CN115154335A - 烤粉的制备方法及彩妆产品 - Google Patents
烤粉的制备方法及彩妆产品 Download PDFInfo
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- CN115154335A CN115154335A CN202210880422.7A CN202210880422A CN115154335A CN 115154335 A CN115154335 A CN 115154335A CN 202210880422 A CN202210880422 A CN 202210880422A CN 115154335 A CN115154335 A CN 115154335A
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Abstract
本申请涉及一种烤粉的制备方法及彩妆产品。制备方法包括：将粉体主料与添加料进行混合，得到混合分散浆料；在第一环境条件下采用超临界CO2对混合分散浆料进行干燥处理，所述第一环境条件包括第一温度25～50℃及第一压强5～50MPa；接着进行焙烧得到烤粉。本申请利用超临界CO2流体扩散系数比液体大，渗透性好，传质过程阻力小的特性，通过超临界CO2对烤粉进行干燥，使CO2能够进入物质内部，与烤粉粒子发生温和、快速地的交换或传递，物质本身不会发生收缩、碎裂，从而能够很大程度上保持被烘烤物质的结构和状态，有效防止物料烤粉的粉体粒子的团聚趋势加剧、凝并，及毛细孔的塌陷，避免烤粉比表面积和孔容降低，解决现有的烤粉工艺中存在的技术问题。
Description
技术领域
本申请涉及彩妆工艺技术领域，特别是涉及一种烤粉的制备方法及彩妆产品。
背景技术
在彩妆行业中，烤粉成为一种主流彩妆型品类，包括粉饼、胭脂和眼影等具体的产品类型，按制备类型可以分为油蜡烤粉和乳液烤粉等烤粉产品。
与普通压粉工艺制备的彩妆粉相比，采用焙烤制得的烤粉贴肤性更好，涂抹更均匀、细腻、容易上色。烤粉工艺一般是直接对浆料高温烘烤得到成品。但是高温烘烤导致得到烤粉粒子团聚，毛细孔塌陷严重，烤粉的粒子团聚和毛细孔塌陷导致比表面积和孔容降低，使得烤粉的应用体在使用中不够丝滑。
因此，为了解决上述技术问题，本申请进行了相应研究，并得到解决上述问题的如下技术方案。
发明内容
本申请实施例提供的烤粉的制备方法，能够解决现有的烤粉工艺在较高煅烧温度下使粒子团聚、毛细孔塌陷严重，导致烤粉比表面和孔容降低的问题。
本申请实施例提供一种烤粉在彩妆产品中的应用，即作为彩装产品的组成组分，彩妆产品具体是隔离霜、粉饼、胭脂、遮瑕膏、粉底、眉笔、眼影盘、眼线笔、睫毛膏、腮红、修容和口红中的一种，其中均包括根据本申请的烤粉制备方法制备的烤粉。
本申请的实施例提供的遮瑕膏，包括通过烤粉的制备方法制备的烤粉，能够使遮瑕膏具有良好的耐寒热稳定性和细腻滑爽的肤感和滋润度，解决现有的烤粉在应用体中不够丝滑的技术问题。
本申请的第一方面是提供一种烤粉的制备方法，包括：
将粉体主料与添加料进行混合，得到混合分散浆料；
在第一环境条件下采用超临界CO2对所述混合分散浆料进行干燥处理得到干燥后的粉体，所述第一环境条件包括第一温度25℃至50℃，以及第一压强5MPa至50MPa的条件参数；
将完成干燥的所述粉体进行焙烧即得到烤粉。
