CN115028495A - Multifunctional water-soluble fertilizer and preparation method thereof - Google Patents
Multifunctional water-soluble fertilizer and preparation method thereof Download PDFInfo
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- CN115028495A CN115028495A CN202210709636.8A CN202210709636A CN115028495A CN 115028495 A CN115028495 A CN 115028495A CN 202210709636 A CN202210709636 A CN 202210709636A CN 115028495 A CN115028495 A CN 115028495A
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- vitamin
- soluble fertilizer
- stirring
- multifunctional water
- water
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 229940088594 vitamin Drugs 0.000 claims abstract description 23
- 229930003231 vitamin Natural products 0.000 claims abstract description 23
- 235000013343 vitamin Nutrition 0.000 claims abstract description 23
- 239000011782 vitamin Substances 0.000 claims abstract description 23
- 239000000654 additive Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 230000000749 insecticidal effect Effects 0.000 claims abstract description 17
- 230000000996 additive effect Effects 0.000 claims abstract description 16
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims abstract description 14
- -1 compound sodium nitrophenolate Chemical class 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 8
- CJUUXVFWKYRHAR-UHFFFAOYSA-M 1-Naphthaleneacetic acid sodium salt Chemical compound [Na+].C1=CC=C2C(CC(=O)[O-])=CC=CC2=C1 CJUUXVFWKYRHAR-UHFFFAOYSA-M 0.000 claims abstract description 7
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 claims abstract description 7
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 claims abstract description 7
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 7
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims abstract description 7
- 235000011130 ammonium sulphate Nutrition 0.000 claims abstract description 7
- 239000004202 carbamide Substances 0.000 claims abstract description 7
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002509 fulvic acid Substances 0.000 claims abstract description 7
- 229940095100 fulvic acid Drugs 0.000 claims abstract description 7
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims abstract description 7
- 235000019341 magnesium sulphate Nutrition 0.000 claims abstract description 7
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims abstract description 7
- 235000019796 monopotassium phosphate Nutrition 0.000 claims abstract description 7
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229910052939 potassium sulfate Inorganic materials 0.000 claims abstract description 7
- 235000011151 potassium sulphates Nutrition 0.000 claims abstract description 7
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims abstract description 7
- 238000005507 spraying Methods 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims description 38
- 238000003756 stirring Methods 0.000 claims description 37
- 239000000284 extract Substances 0.000 claims description 25
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- 241000736851 Tagetes Species 0.000 claims description 24
- 230000009920 chelation Effects 0.000 claims description 24
- 240000000233 Melia azedarach Species 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 21
- 238000001816 cooling Methods 0.000 claims description 20
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 16
- 229930003270 Vitamin B Natural products 0.000 claims description 15
- 235000019156 vitamin B Nutrition 0.000 claims description 15
- 239000011720 vitamin B Substances 0.000 claims description 15
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 claims description 14
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 12
- 238000005303 weighing Methods 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 10
- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 claims description 10
- 229910000831 Steel Inorganic materials 0.000 claims description 9
- 239000000498 cooling water Substances 0.000 claims description 9
- 239000010959 steel Substances 0.000 claims description 9
- 238000003860 storage Methods 0.000 claims description 9
- 238000000108 ultra-filtration Methods 0.000 claims description 9
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 8
- 229930003268 Vitamin C Natural products 0.000 claims description 8
- 239000000287 crude extract Substances 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- 239000008103 glucose Substances 0.000 claims description 8
- 150000005846 sugar alcohols Chemical class 0.000 claims description 8
- 235000019154 vitamin C Nutrition 0.000 claims description 8
- 239000011718 vitamin C Substances 0.000 claims description 8
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 8
- YBJHBAHKTGYVGT-ZKWXMUAHSA-N (+)-Biotin Chemical compound N1C(=O)N[C@@H]2[C@H](CCCCC(=O)O)SC[C@@H]21 YBJHBAHKTGYVGT-ZKWXMUAHSA-N 0.000 claims description 7
