CN115119954A - Floral fragrant mint essence for electronic atomized liquid and preparation method thereof - Google Patents

Floral fragrant mint essence for electronic atomized liquid and preparation method thereof Download PDF

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CN115119954A
CN115119954A CN202210681876.1A CN202210681876A CN115119954A CN 115119954 A CN115119954 A CN 115119954A CN 202210681876 A CN202210681876 A CN 202210681876A CN 115119954 A CN115119954 A CN 115119954A
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mint
floral
fragrance
oil
atomized liquid
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CN115119954B (en
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华健
翁艾慧
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Shenzhen Vatican Living Life Science Ltd By Share Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303Plant extracts other than tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/10Devices using liquid inhalable precursors
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a floral fragrant mint essence base for electronic atomized liquid and a preparation method thereof, wherein the floral fragrant mint essence base for electronic atomized liquid comprises the following raw materials in percentage by mass: 15.0 to 25.0 percent of water-soluble floral essence, 0.05 to 0.15 percent of citronella oil, 0.03 to 0.07 percent of lemon oil, 1.2 to 1.6 percent of mint extract, 0.1 to 0.5 percent of menthol, 0.03 to 0.07 percent of spearmint oil and 72.61 to 83.59 percent of propylene glycol. According to the invention, the flower fragrance, the citronella grass fragrance and the mint fragrance are combined into the flower and grass fragrant mint base for the electronic atomized liquid, the diversity of the mint taste of the electronic atomized liquid is enriched, the sweetness of fruity mint and mint is removed, the single spicy mint taste is removed, and the flower fragrance and the mint fragrance are mixed, so that the flower and grass fragrant mint base for the electronic atomized liquid, which can relieve depression, fatigue and virus, can coordinate the flower fragrance, the lemon grass fragrance and the mint fragrance, is provided, the advantages of the flower fragrance, the lemon grass fragrance and the mint fragrance are complementary, and the flower fragrance, the lemon grass fragrance and the mint fragrance can relieve emotion and pressure of a smoker while being fresh and palatable, so that a certain cure is brought to the body and the mind.

Description

Floral fragrant mint essence for electronic atomized liquid and preparation method thereof
Technical Field
The invention relates to the technical field of electronic atomized liquid, in particular to a floral fragrant mint essence base for electronic atomized liquid and a preparation method thereof.
Background
Unlike traditional cigarettes, electronic cigarettes have evolved a wide variety of taste styles from the original tobacco-like flavor to flavors of mint, fruits, drinks, and the like, with the mint flavor often appearing in electronic cigarette products. Mint is a plant of the genus mentha of the family labiatae, is one of the traditional Chinese medicines, and has the effects of dispelling wind, dissipating heat and detoxifying. The modern medicine further analyzes the components of the mint, and the mint oil and the menthol can achieve the effects of refreshing, cholagogue, anti-inflammatory, analgesic, antifungal, antiviral and even antitussive to a certain extent.
The mint flavors commonly used in electronic cigarettes are peppermint, spearmint, tobacco mint and fruity mint, and the individual lemongrass flavors are common in electronic cigarettes. However, at present, electronic cigarettes with floral or herbal savory flavors rarely appear on the market. The fragrant fragrance of flowers can bring pleasant and relaxed feeling to people, and the 'flower fragrance disease treatment' in ancient China and early plant tincture of European people are proved by practice that the flower fragrance can have certain influence on the emotion and health of people. The flower fragrance contains aromatic esters, alcohols, aldehydes, ketones, etc., and can stimulate respiratory center of human body to promote respiratory function. The beneficial fragrance can regulate nervous system, promote blood circulation, and make energy, thinking and organism activity reach high level, namely 'flower fragrance therapy'.
Therefore, how to prepare the electronic cigarette with the fragrance of the flowers or the fragrance of the flowers and the grass and the flavor of the mint according to the electronic cigarette with the single flavor of the lemongrass or the flavor of the mint becomes one of the products which are urgently needed in the market of the electronic cigarette at present.