超临界干燥是液体CO2置换样品中溶剂的过程，然后调节温度、压强，缓慢降压获得干燥产品，CO2可以继续循环利用，符合环保、可持续发展的理念。
根据本申请的一个实施例，得到混合分散浆料的步骤包括：
选取各粉体进行搅拌混合得到所述粉体主料，其中，搅拌转速300rpm至800rpm，混合时间为5分钟至15分钟；以及将所述添加料添加到所述粉体主料中搅拌混合，得到混合分散浆料；其中，所述添加料的混合转速与所述粉体主料的转速相同，混合时间为1分钟至5分钟；所述干燥处理步骤中所述混合分散浆料的干燥处理时间为5分钟至30分钟：所述焙烧步骤中所述粉体的焙烧条件为：焙烧温度60℃至120℃，焙烧时间1小时至5小时。
根据本申请的一个实施例，得到所述粉体主料的混合条件为搅拌转速400rpm至600rpm，混合时间5分钟至10分钟；所述添加料的混合时间为1分钟至3分钟；所述干燥处理的环境条件为：干燥温度为35℃至45℃，干燥压强为10MPa至15MPa，干燥处理的时间为10分钟至20分钟：焙烧条件为：焙烧温度70℃至90℃，焙烧时间1小时至2小时。
根据本申请的一个实施例，混合分散浆料采用烘箱进行干燥，烘箱中设有烘干用的模具，完成分散后的混合分散浆料置于模具内，干燥步骤的干燥条件为：干燥温度为25℃至50℃，优选干燥温度为35℃至45℃；干燥压强为5MPa至50MPa，优选干燥压强为10MPa至15MPa，干燥时间为5分钟至30分钟，优选干燥时间10分钟至20分钟。
根据本申请的一个实施例，粉体主料包括改性淀粉、合成氟金云母、绢云母、滑石粉、硅石、一氮化硼、有机硅弹体、碳酸钙、珍珠粉、蚕丝粉、硬脂酸锌、硬脂酸铝、月桂酰赖氨酸、聚甲基倍半硅氧烷、高岭土、尼龙-12，锦纶-12、金刚粉、氧化锌、硫酸钡、羟基磷灰石、氢氧化铝、肉豆蔻酸镁、软玉粉中的一种或者多种。
具体的，改性淀粉是改性玉米淀粉、淀粉辛烯基琥珀酸铝、醋脂淀粉、羧甲基淀粉中的一种或几种。有机硅弹性体包括聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷交联聚合物、乙烯基聚二甲基硅氧烷/聚甲基硅氧烷倍半硅氧烷交联聚合物、聚二甲基硅氧烷交联聚合物中的一种或几种。
在本申请得到混合分散浆料的步骤中，添加料包括粘合剂、活性物、抗氧化剂、防腐剂。
根据本申请的一个实施例，粘合剂为辛酸/癸酸甘油三酯、白油、异壬酸异壬酯、合成蜡、聚二甲基硅氧烷、二苯基聚二甲基硅氧烷、环五聚二甲基硅氧烷、乙基纤维素、微晶蜡、白蜂蜡、氢化棕榈油酸、地蜡、硬脂醇硬脂酸蜡、小烛树蜡、巴西棕榈蜡、石蜡、纯地蜡、糊精棕榈酸酯、三山嵛精中的一种或者多种。
根据本申请的一个实施例，活性物为透明质酸钠、水解透明质酸、寡聚透明质酸、赤芝提取物、茉莉花提取物、山茶花提取物、白及提取物、白术提取物、桃花提取物、白蔹提取物中的一种或者多种。
根据本申请的一个实施例，抗氧化剂为生育酚、维生素E、白藜芦醇、对羟基苯乙酮、维生素C、富勒烯、抗坏血酸葡萄糖苷、抗坏血酸棕榈酸酯、生育酚乙酸酯、视黄醇棕榈酸酯中的一种或者多种。维生素C即抗坏血酸。
根据本申请的一个实施例，防腐剂为苯氧乙醇、乙基己基甘油、辛甘醇中的一种或者几种。
相比一般烤箱焙烧工艺制备的烤粉，采用本申请在超临界CO2条件下烤粉的制备方法制备的烤粉，具有更好的杀菌效果；其中，超临界CO2是指压强大于一般大气压0.101325MPa条件下，在本申请中即指模具内5MPa至50MPa下介于气态与液态之间的CO2流体。