- GHOKWGTUZJEAQD-UHFFFAOYSA-N Chick antidermatitis factor Natural products OCC(C)(C)C(O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-UHFFFAOYSA-N 0.000 claims description 7
- SQUHHTBVTRBESD-UHFFFAOYSA-N Hexa-Ac-myo-Inositol Natural products CC(=O)OC1C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C1OC(C)=O SQUHHTBVTRBESD-UHFFFAOYSA-N 0.000 claims description 7
- 229930003756 Vitamin B7 Natural products 0.000 claims description 7
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 claims description 7
- 229960000367 inositol Drugs 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 229960003966 nicotinamide Drugs 0.000 claims description 7
- 235000005152 nicotinamide Nutrition 0.000 claims description 7
- 239000011570 nicotinamide Substances 0.000 claims description 7
- 235000019161 pantothenic acid Nutrition 0.000 claims description 7
- 239000011713 pantothenic acid Substances 0.000 claims description 7
- 229940055726 pantothenic acid Drugs 0.000 claims description 7
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 claims description 7
- 235000011912 vitamin B7 Nutrition 0.000 claims description 7
- 239000011735 vitamin B7 Substances 0.000 claims description 7
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 229930003779 Vitamin B12 Natural products 0.000 claims description 5
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 claims description 5
- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 claims description 5
- 235000019163 vitamin B12 Nutrition 0.000 claims description 5
- 239000011715 vitamin B12 Substances 0.000 claims description 5
- 235000019158 vitamin B6 Nutrition 0.000 claims description 5
- 239000011726 vitamin B6 Substances 0.000 claims description 5
- 229940011671 vitamin b6 Drugs 0.000 claims description 5
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 claims description 4
- 241000628997 Flos Species 0.000 claims description 4
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 claims description 4
- 229930003451 Vitamin B1 Natural products 0.000 claims description 4
- 229930003471 Vitamin B2 Natural products 0.000 claims description 4
- 229930003761 Vitamin B9 Natural products 0.000 claims description 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 4
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 claims description 4
- 238000004811 liquid chromatography Methods 0.000 claims description 4
- 239000012528 membrane Substances 0.000 claims description 4
- 235000013379 molasses Nutrition 0.000 claims description 4
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 4
- 229960002477 riboflavin Drugs 0.000 claims description 4
- 229960003495 thiamine Drugs 0.000 claims description 4
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 claims description 4
- 235000010374 vitamin B1 Nutrition 0.000 claims description 4
- 239000011691 vitamin B1 Substances 0.000 claims description 4
- 235000019164 vitamin B2 Nutrition 0.000 claims description 4
- 239000011716 vitamin B2 Substances 0.000 claims description 4
- 235000019159 vitamin B9 Nutrition 0.000 claims description 4
- 239000011727 vitamin B9 Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 235000013877 carbamide Nutrition 0.000 claims description 3
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- 238000005485 electric heating Methods 0.000 claims description 3
- 239000012530 fluid Substances 0.000 claims description 3
- 239000011229 interlayer Substances 0.000 claims description 3
- 239000005416 organic matter Substances 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000012360 testing method Methods 0.000 claims description 3
- 239000000080 wetting agent Substances 0.000 claims description 3
- 239000000575 pesticide Substances 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 abstract description 10
- 238000003973 irrigation Methods 0.000 abstract description 5
- 230000002262 irrigation Effects 0.000 abstract description 5
- 238000011161 development Methods 0.000 abstract description 4
- 230000010354 integration Effects 0.000 abstract description 4
- 230000004720 fertilization Effects 0.000 abstract description 3
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 abstract description 3
- LWIHDJKSTIGBAC-UHFFFAOYSA-K potassium phosphate Substances [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 abstract description 3
- 230000037208 balanced nutrition Effects 0.000 abstract description 2
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- 238000010521 absorption reaction Methods 0.000 description 6
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- 235000013305 food Nutrition 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
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- 239000007921 spray Substances 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