Disclosure of Invention
In order to solve the problem that the electronic cigarette with single mint taste is bitter and spicy in taste, the first object of the application is to provide a floral and herbal mint essence base for electronic atomized liquid. The second purpose of the application is to provide a preparation method of the floral fragrant mint essence base for the electronic atomized liquid. Different from pungent and cool stimulation of pure mint and sweet and greasy fruit-flavor mint, the warmness and softness of flowers and plants enrich the diversity of mint flavors of the electronic atomized liquid.
In order to achieve the purpose, the invention provides the following technical scheme:
a floral fragrant mint essence base for electronic atomized liquid comprises the following raw materials in percentage by mass:
Figure BDA0003696574410000021
as a further scheme of the invention, the method comprises the following raw materials in percentage by mass:
Figure BDA0003696574410000022
as a further aspect of the present invention, the water-soluble floral essence comprises an essence prepared by mixing one or more of hexyl acetate, geraniol, cinnamyl alcohol, myrcene, nerol, terpineol, benzyl acetate, phenethyl alcohol, linalool, white orchid oil, tree orchid oil, anisic aldehyde, methyl dihydrojasmonate, lily essence, jasmine oil, rose oil, geranyl acetate, styryl acetate, ylang oil, lavender oil and beta-ionone with a solvent.
As a further aspect of the invention, the solvent is propylene glycol.
As a further proposal of the invention, the citronella oil is prepared by steam distillation of the whole grass of citronella.
As a still further aspect of the present invention, the lemon oil is lemon oil extracted from fresh peel of lemon.
As a still further aspect of the present invention, the mint extract is an essential oil component extracted from the aerial part of pustula pulchella of the family labiatae.
As a further aspect of the present invention, the spearmint oil is a liquid extracted from fresh leaves and stems of spearmint, which is also called spearmint or spearmint.
A preparation method of a floral fragrant mint essence base for electronic atomization liquid comprises the following steps:
s10, weighing propylene glycol according to mass percentage, taking the propylene glycol as a solvent, sequentially adding citronella oil, lemon oil and spearmint oil according to mass percentage into the propylene glycol, adding water-soluble flower fragrance essence, and uniformly stirring to obtain a flower and plant fragrance base solution;
and S20, adding the mint extract and the menthol which are weighed according to the mass percentage into the floral scent base liquid in the step S10, and stirring and uniformly mixing to obtain the floral scent mint base.
As a further scheme of the invention, the mixing temperature in the preparation process of the floral fragrant mint essence base is 20-40 ℃, and the stirring speed is 150-220 r/min.
As a further scheme of the invention, the floral herb savory base is also used for preparing electronic cigarette atomized liquid, and the electronic cigarette atomized liquid is prepared from the following raw materials by weight:
10g of floral mint essence, 2g of cooling agent, 0.1g of sucralose, 5g of nicotine, 50g of glycerol and 42.9g of propylene glycol.
As a further scheme of the invention, the preparation method of the electronic cigarette atomized liquid comprises the following steps: and uniformly stirring and mixing 10g of the weighed floral mint essence, 2g of cooling agent, 0.1g of sucralose, 5g of nicotine, 50g of glycerol and 42.9g of propylene glycol to obtain the electronic cigarette atomized liquid.
Compared with the prior art, the invention has the beneficial effects that:
according to the floral fragrant mint base and the preparation method thereof, the floral fragrance, the citronella grass fragrance and the mint fragrance are combined to form the floral fragrant mint base for the electronic atomized liquid, the diversity of mint tastes of the electronic atomized liquid is enriched, the sweetness of fruity mint and mint is removed, the single spicy taste of mint is removed, the floral fragrance and the mint fragrance are mixed, and the floral fragrant mint base for the electronic atomized liquid, which can relieve depression, resist fatigue and resist viruses, is provided.
The floral fragrance mint essence prepared from the raw materials used in the application according to the proportion is applied to the electronic atomized liquid, so that the floral fragrance, the lemon grass fragrance and the mint fragrance can be coordinated, the advantages of the floral fragrance, the lemon grass fragrance and the mint fragrance are complemented, and the floral fragrance, the lemon grass fragrance and the mint fragrance can relieve the emotion of a smoker, release pressure and bring certain cure to the mind and body while being fresh and palatable.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to specific embodiments.