本申请利用超临界CO2流体的流动性、渗透性好、传质过程阻力小和具有高扩散系数的特性，通过超临界CO2流体对混合分散浆料进行超临界干燥处理，使超临界CO2流体利用渗透性好的特性充斥于粉体粒子间隙，与烤粉粒子发生温和、快速地进行物质的交换或传递，从而能够很大程度上保持被烘烤或者焙烧物质的结构和状态，粉体物质本身不会发生收缩、碎裂，有效防止烤粉的粉体粒子的团聚趋势加剧、凝并，以及毛细孔的塌陷。同时，通过介于气态和液态间流动的超临界CO2流体传热，能够降低干燥温度，干燥过程温和，更大程度上避免了烤粉受热不均匀而破坏物体结构，如避免粉体粒子比表面和孔容减小；在干燥过程中利用溶解能力大的特性，溶解吸收混合分散浆料中的待干燥成分，使干燥速度更快。
采用超临界CO2对混合分散浆料进行干燥制备的烤粉粒子尺寸分布均匀，大小可控。制备的烤粉内部网络和孔隙结构与焙烧的粉饼基本相同，但烤粉粒子不会产生团聚，且比表面积和孔容也不会变小。在制备的彩妆中显示出优越性，如动态摩擦系数小，使得粉质更细腻，肤感更好，具有极佳的滑爽效果。以工艺时间计算，相比现有工艺烘烤4小时至10小时的时长，本申请采用超临界CO2制备烤粉的时长缩短至1小时到5.5小时.，大大缩短了制备用的时间，且过程更简单，适合工业化，具有显著的经济效益和环保效果。
附图说明
下面将参考附图来描述本申请示例性实施例的特征、优点和技术效果。
图1为本申请提供的烤粉制备方法的步骤流程图；
具体实施方式
下面结合附图和实施例对本申请的实施方式作进一步详细描述。以下实施例的详细描述和附图用于示例性地说明本申请的原理，但不能用来限制本申请的范围，即本申请不限于所描述的实施例。
本申请实施例提供一种烤粉的制备方法，以及根据该方法制得的烤粉。烤粉包括粉体主料和添加料，具体的，添加料包括粘合剂、活性物、抗氧化剂、防腐剂。
粉体主料，即填充粉，选自改性淀粉、合成氟金云母、绢云母、滑石粉、硅石、一氮化硼、有机硅弹体、碳酸钙、珍珠粉、蚕丝粉、硬脂酸锌、硬脂酸铝、月桂酰赖氨酸、聚甲基倍半硅氧烷、高岭土、尼龙-12，锦纶-12、金刚粉、氧化锌、硫酸钡、羟基磷灰石、氢氧化铝、肉豆蔻酸镁、软玉粉中的一种或者多种，组分可以任意比例复配。
粘合剂选自辛酸/癸酸甘油三酯、白油、异壬酸异壬酯、合成蜡、聚二甲基硅氧烷、二苯基聚二甲基硅氧烷、环五聚二甲基硅氧烷、乙基纤维素、微晶蜡、白蜂蜡、氢化棕榈油酸、地蜡、硬脂醇硬脂酸蜡、小烛树蜡、巴西棕榈蜡、石蜡、纯地蜡、糊精棕榈酸酯、三山嵛精中的一种或者多种。
活性物选自透明质酸钠、水解透明质酸、寡聚透明质酸、赤芝提取物、茉莉花提取物、山茶花提取物、白及提取物、白术提取物、桃花提取物、白蔹提取物中的一种或者多种。抗氧化剂选自生育酚、维生素E、白藜芦醇、对羟基苯乙酮、维生素C、富勒烯、抗坏血酸葡萄糖苷、抗坏血酸棕榈酸酯、生育酚乙酸酯、视黄醇棕榈酸酯中的一种或者多种。防腐剂选自苯氧乙醇、乙基己基甘油、辛甘醇中的一种或者几种。
图1为本申请提供的烤粉的制备方法的步骤流程图。
如图1所示，根据本申请的实施方式，烤粉的制备方法包括以下步骤：
S1、将粉体主料与添加料进行混合，得到混合分散浆料；得到混合分散浆料的具体步骤包括：首先，选取各填充粉粉体进行搅拌混合得到所述粉体主料，其中，搅拌转速300至800rpm，混合时间为5分钟至15分钟；其次，将所述添加料添加到所述粉体主料中搅拌混合，得到混合分散浆料；其中，所述添加料的混合转速与所述粉体主料的转速相同，混合时间为1分钟至5分钟。
