CN115137685A

CN115137685A - Mild and refreshing female care wet tissue and preparation method thereof

Info

Publication number: CN115137685A
Application number: CN202110884025.2A
Authority: CN
Inventors: 张玉霞; 王卫平
Original assignee: Tongling Tiantian Paper Technology Co ltd
Current assignee: Tongling Tiantian Paper Technology Co ltd
Priority date: 2021-08-03
Filing date: 2021-08-03
Publication date: 2022-10-04
Anticipated expiration: 2041-08-03
Also published as: CN115137685B

Abstract

The invention provides a mild and refreshing feminine care wet tissue in a first aspect, and provides a preparation method of the mild and refreshing feminine care wet tissue in a second aspect. The female care wet tissue is prepared from the raw materials of non-woven fabrics, plant extracts, a humectant, an antibacterial agent, a preservative, citric acid, sodium citrate, ethanol and deionized water, has excellent bactericidal performance, is fresh and cool in use, is not sticky, and has good use feeling.

Description

Mild and refreshing female care wet tissue and preparation method thereof

Technical Field

The invention relates to the field of sanitary products, in particular to the field of nursing wet tissues, and more particularly relates to a mild and refreshing female nursing wet tissue and a preparation method thereof.

Background

The skin of the female private part is tender and sensitive, the private environment is complex, and the cuticle of the private part is thin, so that the infection is easily caused. Urinary tract infection, bacterial vaginitis, mycotic vaginitis, trichomonas vaginitis and non-specific vaginitis are common diseases and frequently encountered diseases of women caused by unclean pudendum. Therefore, it is very important to keep the pudendum clean to ensure the health of women.

In recent years, with the development of wet tissue markets, some wet tissues which can be used for female private part nursing begin to appear, but the quality and the effect of the wet tissues are different, and some wet tissues for private part nursing can only embody the cleaning effect, cannot play the roles of sterilization and bacteriostasis, and cannot maintain the female private parts when in use. Based on the above, the invention provides a mild and refreshing feminine care wet tissue and a preparation method thereof.

Disclosure of Invention

The invention provides a mild and refreshing female care wet tissue in a first aspect, which consists of a non-woven fabric and a care solution; the care solution comprises the following raw materials: plant extract, humectant, antibacterial agent, antiseptic, citric acid, sodium citrate, ethanol, and deionized water.

Preferably, the plant extract is at least one selected from aloe vera extract, tea tree extract, wormwood extract, wild chrysanthemum extract, motherwort extract, rose extract, and the like.

Preferably, the plant extract is a compound substance of an aloe extract, an artemisia argyi extract, a wild chrysanthemum extract, a motherwort extract and a rose extract.

Preferably, the humectant is at least one selected from sodium hyaluronate, glycerin, butylene glycol and 1, 3-propylene glycol.

Preferably, the antibacterial agent is at least one selected from isothiazolinone and its derivatives, polyhexamethylene guanidine salt, chlorhexidine gluconate, cetylpyridinium chloride, chlorhexidine acetate, and chlorhexidine hydrochloride.

Preferably, the preservative is at least one selected from phenoxyethanol, glyceryl caprylate, caprylhydroxamic acid and butanediol.

Preferably, the preservative is a compound substance of phenoxyethanol and glyceryl caprylate.

Preferably, the care solution comprises the following raw materials in percentage by mass: 1-5% of plant extract, 1-10% of humectant, 0.05-0.2% of antibacterial agent, 0.005-0.02% of preservative, 0.01-0.03% of citric acid, 0.01-0.03% of sodium citrate, 2-8% of ethanol and the balance of deionized water.

The invention provides a preparation method of a mild and refreshing female care wet tissue, which is characterized by comprising the following steps:

(1) Preparation of a care solution: adding deionized water, ethanol and humectant into a preparation container, stirring, adding plant extract, humectant, antiseptic and antibacterial agent, mixing, and adjusting pH with citric acid and sodium citrate to obtain a solution;

(2) Preparing a female care wet tissue: and immersing the non-woven fabric into the care solution to obtain the female care wet tissue.

Preferably, the pH value of the care solution in the step (1) is 4.5-6.5.

Compared with the prior art, the invention has the following beneficial effects:

1. in the care solution system prepared by the invention, the combination capability between the care solution and the non-woven fabric is improved through the combined action of a plurality of raw materials.