Aiming at the mint tastes commonly used in electronic cigarettes, such as peppermint, spearmint, tobacco mint and fruity mint, the electronic cigarettes with the fragrance of flowers or plants and mint taste rarely appear in the market at present. How to prepare the electronic cigarette with the fragrance of flowers or the fragrance of flowers and plants and the taste of mint according to the single citronella flavor or mint taste of the electronic cigarette becomes one of the products which are urgently needed in the market of the electronic cigarette at present.
The application provides a floral fragrant mint essence base for electronic atomized liquid, which comprises the following raw materials in percentage by mass: 15.0 to 25.0 percent of water-soluble floral essence, 0.05 to 0.15 percent of citronella oil, 0.03 to 0.07 percent of lemon oil, 1.2 to 1.6 percent of mint extract, 0.1 to 0.5 percent of menthol, 0.03 to 0.07 percent of spearmint oil and 72.61 to 83.59 percent of propylene glycol.
In the present application, unless otherwise specified, the water-soluble floral fragrance includes fragrances obtained by mixing propylene glycol with one or more fragrances selected from hexyl acetate, geraniol, cinnamyl alcohol, myrcene, nerol, terpineol, benzyl acetate, phenethyl alcohol, linalool, ylang-ylang, magnolia oil, anisic aldehyde, methyl dihydrojasmonate, irisone, jasmine oil, rose oil, geranyl acetate, styryl acetate, ylang-ylang oil, lavender oil and β -ionone.
In the present application, the citronella oil is prepared from the whole grass of citronella by steam distillation; the lemon oil is lemon oil extracted from fresh peel of lemon; the herba Menthae extract is volatile oil extracted from aerial part of herba Typhae of Labiatae; the spearmint oil is liquid extracted from fresh stems and leaves of spearmint, and is also called spearmint or spearmint.
The cymbopogon citratus used in the application, which is of medicinal value, is a common tropical perfume with a pleasant and refreshing lemon aroma. The extract is obtained by extracting citronella oil, mainly contains vanillin, vanillyl alcohol and geraniol, and can be used for sterilizing, diminishing inflammation, relaxing muscles and tendons, activating collaterals and relieving pain.
The application also provides a preparation method of the floral fragrant mint essence base for the electronic atomized liquid, which comprises the following steps:
s10, weighing propylene glycol according to mass percentage, taking the propylene glycol as a solvent, sequentially adding citronella oil, lemon oil and spearmint oil according to mass percentage into the propylene glycol, adding water-soluble flower fragrance essence, and uniformly stirring to obtain a flower and plant fragrance base solution;
and S20, adding the mint extract and the menthol which are weighed according to the mass percentage into the floral scent base liquid in the step S10, and stirring and uniformly mixing to obtain the floral scent mint base.
In the application, the floral fragrant mint essence is also used for preparing electronic cigarette atomized liquid, and the electronic cigarette atomized liquid is prepared from the following raw materials in parts by weight:
10g of floral mint essence, 2g of cooling agent, 0.1g of sucralose, 5g of nicotine, 50g of glycerol and 42.9g of propylene glycol.
The raw materials of the electronic cigarette atomized liquid are stirred and mixed uniformly, and the electronic cigarette atomized liquid is obtained.
The following description will be made in conjunction with specific examples 1 to 13.
In examples 1 to 13, the raw materials and the amounts of the raw materials for the floral fragrant menthyl group of the electronic atomization liquid are shown in table 1 of the following table, wherein the amounts of the raw materials are g.
Table 1 examples 1-13 materials and amounts (g) of materials for floral savory mint base for electronically atomized liquid
Figure BDA0003696574410000051
Figure BDA0003696574410000061
Figure BDA0003696574410000071
The specific examples and preparation methods are as follows:
weighing water-soluble floral essence, citronella oil, lemon oil, mint extract, menthol, spearmint oil and propylene glycol required by preparing a floral fragrant and mint base according to the raw materials and the raw material dosage shown in table 1, wherein during preparation, the propylene glycol is weighed according to the mass percentage and is used as a solvent, the citronella oil, the lemon oil and the spearmint oil are sequentially added into the propylene glycol according to the mass percentage, and the water-soluble floral essence is added and then stirred and mixed uniformly to obtain a floral fragrant base solution;
adding the mint extract and menthol which are weighed according to the mass percentage into the floral scent base liquid, and stirring and uniformly mixing to obtain the floral scent mint scent base.
