the crushed materials are decocted, then ethanol is added for microwave treatment, and the filter residue is repeatedly decocted, so that the purity of the Chinese herbal medicine extract is improved, and the mildew-proof effect is improved.
Drawings
FIG. 1 is a schematic flow structure diagram of a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the shelf life of feed according to the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Example 1
Referring to fig. 1, a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of a feed comprises the following steps:
s1: preparing raw materials including 10 parts of formic acid, 15 parts of propionic acid, 5 parts of propionate, 5 parts of citric acid, 6 parts of fumaric acid, 11 parts of Chinese herbal medicine extract, 10 parts of emulsifier and a plurality of parts of water, wherein the propionic acid, the citric acid and the fumaric acid are free acids, and can cause high osmotic pressure outside mould cell walls to dehydrate mould cells, so that a mould-proof effect is achieved;
s2: stirring and mixing, namely heating and mixing formic acid, propionic acid, propionate, citric acid and fumaric acid to obtain a mixed solution A;
s3: adding Chinese herbal medicine extract, adding the Chinese herbal medicine extract into the mixed solution A, and then heating and mixing to obtain mixed solution B;
s4: adding an emulsifier, adding the emulsifier and water into the mixed solution B, and then stirring and mixing to obtain a liquid mildew preventive;
s5: and (4) metering and packaging, namely metering and packaging the liquid mildew preventive to obtain a finished product.
Particularly, the Chinese herbal medicine extract raw materials in the S1 are clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem, the arrangement of adding the Chinese herbal medicine extract which takes the clove, the Chinese violet, the wrinkled gianthyssop herb, the dwarf lilyturf tuber, the pipewort and the honeysuckle stem as the raw materials into the liquid mildew preventive improves the mildew-proof effect of the feed, thereby achieving the purpose of prolonging the storage life of the feed, and the preparation method of the Chinese herbal medicine extract in the S1 comprises the following steps: firstly, clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem are crushed, after crushing, a sieve with 50 meshes is selected for sieving, the screened particles are crushed again, so that clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem are sufficiently crushed for subsequent extraction until all are in powder form, crushed particles are obtained, then, the crushed particles and water are heated and boiled for 30min according to the ratio of 1.
It is to be noted that the emulsifier in S1 is alkylphenol ethoxylates, the propionate in S1 is an ammonium salt, in S2, firstly, 15 parts of propionic acid are added into a reaction kettle, heated for 25min with a steam jacket, and stirred at 50 rpm, then, 10 parts of formic acid, 5 parts of propionate, 5 parts of citric acid, and 6 parts of fumaric acid are added into the reaction kettle to react for 20min, so as to obtain a mixed solution a, in S3, the Chinese herbal medicine extract prepared in S1 is added into the mixed solution a three times, so that the Chinese herbal medicine extract is fully mixed with the mixed solution a, the temperature is controlled at 50 ℃, and the mixture is stirred and mixed at 20 rpm, so as to obtain a mixed solution B, and in S4, the emulsifier and water are added into the mixed solution B, and stirred and mixed at 30 rpm, so as to obtain the liquid mildewproof agent.
Example 2
Referring to fig. 1, a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of feed comprises the following steps:
s1: preparing raw materials, namely 20 parts of formic acid, 18 parts of propionic acid, 10 parts of propionate, 6 parts of citric acid, 6-8 parts of fumaric acid, 15 parts of Chinese herbal medicine extract, 16 parts of emulsifier and a plurality of parts of water, wherein the propionic acid, the citric acid and the fumaric acid are free acids, so that high osmotic pressure can be caused outside the mould cell wall, and the mould cell is dehydrated, so that the mould-proof effect is achieved;
s2: stirring and mixing, namely heating and mixing formic acid, propionic acid, propionate, citric acid and fumaric acid to obtain a mixed solution A;
s3: adding Chinese herbal medicine extract, adding the Chinese herbal medicine extract into the mixed solution A, and then heating and mixing to obtain mixed solution B;
s4: adding an emulsifier, adding the emulsifier and water into the mixed solution B, and then stirring and mixing to obtain a liquid mildew preventive;
s5: and (4) metering and packaging, namely metering and packaging the liquid mildew preventive to obtain a finished product.
Particularly, the Chinese herbal medicine extract raw materials in the S1 are clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem, the arrangement of adding the Chinese herbal medicine extract which takes the clove, the Chinese violet, the wrinkled gianthyssop herb, the dwarf lilyturf tuber, the pipewort and the honeysuckle stem as the raw materials into the liquid mildew preventive improves the mildew-proof effect of the feed, thereby achieving the purpose of prolonging the storage life of the feed, and the preparation method of the Chinese herbal medicine extract in the S1 comprises the following steps: firstly, clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem are crushed, after crushing, a sieve with 50-80 meshes is selected for sieving, the screened particles are crushed again, so that the clove, the Chinese violet, the wrinkled gianthyssop herb, the dwarf lilyturf tuber, the pipewort and the honeysuckle stem are fully crushed for subsequent extraction until all are powdered, crushed material is obtained, then, the crushed material and water are heated and boiled for 40min according to the ratio of 1.