S2、然后，在包括第一温度25～50℃，以及第一压强5～50MPa的第一环境参数条件下采用超临界CO2对所述混合分散浆料进行干燥处理5分钟至30分钟，得到干燥后的粉体；
S3、最后，将完成干燥的所述粉体在60～120℃焙烧温度下焙烧1～5小时，即得到烤粉。
详细实施例
下述实施例更具体地描述了本申请公开的内容，这些实施例仅仅用于阐述性说明，因为在本申请公开内容的范围内进行各种修改和变化对本领域技术人员来说是明显的。除非另有声明，以下实施例中所报道的所有份、百分比、和比值都是基于重量计，而且实施例中使用的所有试剂都可商购获得或是按照常规方法进行合成获得，并且可直接使用而无需进一步处理，以及实施例中使用的仪器均可商购获得。
实施例1：根据本发明的第一方面实施例提供的烤粉的制备方法，包括：将各填充粉粉体加入到搅拌机中，在500rpm至600rpm转速下进行充分搅拌10分钟，得到粉体主料；然后向粉体主料中加入粘合剂、活性物、抗氧化剂、防腐剂四种添加料进行快速搅拌1分钟，得到混合分散浆料；将混合分散浆料装入模具中，在35℃至40℃的温度、10MPa至15MPa的压强下采用超临界CO2干燥10分钟至15分钟，得到干燥的粉体，然后对干燥后的粉体进行焙烧，焙烧温度为80℃-90℃，焙烧1小时，得到烤粉。其中，
填充粉：改性玉米淀粉34.85份，硅石25份，聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷有机硅弹体10份，一氮化硼1份，月桂酰赖氨酸1份，硬脂酸镁8份；
粘合剂：聚二甲基硅氧烷2份，合成蜡6.5份、辛酸/癸酸甘油三酯8份；
活性物：寡聚透明质酸0.5份，山茶花提取物0.5份，白术提取物0.5份，桃花提取物0.5份，赤芝提取物0.5份；
抗氧化剂：维生素E乙酸酯0.2份；防腐剂：苯氧乙醇0.45份，乙基己基甘油0.50份。
实施例2：根据本发明的第一方面实施例提供的烤粉的制备方法，包括：将各填充粉粉体加入到搅拌机中，在500rpm至600rpm转速下进行充分搅拌10分钟，得到粉体主料；然后向粉体主料中加入粘合剂、活性物、抗氧化剂、防腐剂四种添加料并进行快速搅拌1分钟，得到混合分散浆料；将混合分散浆料装入模具中，在35℃至40℃的温度10MPa至15MPa的压强下采用超临界CO2干燥10分钟至15m分钟，得到干燥的粉体，然后对干燥后的粉体进行焙烧，焙烧温度为80℃至90℃，焙烧1小时，得到烤粉。其中，
填充粉：滑石粉34.85份，合成氟金云母25份，碳酸钙5份，高岭土5份，一氮化硼1份，月桂酰赖氨酸1份，羟基磷灰石8份；
粘合剂：三山嵛精2份，石蜡6.5份、辛酸/癸酸甘油三酯8份；
活性物：寡聚透明质酸0.5份，茉莉花提取物0.5份，白及提取物0.5份，桃花提取物0.5份，赤芝提取物0.5份；
抗氧化剂：抗坏血酸棕榈酸酯0.2份；防腐剂：苯氧乙醇0.45份，乙基己基甘油0.50份。
实施例3：根据本发明的第一方面实施例提供的烤粉的制备方法，包括：将各填充粉粉体加入到搅拌机中，在500rpm至600rpm转速下进行充分搅拌10分钟，得到粉体主料；然后向粉体主料中加入粘合剂、活性物、抗氧化剂、防腐剂四种添加料进行快速搅拌1分钟，得到混合分散浆料：将混合分散浆料装入模具中，在35℃至40℃的温度、10MPa至15MPa的压强下采用超临界CO2干燥10分钟至15分钟，得到干燥的粉体，然后对干燥后的粉体进行焙烧，焙烧温度为80℃至90℃，焙烧2小时，得到烤粉。其中，