2. In the care solution system prepared by the invention, the stability of the care solution is improved by adding the specific preservative, and the effect of removing peculiar smell is achieved by the combined action of various plant extracts.

3. In the care solution system prepared by the invention, the combined action of the specific preservative and the specific antibacterial agent further improves the sterilization effect.

4. The feminine care wet tissue prepared by the invention is fresh and cool in use process, is not sticky, and has good use feeling.

Detailed Description

Preferably, the mass ratio of the aloe extract, the wormwood extract, the wild chrysanthemum extract, the motherwort extract and the rose extract is (2-5): (1-3): 2: (1-2): 2.

preferably, the mass ratio of the aloe extract, the wormwood extract, the wild chrysanthemum extract, the motherwort extract and the rose extract is 3:1.5:2:1:2.

the flos Chrysanthemi Indici extract is extracted from the head-shaped inflorescence of Compositae plant such as flos Chrysanthemi Indici (Chrysanthemum indicum L), flos Chrysanthemi Indici (C.borealemak.), and herba Dendranthematis indici (C.lavandaefolium (Fisch.)) and is rich in organic components such as Chrysanthemum alcohol, chrysanthemum ketone, sabinene, vanillyl alcohol, glycosides, epoxy xanthophyll, luteolin, glyceryl behenate, and palmitic acid, and has antibacterial, antiviral, heat clearing away, antiinflammatory, antioxidant, and skin aging preventing effects.

The herba leonuri extract is an extract of the overground part of herba leonuri (leonurus heterophyllus Sweet) of the family labiatae, is rich in organic components such as leonurine, rutin, fumaric acid, leonuridine, arginine, stigmasterol, sitosterol and the like, has good effects of conditioning irregular menstruation, dysmenorrhea, amenorrhea, lochiorrhea, postpartum blood stasis and abdominal pain and the like, and also has the effects of beautifying, face nourishing, aging resisting and aging.

Preferably, the moisturizer is sodium hyaluronate and 1, 3-propylene glycol.

Preferably, the mass ratio of the sodium hyaluronate to the 1, 3-propylene glycol is (0.2-0.8): 2.5.

Preferably, the antibacterial agent is polyhexamethylene guanidine hydrochloride.

Preferably, the mass ratio of the phenoxyethanol to the glyceryl caprylate is 0.5: (2-5).

Preferably, the care solution comprises the following raw materials in percentage by mass: 1-5% of plant extract, 1-10% of humectant, 0.05-0.2% of antibacterial agent, 0.005-0.02% of preservative, 0.01-0.03% of citric acid, 0.01-0.03% of sodium citrate, 2-8% of ethanol and deionized water for supplementing the rest.

In a second aspect, the invention provides a method for preparing a mild and refreshing feminine care wet tissue, which comprises the following steps:

(1) Preparation of a care solution: adding deionized water, ethanol and humectant into a preparation container, stirring, adding plant extract, humectant, antiseptic and antibacterial agent, mixing, and adjusting pH with citric acid and sodium citrate to obtain a care solution;

(2) Preparing a female care wet tissue: and immersing the non-woven fabric in the care solution to obtain the female care wet tissue.

Preferably, the pH value of the care solution in the step (1) is 4.5-6.5.

Preferably, the non-woven fabric is a cotton non-woven fabric which is purchased from Tuguan, tuyuan Compound science and technology Co., ltd, and the model is TY0246.

In the care solution system prepared by the invention, the glyceryl caprylate is added to be intertwined with other raw materials in the care solution, such as plant extracts, through long carbon chains, so that the dispersibility of the plant extracts in the care solution system is improved, and the stability of the care solution system is further improved.

According to the female care wet tissue prepared by the invention, the plurality of specific plant extracts are added into the care solution, active substances contained in the specific plant extracts are fully utilized, the activity of private cell is enhanced, channel warming, cold dispelling, pain relieving and uterus warming are realized, and the health of female pudendum and genital tract is effectively protected.

The present invention will be specifically described below by way of examples. It is to be noted that the following examples are given solely for the purpose of illustration and are not to be construed as limitations on the scope of the invention, as many insubstantial modifications and variations of the invention described above will now occur to those skilled in the art.