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- 244000237986 Melia azadirachta Species 0.000 description 1
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- DFPAKSUCGFBDDF-ZQBYOMGUSA-N [14c]-nicotinamide Chemical compound N[14C](=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-ZQBYOMGUSA-N 0.000 description 1
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Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/26—Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agronomy & Crop Science (AREA)
- Mycology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Soil Sciences (AREA)
- Botany (AREA)
- Fertilizers (AREA)
Abstract
The invention belongs to the technical field of water-soluble fertilizers and discloses a multifunctional water-soluble fertilizer and a preparation method thereof, wherein the multifunctional water-soluble fertilizer comprises, by weight, 30% -50% of urea, 20% -30% of potassium sulfate, 20% -30% of organic matters, 10% -20% of monopotassium phosphate, 3% -7% of compound vitamins, 3% -7% of magnesium sulfate, 4% -8% of ammonium sulfate, 2% -4% of biochemical fulvic acid, 0.1% -0.2% of compound sodium nitrophenolate, 0.04% -0.06% of sodium naphthalene acetate, 0.3% -0.5% of sodium dodecyl benzene sulfonate, 0.2% -0.5% of an auxiliary agent and 0.01% -0.03% of an insecticidal additive. The multifunctional water-soluble fertilizer provided by the invention is easy to dissolve and absorb, the utilization rate is improved, the multifunctional water-soluble fertilizer can be applied to the fertilization requirements of spraying and drip irrigation, the integration of water and fertilizer is realized, the growth and development of crops are promoted, and comprehensive and balanced nutrition is provided for the growth and development of crops.
Description
Technical Field
The invention belongs to the technical field of water-soluble fertilizers, and particularly relates to a multifunctional water-soluble fertilizer and a preparation method thereof.
Background
At present, in agricultural production, chemical fertilizers are extremely important agricultural production resources. In recent decades, the production and consumption of chemical fertilizers in China have been rapidly increased, and become the largest chemical fertilizer producing and consuming countries in the world. However, the traditional compound fertilizer is easy to cause fertilizer loss, water eutrophication, soil structure damage, nutrient imbalance and the like. Meanwhile, the quality of agricultural products is reduced and the food safety problem is increasingly prominent due to the transitional pursuit of yield and the use of a large amount of hormones; the application of the vitamin to crops instead of hormone can increase the yield and improve the quality, and is safe and has no side effect. The water-soluble fertilizer avoids the defects of the traditional compound fertilizer as a novel environment-friendly fertilizer, is convenient to use, has the characteristics of instant dissolution, easy absorption, full nutrients, high utilization rate, water conservation, labor conservation and the like, can be applied by sprinkling irrigation, flushing, drip irrigation and soilless culture, and realizes the integration of water and fertilizer. Therefore, the research and the application of the multifunctional vitamin water-soluble fertilizer are one of measures for high efficiency, environmental protection, water saving and fertilizer saving.
The water-soluble fertilizer is a multi-element compound fertilizer capable of being dissolved in water, is easy to dissolve and absorb, improves the utilization rate, and can be applied to the fertilization requirement of spray and drip irrigation to realize water and fertilizer integration. The preparation of the water-soluble compound fertilizer has the characteristics of convenience, high efficiency, high quality and the like, and also has product diversification, one of the manifestations is that other materials can be additionally added in the granulation process, so that the nutrient composition of the product can be enlarged, the additional value of the product can be improved, and the method is an operation mode which is economic and has use value.
At present, various water-soluble fertilizers in the market are simple in components, few in types of contained nutrient components, single in function, low in utilization rate, high in hormone side effect, inconvenient to apply due to excessive water insoluble substances and secondary pollution caused by excessive heavy metal, and conventional elements used by some water-soluble fertilizers are not absorbed by crops or are low in absorption rate, so that the crops are deficient in elements, physiological diseases occur and disastrous. Therefore, a novel multifunctional water-soluble fertilizer and a preparation method thereof are needed.