填充粉为：淀粉辛烯基琥珀酸铝13.85份，滑石粉20份，碳酸钙25份，聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷有机硅弹体10份，金刚粉1份，锦纶-12为10份；
粘合剂：聚二甲基硅氧烷2份，合成蜡6.5份、辛酸/癸酸甘油三酯8份；
活性物：寡聚透明质酸0.5份，山茶花提取物0.5份，白术提取物0.5份，桃花提取物0.5份，赤芝提取物0.5份；
抗氧化剂：维生素E乙酸酯0.2份：防腐剂：苯氧乙醇0.45份，乙基己基甘油0.50份。
实施例4：根据本发明的第一方面实施例提供的烤粉的制备方法，包括：将各填充粉粉体加入到搅拌机中，在500rpm至600rpm转速下进行充分搅拌10分钟，得到粉体主料；然后向粉体主料中加入粘合剂、活性物、抗氧化剂、防腐剂四种添加料进行快速搅拌1分钟，得到混合分散浆料；将混合分散浆料装入模具中，在35℃至40℃的温度、10MPa至15MPa压强下采用超临界CO2干燥10分钟至15分钟，得到干燥的粉体，然后对干燥后的粉体进行焙烧，焙烧温度为80℃至90℃，焙烧2小时，得到烤粉。其中，
填充粉为：重量比为1：1的改性玉米淀粉和醋脂淀粉34.85份，硅石25份，聚二甲基硅氧烷交联聚合物有机硅弹体10份，珍珠粉1份，蚕丝粉1份，肉豆蔻酸镁8份；
粘合剂：聚二甲基硅氧烷2份，地蜡6.5份、辛酸/癸酸甘油三酯8份；
活性物：透明质酸钠0.5份，山茶花提取物1份，桃花提取物1份；
抗氧化剂：维生素E乙酸酯0.2份；防腐剂：苯氧乙醇0.45份，乙基己基甘油0.50份。
实施例5：根据本发明的第一方面实施例提供的烤粉的制备方法，包括：将各填充粉粉体加入到搅拌机中，在500rpm至600rpm转速下进行充分搅拌10分钟得到粉体主料，然后向粉体主料中加入粘合剂、活性物、抗氧化剂、防腐剂四种添加料进行快速搅拌1分钟，得到混合分散浆料：将混合分散浆料装入模具中，在35℃至40℃的温度、10MPa至15MPa的压强下采用超临界CO2干燥10分钟至15分钟，得到干燥的粉体，然后对干燥后的粉体进行焙烧，焙烧温度为80℃-90℃，焙烧2小时，得到烤粉。其中，
填充粉为：滑石粉34.85份，硅石25份，聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷有机硅弹体10份，聚甲基倍半硅氧烷1份，软玉粉5份，合成氟金云母4份；
粘合剂：异壬酸异壬酯6份，白峰蜡1.5份，石蜡3份，地蜡2份，二苯基聚二甲基硅氧烷4份；
活性物：水解透明质酸1.0份，赤芝提取物1.5份；
抗氧化剂：维生素E乙酸酯0.2份：防腐剂：苯氧乙醇0.45份，乙基己基甘油0.50份。
对比例：根据现有的烤粉技术制备烤粉的工艺，将各填充粉加入到搅拌机中，500rpm至600rpm转速下进行充分搅拌10分钟，然后加入粘合剂、活性物、抗氧化剂、防腐剂进行快速搅拌1分钟，将得到的产品装入模具中，压制成型后，放入烤箱以90℃烘烤4小时，制得烤粉。其中，
填充粉为：改性玉米淀粉34.85份，硅石25份，聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷有机硅弹体10份，一氮化硼1份，月桂酰赖氨酸1份，硬脂酸镁8份；