Example 1

In a first aspect of the invention, a mild and refreshing feminine care wet tissue is provided, which comprises a non-woven fabric and a care solution. The nursing liquid comprises, by mass, 5% of a plant extract, 2.5% of a humectant, 0.05% of polyhexamethylene guanidine hydrochloride, 0.02% of a preservative, 0.015% of citric acid, 0.01% of sodium citrate, 5% of ethanol and the balance deionized water.

The plant extract is a compound substance of an aloe extract, a wormwood extract, a wild chrysanthemum extract, a motherwort extract and a rose extract, and the mass ratio of the aloe extract to the wormwood extract to the wild chrysanthemum extract to the motherwort extract to the rose extract is 3:1.5:2:1:2.

the humectant is sodium hyaluronate and 1, 3-propylene glycol, and the mass ratio of the sodium hyaluronate to the 1, 3-propylene glycol is 0.3:2.5.

the preservative is phenoxyethanol and glyceryl caprylate, and the mass ratio of the phenoxyethanol to the glyceryl caprylate is 0.5:4.

(1) Preparation of a care solution: adding deionized water, ethanol and humectant into a preparation container, stirring, adding plant extract, antiseptic and polyhexamethylene guanidine hydrochloride, mixing, and adjusting pH with citric acid and sodium citrate to obtain a solution with pH of 6.0;

Wherein the aloe extract is purchased from Shaanxi Bai Cunkang Biotech Co., ltd.

The mugwort extract is purchased from Bai Cukang Biotech limited, shaanxi.

The wild chrysanthemum extract is purchased from Shaanxi Baikukang Biotech limited.

Herba Leonuri extract is purchased from Shaanxi Bai Cunkang Biotech limited.

The rose extract is purchased from Shaanxi Bai Cunkang Biotech Co., ltd.

Sodium hyaluronate was purchased from eastern Han dynasty peptide Bio-pharmaceuticals, inc. and has a molecular weight of 20 ten thousand.

Polyhexamethyleneguanidine hydrochloride, CAS No.: 57028-96-3, purchased from Taianjiayue biochemical industries, ltd.

The non-woven fabric is all-cotton non-woven fabric, which is purchased from Tuguan Tuyuan composite science and technology Limited and has the model number TY0246.

Example 2

The invention provides a mild and refreshing feminine care wet tissue which comprises a non-woven fabric and a care solution. The nursing liquid comprises, by mass, 2% of plant extract, 3% of humectant, 0.08% of polyhexamethylene guanidine hydrochloride, 0.02% of preservative, 0.015% of citric acid, 0.01% of sodium citrate, 4% of ethanol and the balance of deionized water.

the preservative is phenoxyethanol and glyceryl caprylate, and the mass ratio of the phenoxyethanol to the glyceryl caprylate is 0.5:2.

(1) Preparation of the care solution: adding deionized water, ethanol and humectant into a preparation container, stirring, adding plant extract, antiseptic and polyhexamethylene guanidine hydrochloride, mixing, and adjusting pH with citric acid and sodium citrate to obtain a pH of 5.5;

Wherein the aloe extract is purchased from Bai Cukang Biotech limited, shaanxi.

The mugwort extract is purchased from Bai Cukang Biotech limited, shaanxi.

Herba Leonuri extract is purchased from Shaanxi Bai Cunkang Biotech limited.

The rose extract is purchased from Shaanxi Baikukang Biotech limited.

Polyhexamethyleneguanidine hydrochloride, CAS No.: 57028-96-3, purchased from Taian Jiayue Biochemical Co., ltd.

Example 3

The first aspect of the invention provides a mild and refreshing feminine care wet wipe, and the second aspect of the invention provides a preparation method of the mild and refreshing feminine care wet wipe, wherein the specific implementation mode and the raw materials are the same as those in example 1, except that no plant extract is added.

Example 4

The invention provides a mild and refreshing feminine care wet tissue in a first aspect, and provides a preparation method of the mild and refreshing feminine care wet tissue in a second aspect, the specific implementation mode and the used raw materials are the same as those in example 1, and the difference is that the preservative is phenoxyethanol.

Example 5

The first aspect of the invention provides a mild and refreshing feminine care wet tissue, and the second aspect of the invention provides a preparation method of the mild and refreshing feminine care wet tissue, wherein the specific implementation mode and the used raw materials are the same as those in example 1, except that the humectant is 1, 3-propylene glycol.