Comparative example
The difference from example 1 is that the water-soluble floral essence and the weights of the citronella oil and the lemon oil are different, and the mint bases of comparative examples 1 to 3 are configured, wherein the raw materials and the amounts of the raw materials of the mint bases of comparative examples 1 to 3 are shown in table 2 of the following table, and the amounts of the raw materials are g.
TABLE 2 COMPARATIVE EXAMPLES 1-3 peppermint-based raw materials and amounts (g) of raw materials
Component name Comparative example 1 Comparative example 2 Comparative example 3
Water-soluble floral essence/g / 20.0 20.0
CitronellaOil/g 0.1 / 0.1
Lemon oil/g 0.05 0.05 /
Mint extract/g 1.4 1.4 1.4
Menthol/g 0.3 0.3 0.3
Spearmint oil/g 0.05 0.05 0.05
Propylene glycol/g 98.08 78.18 78.13
The specific examples and preparation methods are as follows:
weighing water-soluble floral essence, citronella oil, lemon oil, mint extract, menthol, spearmint oil and propylene glycol required by preparing the menthyl according to the raw materials and the raw material dosage shown in the table 2, when the preparation is carried out, weighing the propylene glycol according to the mass percentage, taking the propylene glycol as a solvent, sequentially adding the citronella oil, the lemon oil and the spearmint oil into the propylene glycol according to the mass percentage, adding the water-soluble floral essence, and then stirring and uniformly mixing to obtain the menthyl base solution;
adding the mint extract and menthol which are weighed according to the mass percentage into the floral scent base liquid, and stirring and uniformly mixing to obtain the mint scent base.
Performance test
The mint-type bases prepared in examples 1 to 13 and comparative examples 1 to 3 were prepared as an electronic atomized liquid: 10g of the example or the comparative example, 2g of cooling agent, 0.1g of sucralose, 5g of nicotine, 50g of glycerol and 42.9g of propylene glycol are taken, stirred and mixed uniformly, and respectively put into an electronic smoking set for smoking evaluation. Wherein the resistance value of the atomizer of the electronic smoking set is 1.2 omega heating wire, and the atomization voltage is 3.8V. The number of persons participating in the suction evaluation is 20, and the evaluation items comprise harmony, flower aroma, freshness, joyfulness and mint aroma by adopting a nameless evaluation system. After the scores are counted, a comprehensive average score is calculated, the score is about one digit after the decimal point, and the judgment result is shown in the table 3 of the following table:
TABLE 3 determination results
Figure BDA0003696574410000081
Figure BDA0003696574410000091
As can be seen by combining comparative examples 1 to 3 with Table 3, the fresh and faint notes of the floral aroma can smooth the bitterness and pungency peculiar to peppermint, and reduce the discomfort of the smoker to the mouth when the smoker inhales the peppermint aroma. The fresh, sour and sweet and fragrant aroma of the citronella oil and the lemon oil can enrich the whole aroma framework, further mix the pungency of the mint, bring pleasant sense for smokers, set off the sweet aroma of the flower aroma, and avoid the deviation of the flower aroma to the style of the daily chemical flower aroma.
It can be seen from the combination of examples 4-13 and Table 3 that the increased amount of menthol and spearmint oil resulted in a gradually pronounced bitter or even pungent taste of mint, a single overall fragrance, and a loss of the sense of layering. And the addition amount of the lemongrass and the lemon oil is increased, so that the fragrance of the flower is obviously covered, and the key tone of the flower is lost.
As can be seen from the combination of examples 1-3 and table 3, the overall fragrance harmony of the atomized liquid decreased with the increase in the amount of the water-soluble floral fragrance added. An appropriate floral concentration gives a pleasant and soothing feeling, but too high a floral concentration causes mental and physiological discomfort to the human body.
In conclusion, the floral herbal fragrance mint essence prepared from the raw materials used in the application according to the proportion is applied to the electronic atomization liquid, so that the floral fragrance, the lemon herbal fragrance and the mint fragrance can be coordinated, the advantages of the floral fragrance, the lemon herbal fragrance and the mint fragrance are complemented, and the fragrance, the lemon herbal fragrance and the mint fragrance are refreshing and palatable, so that a smoker can relieve the emotion and the stress, and a certain cure effect is brought to the mind and the body.