粘合剂：聚二甲基硅氧烷2份，合成蜡6.5份、辛酸/癸酸甘油三酯8份；
活性物：寡聚透明质酸0.5份，山茶花提取物0.5份，白术提取物0.5份，桃花提取物0.5份，赤芝提取物0.5份；
抗氧化剂：维生素E乙酸酯0.2份：防腐剂：苯氧乙醇0.45份，乙基己基甘油0.50份。
接着将实施例1-5和对比例制备的烤粉进行性能测试，测试方法及实验数据如下：性能测试
1.稳定性测试
稳定性测试以实施例1至5和对比例制得的烤粉制作的粉饼进行。
耐寒耐热试验：
为了保持产品在储存、使用过程中性能稳定、不发生物理化学变化，不出现渗油、析水、粗粒、破乳等现象，应对配方进行高温、低温储存稳定性试验。实验室中粉饼在高温、低温储存的稳定性试验可采取以下方法进行：
1)在40℃至50℃电热恒温培养箱中放置30天至50天，恢复室温后观察；
2)24小时内，在0℃至50℃之间来回频繁变化，即在0℃恒温箱中存放2小时，再放入50℃下存放2小时，依次循环多次，如此反复操作15天到30天，恢复室温后观察；
3)在-5℃及40℃下循环存放3次，分别每次存放24小时，即在-5℃存放24小时后，在室温下存放24小时，再放入40℃恒温箱中存放24小时，依次循环3次，观察其稳定性；
4)在-5℃下存放1周，观察其稳定性。
粘合力试验：
将实施例1-5和对比例制备的烤粉制成粉饼，使粉饼在离地面1米左右距离进行自由落体落下(切勿用力往下扔粉饼)，观察粉饼是否有裂开的现象。
表1样品的稳定性检测
| 样品 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | 对比例 |
| 耐寒 | 无变化 | 无变化 | 无变化 | 无变化 | 无变化 | 无变化 |
| 耐热 | 无变化 | 无变化 | 无变化 | 无变化 | 无变化 | 无变化 |
| 粘合力 | 无变化 | 无变化 | 无变化 | 无变化 | 无变化 | 无变化 |
表1的结果表明，采用超临界CO2干燥和焙烧与对比例中的普通烘箱焙烧制得的烤粉稳定性均良好。实施例1-3中采用超临界CO2的焙烧时间不同，分别是1、1.5、2小时，但稳定性差别不大，证明焙烧时长对样品稳定性几乎无影响。但是，对比超临界CO2焙烧与烘箱烘烤，前者所用时间更少。
2.肤感测试
2.1动摩擦系数测试
动摩擦系数通过Kato-Tech Co公司生产的“kes-se”摩擦测试仪测定得到粉末的平均摩擦系数。本测试仪可精确测试人接触物体时感觉到的“光滑感”、“粗糙感”、“爽滑感”，并以数值进行分析。将试样的滑爽度作为平均摩擦系数(符号：MIU)，将粗燥感作为平均摩擦系数的变动(摩擦系数μ的平均偏差、符号MMD)，通过将其数值化，使以往凭借主观感官评价的产品性能评价，可通过客观的数据进行定量化评价。
测试目的在于将人指尖的感觉数值化，仅将人感觉的到的频率区域(活性2次滤波器)作为数据获取，传感器部的荷重和表面处理也模仿指尖的设计，数据可与感官评价关联在一起，即使是微小的差异也可通过高度的再现性正确输出。
测试方法：
1、将一个试样的试验表面向上，平整的固定在摩擦系数测试仪水平试验台上。试样设置方向应与试验台的长度方向平行：
2、将同一实施例的另一试样的试验表面向下，包住滑块，用胶带在滑块前沿和上表面固定式样；