Through the above analysis, the problems and defects of the prior art are as follows:
(1) the traditional compound fertilizer is easy to cause fertilizer loss, water eutrophication, soil structure damage, nutrient imbalance and the like. Meanwhile, the quality of agricultural products is reduced and the food safety problem is increasingly prominent due to the transitional pursuit of yield and the use of a large amount of hormones.
(2) Various water-soluble fertilizers in the market are simple in components, few in variety of contained nutritional ingredients, single in function, low in utilization rate, high in hormone content side effect, inconvenient to apply due to excessive water insoluble substances, and secondary pollution caused by excessive heavy metals, and the conventional elements used in some water-soluble fertilizers are not absorbed by crops or are low in absorption rate, so that the crops are deficient in elements, physiological diseases occur, and the loss is heavy.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a multifunctional water-soluble fertilizer and a preparation method thereof.
The invention is realized in such a way that the preparation method of the multifunctional water-soluble fertilizer comprises the following steps:
step one, preparing compound vitamin: mixing vitamin C, vitamin B6, vitamin B12 and nicotinamide according to a ratio of 1: 1: 1: 1, adding the mixture into a stirring kettle, and mixing and stirring for 10-20 min to form a mixture A; meanwhile, vitamin B1, vitamin B2, vitamin B9, vitamin H, pantothenic acid and inositol were mixed in a ratio of 1: 1: 2: 3, weighing the components according to the weight ratio, adding the components into another stirring kettle, and stirring for 10-20 min to form a mixture B; simultaneously adding the mixture A and the mixture B into a third stirring kettle, and stirring for 20-30 min to complete the preparation of the multivitamin, so as to obtain the multivitamin for later use;
step two, preparing the insecticidal additive: weighing marigold and chinaberry root respectively, crushing, putting into a flash extractor, adding 70-85% ethanol solution which is 5-12 times of that of the marigold and chinaberry root, performing flash extraction respectively, and filtering to obtain extract; ultrafiltering the extractive solution with ultrafiltration membrane, concentrating under reduced pressure, and drying to obtain crude extract; separating and purifying the crude extract by liquid chromatography, and collecting marigold and chinaberry root components respectively; vacuum concentrating marigold and cortex Meliae root respectively, crystallizing, filtering, washing, and drying to obtain marigold extractive solution and cortex Meliae root extractive solution; mixing flos Tagetis Erectae extract, cortex Meliae extract, flos Tagetis Erectae extract and cortex Meliae extract, and stirring to obtain pesticide additive;
step three, chelation reaction: weighing and matching the multivitamins prepared in the step one and the insecticidal additive prepared in the step two with glucose, sugar alcohol and amino-oligosaccharin according to the weight ratio of the formula, simultaneously adding the mixture into a chelation reaction kettle, and carrying out heating reaction and stirring; when the temperature of the reaction kettle reaches 40 ℃, carrying out constant temperature control, stirring for 20-30 min under the constant temperature state, and finishing the chelation reaction; the chelation reaction kettle is a closed kettle body, a heating jacket is arranged outside the kettle body, and a stirring paddle is arranged on the inner side of the kettle body;
regulating the temperature of the reaction kettle to 50 +/-5 ℃, sequentially adding urea, potassium sulfate, potassium dihydrogen phosphate, magnesium sulfate, ammonium sulfate, biochemical fulvic acid, compound sodium nitrophenolate, sodium naphthylacetate and sodium dodecyl benzene sulfonate, and stirring for 30-50 min; then adding an auxiliary agent to carry out pH value test; when the pH value is 6-8, completely inputting the product into a cooling tank, continuously stirring, cooling with water, and inputting the product into a storage tank after the temperature is reduced to room temperature;
step five, granulating and forming: uniformly distributing the product stored in the storage tank on a steel belt of a rotary belt type condensation granulator moving at a constant speed below the storage tank by a material pump and a material distributor; and (3) cooling and solidifying the product by a spraying device to form a particle finished product while the product moves on the steel belt, so that the multifunctional water-soluble fertilizer can be obtained.