Performance testing

1. And (4) the adsorption performance of the care solution.

Cutting a non-woven fabric into square cloth blocks with the same mass, recording the mass as W0, immersing the cut cloth blocks into the nursing liquid prepared in the embodiment for 1min, taking out the cloth blocks, immediately hanging the cloth blocks in a thermostat with the temperature of 20 ℃ and the humidity of 75%, placing a glass collector below each cloth block, collecting the dropped nursing liquid, hanging the cloth blocks for 10min, weighing the cloth blocks, recording the mass as W2, and weighing the nursing liquid in the glass collector, wherein the recording mass is W1. And (6) calculating the adsorption capacity of the care solution.

Adsorption capacity = (W2-W0)/(W1 + W2-W0) × 100%.

2. Stability of the care solution.

The nursing liquid is filled into a glass beaker, the glass beaker is sealed by a breathable sealing film, and the glass beaker is placed in a thermostat with the temperature of 54 ℃ and the humidity of 90 percent for 45 days. After being taken out, the nursing liquid is observed whether to have precipitation and layering phenomena or not, and whether the smell of the nursing liquid changes or not is observed.

3. Sterilizing property.

And (4) carrying out bacteriostatic performance test by referring to the GB/T15979-2002 standard.

The results of the above tests are reported in table 1.

TABLE 1

	Adsorption capacity	Stability of	Sterilizing property
				Example 1	82.50％	No peculiar smell, no precipitate and no layering	99.40％
Example 2	81.40％	No peculiar smell, no precipitate and no layering	99.30％
				Example 3	80.10％	No peculiar smell, no precipitation and layering	97.80％
Example 4	78.50％	Peculiar smell, precipitate and no layering	94.20％
				Example 5	60.80％	No peculiar smell, no precipitate and no layering	97.60％

Finally, it is pointed out that the foregoing examples are illustrative only, serving to explain some of the characteristics of the process according to the invention. The appended claims are intended to claim as broad a scope as can be conceived and the examples presented herein are merely illustrative of selected implementations in accordance with all possible combinations of examples. Accordingly, it is applicants' intention that the appended claims are not to be limited by the choice of examples illustrating features of the invention. Where the claims recite a range of values, such ranges are intended to include all sub-ranges subsumed therein, and variations within the ranges are intended to be encompassed by the claims as appended hereto where possible.

Claims

1. A mild and refreshing female care wet tissue is characterized in that the care wet tissue consists of non-woven fabrics and a care solution; the care solution comprises the following raw materials: plant extract, humectant, antibacterial agent, antiseptic, citric acid, sodium citrate, ethanol, and deionized water.

2. The feminine care wet wipe as set forth in claim 1, wherein the plant extract is at least one selected from the group consisting of aloe vera extract, tea tree extract, wormwood extract, wild chrysanthemum extract, motherwort extract, rose extract, and the like.

3. The feminine care wet wipe set forth in claim 1 wherein the botanical extract is a combination of aloe vera extract, wormwood extract, wild chrysanthemum extract, motherwort extract, and rose extract.

4. The feminine care wet wipe as set forth in claim 1 wherein the humectant is selected from at least one of sodium hyaluronate, glycerin, butylene glycol, and 1, 3-propylene glycol.

5. The feminine care wet wipe set forth in claim 1 wherein the antimicrobial agent is selected from at least one of isothiazolinone and derivatives thereof, polyhexamethylene guanidine salts, chlorhexidine gluconate, cetylpyridinium chloride, chlorhexidine acetate, chlorhexidine hydrochloride.

6. The feminine care wet wipe of claim 1, wherein the preservative is selected from at least one of phenoxyethanol, glyceryl caprylate, caprylhydroxamic acid, butylene glycol.

7. The feminine care wet wipe of claim 6, wherein the preservative is a combination of phenoxyethanol and glyceryl caprylate.

8. The feminine care wet wipe as set forth in claim 1, wherein the lotion comprises the following raw materials in percentage by mass: 1-5% of plant extract, 1-10% of humectant, 0.05-0.2% of antibacterial agent, 0.005-0.02% of preservative, 0.01-0.03% of citric acid, 0.01-0.03% of sodium citrate, 2-8% of ethanol and deionized water for supplementing the rest.

9. A method of making a feminine care wet wipe as set forth in any one of claims 1-8 comprising the steps of:

10. The method according to claim 9, wherein the pH of the solution in step (1) is 4.5 to 6.5.