3、将固定好有式样的滑块无冲击地放在第一个试样中央，并使两试样的试验方向与滑块方向平行且测力系统恰好不受力。
4、力的第一个峰值为静摩擦力Fs。两式样相对移动70mm内的力的平均值(不包括静摩擦力)为动摩擦力Fd。
5、如在静摩擦力之后出现力值震荡，测不能测量动摩擦力。此时应取消滑块和负荷传感器间的弹簧，单独测量动摩擦力。
表2各样品的动态摩擦系数测试结果
| 样品 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | 对比例 |
| Fd | 0.45 | 0.25 | 0.38 | 0.46 | 0.24 | 0.58 |
表2的结果表明，实施例2、5动摩擦系数最小，其次是实施例3，对比例动摩擦系数较大；可能是实施例2、3、5含有滑石粉，具有极佳的滑爽效果，使得动态摩擦系数较小的缘故，且根据实施例2、5和3的对比可以得出滑石粉含量越高，动态摩擦系数越小；动态摩擦系数小能够从侧面证明采用超临界CO2干燥处理和焙烧过的烤粉粉体颗粒细腻、蓬松肤感好。
2.2受试者测试
将本申请实施例1-5和对比例制备的烤粉测试肌肤感受。性能检测试验随机选择18-40岁的健康女性36人，用同样的烤粉在左胳膊内侧画线(右胳膊为空白对照)，记录刚涂抹上试样时手上的肌肤感受，根据评判标准，取得平均值。评判标准为：
表3测试指标和评价指标
表4各样品的肤感测试结果
| 样品 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | 对比例 |
| 肤感 | 8.6 | 9.8 | 9.0 | 8.5 | 9.7 | 7.1 |
| 滋润度 | 9.0 | 9.1 | 9.0 | 9.3 | 9.9 | 8.9 |
表4的结果表明，实施例5和实施例2肤感较好，可能是滑石粉比较滑爽的原因；采用含超临界CO2处理过的烤粉的样品比对比例烘箱焙烧的烤粉肤感均要好；各实施例滋润度较好，差别不大，然而实施例5肤感较其它实施例要好，可能是透明质酸钠的含量较高，滋润度较好的缘故。
从上述性能测试结果可以看出，与现有的烤粉工艺相比，本申请实施方式制备烤粉的方法，通过利用CO2临界状态下的扩散系数大、渗透性好、传质过程阻力小的特性，采用超临界CO2对混合分散浆料进行干燥和焙烧，使CO2能够进入烤粉粉体内部，使烤粉粉体本身不会发生收缩、碎裂，从而保持烤粉的结构和状态，避免粉体粒子团聚、凝并，以及毛细孔塌陷；且CO2本身处于流体状态，能够将受到的热量快速传递到烤粉粉体中，进一步避免烤粉粉体局部过热导致的粒子团聚和毛细孔塌陷；同时超临界CO2还可以通过吸收热量和溶解力大的特性调节降低干燥处理时的干燥温度。
实施例1-5制备的烤粉具有在耐寒、热状况下，烤粉本申及粘合力具有良好的稳定性；且实施例1-5的动摩擦系数均小于对比例的动摩擦系数，说明本申请的烤粉粉体颗粒细腻，不容易团聚，且采用滑石粉能够进一步减小动摩擦系数；根据本申请的技术方案制备的烤粉具有滑爽的肤感和滋润度。
虽然已经参考优选实施例对本申请进行了描述，但在不脱离本申请的范围的情况下，可以对其进行各种改进并且可以用等效物替换其中的部件，尤其是，只要不存在结构冲突，各个实施例中所提到的各项技术特征均可以任意方式组合起来。本申请并不局限于文中公开的特定实施例，而是包括落入权利要求的范围内的所有技术方案。
Claims (14)
1.一种烤粉的制备方法，其特征在于，包括：