It is noted that the emulsifier in S1 is alkylbenzene sulfonate, the propionate in S1 is alkali metal salt, in S2, first, 18 parts of propionic acid are added into a reaction kettle, heated by a steam jacket for 35min, and stirred at 60 rpm, then, 20 parts of formic acid, 10 parts of propionate, 6 parts of citric acid, and 8 parts of fumaric acid are added into the reaction kettle to react for 30min, so as to obtain a mixed solution a, in S3, the Chinese herbal medicine extract prepared in S1 is added into the mixed solution a three times, so as to sufficiently mix the Chinese herbal medicine extract with the mixed solution a, and the temperature is controlled at 60 ℃, and the mixed solution B is obtained by stirring and mixing at 35 rpm, in S4, an emulsifier and water are added into the mixed solution B, and stirring and mixing are performed at 40 rpm, so as to obtain the liquid fungicide.
Example 3
Referring to fig. 1, a preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of a feed comprises the following steps:
s1: preparing raw materials including 15 parts of formic acid, 17 parts of propionic acid, 8 parts of propionate, 5 parts of citric acid, 7 parts of fumaric acid, 13 parts of Chinese herbal medicine extract, 15 parts of emulsifier and a plurality of parts of water, wherein the propionic acid, the citric acid and the fumaric acid are free acids, so that high osmotic pressure can be caused outside the mould cell wall, and the mould cell is dehydrated, so that the mould proof effect is achieved;
s2: stirring and mixing, namely heating and mixing formic acid, propionic acid, propionate, citric acid and fumaric acid to obtain a mixed solution A;
s3: adding Chinese herbal medicine extract, adding the Chinese herbal medicine extract into the mixed solution A, and then heating and mixing to obtain mixed solution B;
s4: adding an emulsifier, adding the emulsifier and water into the mixed solution B, and then stirring and mixing to obtain a liquid mildew preventive;
s5: and (4) metering and packaging, namely metering and packaging the liquid mildew preventive to obtain a finished product.
Particularly, the Chinese herbal medicine extract raw materials in the S1 are clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem, the arrangement of adding the Chinese herbal medicine extract which takes the clove, the Chinese violet, the wrinkled gianthyssop herb, the dwarf lilyturf tuber, the pipewort and the honeysuckle stem as the raw materials into the liquid mildew preventive improves the mildew-proof effect of the feed, thereby achieving the purpose of prolonging the storage life of the feed, and the preparation method of the Chinese herbal medicine extract in the S1 comprises the following steps: firstly, clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem are crushed, after crushing, a sieve with 50-80 meshes is selected for sieving, the screened particles are crushed again, so that the clove, the Chinese violet, the wrinkled gianthyssop herb, the dwarf lilyturf tuber, the pipewort and the honeysuckle stem are fully crushed for subsequent extraction until all are powdered, crushed material is obtained, then, the crushed material and water are heated and boiled for 35min according to the ratio of 1.
It is to be noted that the emulsifier in S1 is alkylbenzene sulfonate, the propionate in S1 is ammonium salt, in S2, firstly, 17 parts of propionic acid are added into a reaction kettle, the mixture is heated by a steam jacket for 26min, and stirred at 57 rpm, then, 15 parts of formic acid, 8 parts of propionate, 5 parts of citric acid and 7 parts of fumaric acid are added into the reaction kettle to react for 22min, so as to obtain a mixed solution a, in S3, the Chinese herbal medicine extract prepared in S1 is added into the mixed solution a three times, so as to fully mix the Chinese herbal medicine extract with the mixed solution a, the temperature is controlled at 57 ℃, and the mixture is stirred and mixed at 27 rpm, so as to obtain a mixed solution B, in S4, the emulsifier and water are added into the mixed solution B, and stirred and mixed at 38 rpm, so as to obtain the liquid fungicide.
In the description herein, it is noted that relational terms such as first and second, and the like, are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. A preparation method of a high-efficiency liquid mildew inhibitor capable of prolonging the storage life of feed is characterized by comprising the following steps:
s1: preparing raw materials, 10-20 parts of formic acid, 15-18 parts of propionic acid, 5-10 parts of propionate, 5-6 parts of citric acid, 6-8 parts of fumaric acid, 11-15 parts of Chinese herbal medicine extract, 10-16 parts of emulsifier and a plurality of parts of water;
s2: stirring and mixing, namely heating and mixing formic acid, propionic acid, propionate, citric acid and fumaric acid to obtain a mixed solution A;
s3: adding Chinese herbal medicine extract, adding the Chinese herbal medicine extract into the mixed solution A, and then heating and mixing to obtain mixed solution B;
s4: adding an emulsifier, adding the emulsifier and water into the mixed solution B, and then stirring and mixing to obtain a liquid mildew preventive;
s5: and (4) metering and packaging, namely metering and packaging the liquid mildew preventive to obtain a finished product.