Therefore, the floral fragrant mint base and the preparation method thereof provided by the invention combine the floral fragrance, the citronella grass fragrance and the mint fragrance into the floral fragrant mint base for the electronic atomized liquid, enrich the diversity of the mint taste of the electronic atomized liquid, remove the sweetness of fruity mint and mint, and the single spicy taste of mint, mix the floral fragrance and the mint fragrance, and provide the floral fragrant mint base for the electronic atomized liquid, which can relieve depression, resist fatigue and resist viruses.
While the preferred embodiments of the present invention have been described in detail, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art.

Claims (10)

1. A floral fragrant mint essence for electronic atomized liquid is characterized by comprising the following raw materials in percentage by mass:
Figure FDA0003696574400000011
2. the floral fragrant mint base for the electronic atomized liquid as claimed in claim 1, comprising the following raw materials by mass:
Figure FDA0003696574400000012
3. the floral savory for electronically atomized liquid of claim 2, wherein the water-soluble floral fragrance comprises a fragrance obtained by mixing one or more fragrances selected from the group consisting of hexyl acetate, geraniol, cinnamyl alcohol, myrcene, nerol, terpineol, benzyl acetate, phenethyl alcohol, linalool, alband leaf oil, magnolia oil, anisic aldehyde, methyl dihydrojasmonate, lily of the valley, jasmine oil, rose oil, geranyl acetate, styryl acetate, ylacetate, ylang-ylang oil, lavender oil and β -ionone with a solvent.
4. A floral savory base for an electronically atomized liquid according to claim 3, wherein the solvent is propylene glycol.
5. The floral bergamot base for an electronically atomized liquid of claim 2, wherein the citronella oil is prepared from whole grass of citronella by steam distillation.
6. The floral scented peppermint base for use in an electronically atomized liquid of claim 2, wherein the lemon oil is lemon oil extracted from fresh peel of lemon.
7. The floral savory for electronically atomized liquid of claim 2, wherein the mint extract is a volatile oil component extracted from aerial parts of a plant, pulegand, of the family labiatae.
8. The floral vanilla mint flavor base for an electronically atomized liquid as claimed in claim 2, wherein said spearmint oil is a liquid extracted from fresh stems and leaves of spearmint, also known as spearmint or spearmint.
9. A method for preparing a floral scented mint base for an electronically atomized liquid as claimed in any one of claims 1 to 8, comprising the steps of:
s10, weighing propylene glycol according to mass percentage, taking the propylene glycol as a solvent, sequentially adding citronella oil, lemon oil and spearmint oil according to mass percentage into the propylene glycol, adding water-soluble flower fragrance essence, and uniformly stirring to obtain a flower and plant fragrance base solution;
and S20, adding the mint extract and the menthol which are weighed according to the mass percentage into the floral scent base liquid in the step S10, and stirring and uniformly mixing to obtain the floral scent mint base.
10. The method for preparing the floral bergamot base for the electronically atomized liquid as claimed in claim 9, wherein the floral bergamot base is further used for preparing the electronically atomized liquid, and the electronically atomized liquid is prepared from the following raw materials by weight:
10g of floral mint essence, 2g of cooling agent, 0.1g of sucralose, 5g of nicotine, 50g of glycerol and 42.9g of propylene glycol.
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CN111671134A (en) * 2020-06-22 2020-09-18 福建中烟工业有限责任公司 Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid
CN113615860A (en) * 2021-08-16 2021-11-09 深圳市真味生物科技有限公司 Cooling agent for cigarettes and cooling taste type electronic atomized liquid

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CN104983063A (en) * 2015-05-31 2015-10-21 中国烟草总公司郑州烟草研究院 Improved preparation method for electronic cigarette smoke solution
US20170251723A1 (en) * 2016-03-03 2017-09-07 Altria Client Services Llc Methods to add menthol, botanic materials, and/or non-botanic materials to a cartridge, and/or an electronic vaping device including the cartridge
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2024131267A1 (en) * 2022-12-19 2024-06-27 惠州市新泓威科技有限公司 Electronic cigarette atomization liquid having antidepressant effect, and preparation method therefor

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