将粉体主料与添加料进行混合，得到混合分散浆料；
在第一环境条件下采用超临界CO2对所述混合分散浆料进行干燥处理得到干燥后的粉体，所述第一环境条件包括第一温度25～50℃，以及第一压强5～50MPa的条件参数；
将完成干燥的所述粉体进行焙烧得到烤粉。
2.根据权利要求1所述的烤粉的制备方法，其特征在于，所述得到混合分散浆料的步骤中，所述粉体主材包括改性淀粉、合成氟金云母、绢云母、滑石粉、硅石、一氮化硼、有机硅弹体、碳酸钙、珍珠粉、蚕丝粉、硬脂酸锌、硬脂酸铝、月桂酰赖氨酸、聚甲基倍半硅氧烷、高岭土、尼龙-12，锦纶-12、金刚粉、氧化锌、硫酸钡、羟基磷灰石、氢氧化铝、肉豆蔻酸镁、软玉粉中的一种或者多种。
3.根据权利要求1或2所述的烤粉的制备方法，其特征在于，所述得到混合分散浆料的步骤中，所述添加料包括粘合剂、活性物、抗氧化剂、防腐剂。
4.根据权利要求3所述的烤粉的制备方法，其特征在于，所述粘合剂为辛酸/癸酸甘油三酯、白油、异壬酸异壬酯、合成蜡、聚二甲基硅氧烷、二苯基聚二甲基硅氧烷、环五聚二甲基硅氧烷、乙基纤维素、微晶蜡、白蜂蜡、氢化棕榈油酸、地蜡、硬脂醇硬脂酸蜡、小烛树蜡、巴西棕榈蜡、石蜡、纯地蜡、糊精棕榈酸酯、三山嵛精中的一种或者多种。
5.根据权利要求3所述的烤粉的制备方法，其特征在于，所述活性物为透明质酸钠、水解透明质酸、寡聚透明质酸、赤芝提取物、茉莉花提取物、山茶花提取物、白及提取物、白术提取物、桃花提取物、白蔹提取物中的一种或者多种。
6.根据权利要求3所述的烤粉的制备方法，其特征在于，所述抗氧化剂为生育酚、维生素E、白藜芦醇、对羟基苯乙酮、维生素C、富勒烯、抗坏血酸葡萄糖苷、抗坏血酸棕榈酸酯、生育酚乙酸酯、视黄醇棕榈酸酯中的一种或者多种。
7.根据权利要求3所述的烤粉的制备方法，其特征在于，所述防腐剂为苯氧乙醇、乙基己基甘油、辛甘醇中的一种或者几种。
8.根据权利要求1所述的烤粉的制备方法，其特征在于，所述得到混合分散浆料的步骤包括：
选取各粉体进行搅拌混合得到所述粉体主料，其中，搅拌转速300rpm至800rpm，混合时间为5分钟至15分钟；
将所述添加料添加到所述粉体主料中搅拌混合，得到混合分散浆料：其中，所述添加料的混合转速与所述粉体主料的转速相同，混合时间为1分钟至5分钟。
9.根据权利要求8所述的烤粉的制备方法，其特征在于，所述干燥处理步骤中所述混合分散浆料的干燥处理时间为5分钟至30分钟。
10.根据权利要求8所述的烤粉的制备方法，其特征在于，所述粉体的焙烧条件为：焙烧温度60℃至120℃，焙烧时间1小时至5小时。
11.根据权利要求8所述的烤粉的制备方法，其特征在于，所述得到所述粉体主料的混合条件为搅拌转速400rpm至600rpm，混合时间5分钟至10分钟；所述添加料的混合时间为1分钟至3分钟。
12.据权利要求9所述的烤粉的制备方法，其特征在于，所述干燥处理的环境条件为：干燥温度为35℃至45℃，干燥压强为10MPa至15MPa，干燥处理的时间为10分钟至20分钟。
13.据权利要求10所述的烤粉的制备方法，其特征在于，所述粉体的焙烧条件为：焙烧温度70℃-90℃，焙烧时间1小时至2小时。
14.一种彩妆产品，其特征在于，包括烤粉，所述烤粉根据权利要求1-13任一项所述的烤粉制备方法得到。
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