Further, in the second step, the voltage of the flash extraction is 120-160V, and the extraction time is 60-120 s; the operating pressure of the ultrafiltration concentration is 0.5-2.5 MPa.
Further, in the third step, the constant temperature control includes:
the chelation reaction kettle is heated in an electric heating mode, and when the temperature of the chelation reaction kettle reaches the specified temperature, the temperature of the chelation reaction kettle is controlled by a thermostat.
Further, in the fourth step, the cooling includes: and (3) inputting the product into a cooling tank, and introducing refrigerating fluid into an interlayer of the cooling tank to perform cooling reaction until the temperature is room temperature.
Further, in the fifth step, the temperature of the inlet of the distributing device is controlled to be 80-120 ℃, the rotating speed of the steel belt is controlled to be 15-50 r/min, the temperature of the cooling water inlet of the spraying device is less than or equal to 40 ℃, the pressure of the cooling water inlet is 0.2-0.6 MPa, the pressure of the cooling water outlet is normal pressure, and the return water temperature is controlled to be 25-45 ℃.
The invention also aims to provide the multifunctional water-soluble fertilizer prepared by the preparation method of the multifunctional water-soluble fertilizer, which comprises 30-50 wt% of urea, 20-30 wt% of potassium sulfate, 20-30 wt% of organic matters, 10-20 wt% of monopotassium phosphate, 3-7 wt% of compound vitamins, 3-7 wt% of magnesium sulfate, 4-8 wt% of ammonium sulfate, 2-4 wt% of biochemical fulvic acid, 0.1-0.2 wt% of compound sodium nitrophenolate, 0.04-0.06 wt% of sodium naphthalene acetate, 0.3-0.5 wt% of sodium dodecyl benzene sulfonate, 0.2-0.5 wt% of additives and 0.01-0.03 wt% of insecticidal additives.
Further, the organic matter comprises, by weight, 10% -20% of amino-oligosaccharin, 40% -50% of sugar alcohol and 40% -50% of glucose.
Further, the compound vitamin comprises, by weight, 15% -25% of vitamin C, 115% -25% of vitamin B, 20.5% -6% of vitamin B, 615% -25% of vitamin B, 90.5% -6% of vitamin B, 120.5% -6% of vitamin B, 0.5% -6% of vitamin H, 0.5% -6% of pantothenic acid, 15% -25% of nicotinamide and 0.5% -6% of inositol.
Furthermore, the insecticidal additive comprises 40-50 wt% of marigold extract, 30-40 wt% of chinaberry root extract and 20-25 wt% of concentrated molasses.
Further, the auxiliary agent comprises 50-60% of penetrating agent and 50-60% of synergist by weight percentage; the penetrant is a wetting agent, and the synergist is one or a combination of yeast powder or yeast concentrated solution.
By combining all the technical schemes, the invention has the advantages and positive effects that: the multifunctional water-soluble fertilizer provided by the invention is easy to dissolve and absorb, the utilization rate is improved, and more importantly, the multifunctional water-soluble fertilizer can be applied to the fertilization requirement of spray and drip irrigation, and the integration of water and fertilizer is realized. The preparation of the water-soluble compound fertilizer has the characteristics of convenience, high efficiency, high quality and the like, and simultaneously has the characteristics of product diversification, crop resistance enhancement, crop growth and development promotion, comprehensive and balanced nutrition provision for the crop growth and development, soil physical property improvement and crop disease improvement caused by deficiency.
Meanwhile, the multifunctional water-soluble fertilizer provided by the invention is also added with an insecticidal additive, and the marigold extracting solution is combined with molasses so as to increase the reproduction of fungi for inhibiting root-knot nematodes; the melia azedarach extracting solution has insecticidal action, and the combination of the melia azedarach extracting solution and the melia azedarach extracting solution can effectively prevent and kill root-knot nematodes and promote root development.