2. The method for preparing the high-efficiency liquid mildew preventive capable of prolonging the storage life of the feed according to claim 1, wherein the Chinese herbal medicine extract raw materials in S1 are clove, chinese violet, wrinkled gianthyssop herb, dwarf lilyturf tuber, pipewort and honeysuckle stem.
3. The method for preparing the high-efficiency liquid mildew inhibitor capable of prolonging the feed storage life according to claim 2, wherein the Chinese herbal medicine extract in S1 is prepared by the following steps: firstly, clove, chinese violet, agastache rugosus, dwarf lilyturf tuber, pipewort and honeysuckle stem are crushed, after the crushing is finished, a sieve with 50-80 meshes is selected for sieving, the screened particles are crushed again until the particles are completely powdery to obtain crushed materials, then the crushed materials and water are heated and boiled for 30-40min according to the ratio of 1.
4. The method for preparing the high-efficiency liquid mildew preventive capable of prolonging the storage life of feeds according to claim 1, wherein the emulsifier in S1 is one or more of alkylphenol ethoxylates, tween and alkylbenzene sulfonate.
5. The method for preparing the liquid fungicide according to claim 1, wherein the propionate in S1 is one or more of ammonium salt or alkali metal salt.
6. The method for preparing a high-efficiency liquid mildew preventive capable of prolonging the storage life of feed according to claim 5, wherein in S2, 15-18 parts of propionic acid is firstly added into a reaction kettle, the mixture is heated for 25-35min by a steam jacket, and is stirred at 50-60 r/min, and then 10-20 parts of formic acid, 5-10 parts of propionate, 5-6 parts of citric acid and 6-8 parts of fumaric acid are added into the reaction kettle for reaction for 20-30min, so as to obtain a mixed solution A.
7. The method for preparing the liquid fungicide according to claim 6, wherein the herb extract obtained in step S1 is added to the mixture A in step S3 in three times, and the temperature is controlled at 50-60 ℃, and the mixture is stirred and mixed at 20-35 rpm to obtain a mixture B.
8. The method for preparing the high-efficiency liquid mildew preventive capable of prolonging the storage life of the feed according to claim 1, wherein an emulsifying machine and water are added into the mixed solution B in the step S4, and the mixture is stirred and mixed at 30-40 r/min to obtain the liquid mildew preventive.
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040170729A1 (en) * | 2003-02-28 | 2004-09-02 | Jesuadimai Ignatius Xavier Antony | Mold inhibitor having reduced corrosiveness |
| CN105166587A (en) * | 2015-09-07 | 2015-12-23 | 王璐 | Drying mildewproof bactericide for feeds |
| CN107212240A (en) * | 2017-07-19 | 2017-09-29 | 合肥浦邦农业科技有限公司 | A kind of Midew preventive for feed and preparation method thereof |
| CN107259294A (en) * | 2017-06-21 | 2017-10-20 | 宜兴市天石饲料有限公司 | Feedstuff mildew-resistant additive and preparation method thereof |
| KR20180000864A (en) * | 2016-06-24 | 2018-01-04 | 순천대학교 산학협력단 | A microzyme feed composition for chicken comprising meal beetle and a method for increasing feed efficiency and meatiness of chicken by using same |
| CN108056357A (en) * | 2017-11-30 | 2018-05-22 | 南宁学院 | A kind of method for preventing feed mold |
| CN110959799A (en) * | 2018-09-28 | 2020-04-07 | 湖南现代资源生物科技有限公司 | Preparation method and application of feed mildew preventive |
| CN110973443A (en) * | 2019-12-23 | 2020-04-10 | 宜兴市天石饲料有限公司 | Propionic acid and sodium propionate type Chinese herbal medicine mildew preventive and preparation method thereof |
-
2022
- 2022-07-14 CN CN202210832673.8A patent/CN115176957A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040170729A1 (en) * | 2003-02-28 | 2004-09-02 | Jesuadimai Ignatius Xavier Antony | Mold inhibitor having reduced corrosiveness |
| CN105166587A (en) * | 2015-09-07 | 2015-12-23 | 王璐 | Drying mildewproof bactericide for feeds |
| KR20180000864A (en) * | 2016-06-24 | 2018-01-04 | 순천대학교 산학협력단 | A microzyme feed composition for chicken comprising meal beetle and a method for increasing feed efficiency and meatiness of chicken by using same |
| CN107259294A (en) * | 2017-06-21 | 2017-10-20 | 宜兴市天石饲料有限公司 | Feedstuff mildew-resistant additive and preparation method thereof |
| CN107212240A (en) * | 2017-07-19 | 2017-09-29 | 合肥浦邦农业科技有限公司 | A kind of Midew preventive for feed and preparation method thereof |
| CN108056357A (en) * | 2017-11-30 | 2018-05-22 | 南宁学院 | A kind of method for preventing feed mold |
| CN110959799A (en) * | 2018-09-28 | 2020-04-07 | 湖南现代资源生物科技有限公司 | Preparation method and application of feed mildew preventive |
| CN110973443A (en) * | 2019-12-23 | 2020-04-10 | 宜兴市天石饲料有限公司 | Propionic acid and sodium propionate type Chinese herbal medicine mildew preventive and preparation method thereof |
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