The invention carries out scientific compatibility on a plurality of vitamins to form the compound vitamin, and overcomes the defects that a single vitamin is not easy to be absorbed by crops, and has slow absorption, slow effect and unobvious effect; the sugar alcohol, the glucose and the vitamins are organically combined, so that the activity of the vitamins can be maintained, and the absorption, utilization and conversion of the vitamins and other nutrients by crops are promoted; the vitamin C, the vitamin B6, the vitamin B12 and the nicotinamide are combined according to the weight ratio of 1: 1, so that the activity of the vitamin can be exerted to the maximum extent, the decomposition and transformation of soil organic matters are promoted, the dissolving capacity of crop nutrition in soil is improved, and the effectiveness is increased; the amino-oligosaccharin and the vitamin are organically combined, so that the growth of crops is promoted, the yield is increased, the crops can be induced to generate stress resistance, and the disease resistance, cold resistance and drought resistance of the crops are enhanced.
Compared with the prior art, the invention also has the following effects:
(1) the fertilizer and water of the invention are applied simultaneously, the absorption is fast, the effect is fast, the fertilizer contains the nutrient components necessary for the growth of crops, the mixture ratio is scientific;
(2) the soil structure is improved, and the nutrient absorption of crops is further promoted;
(3) the yield increasing effect is obvious, and the quality of crops is improved; by using the product, the disease resistance, cold resistance and drought resistance of crops are enhanced, the insect damage is less, the yield is high, the yield can be increased by more than 30 percent, and the economic crops can reach more than 50 percent.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings needed to be used in the embodiments of the present invention will be briefly described below, and it is obvious that the drawings described below are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to the drawings without creative efforts.
Fig. 1 is a flow chart of a multifunctional water-soluble fertilizer and a preparation method thereof provided by the embodiment of the invention.
FIG. 2 is a flow chart of a method for preparing a multivitamin composition provided by an embodiment of the present invention.
FIG. 3 is a flow chart of a method for preparing marigold extract according to an embodiment of the present invention.
FIG. 4 is a flow chart of a method for preparing an extract from the root of Melia azedarach according to an embodiment of the present invention.
FIG. 5 is a flow chart of a chelation reaction provided in an embodiment of the invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Aiming at the problems in the prior art, the invention provides a multifunctional water-soluble fertilizer and a preparation method thereof, and the invention is described in detail with reference to the accompanying drawings.
The multifunctional water-soluble fertilizer provided by the embodiment of the invention comprises, by weight, 30% -50% of urea, 20% -30% of potassium sulfate, 20% -30% of organic matters, 10% -20% of monopotassium phosphate, 3% -7% of compound vitamins, 3% -7% of magnesium sulfate, 4% -8% of ammonium sulfate, 2% -4% of biochemical fulvic acid, 0.1% -0.2% of compound sodium nitrophenolate, 0.04% -0.06% of sodium naphthalene acetate, 0.3% -0.5% of sodium dodecyl benzene sulfonate, 0.2% -0.5% of an auxiliary agent and 0.01% -0.03% of an insecticidal additive.
The organic matter provided by the embodiment of the invention comprises, by weight, 10% -20% of amino-oligosaccharide, 40% -50% of sugar alcohol and 40% -50% of glucose.
The compound vitamin provided by the embodiment of the invention comprises, by weight, 15% -25% of vitamin C, 115% -25% of vitamin B, 20.5% -6% of vitamin B, 615% -25% of vitamin B, 90.5% -6% of vitamin B, 120.5% -6% of vitamin B, 0.5% -6% of vitamin H, 0.5% -6% of pantothenic acid, 15% -25% of nicotinamide and 0.5% -6% of inositol.
The insecticidal additive provided by the embodiment of the invention comprises 40-50% of marigold extract, 30-40% of chinaberry root extract and 20-25% of concentrated molasses by weight percentage.
The auxiliary agent provided by the embodiment of the invention comprises 50-60% of penetrant and 50-60% of synergist by weight percentage; the penetrant is a wetting agent, and the synergist is one or a combination of yeast powder or yeast concentrated solution.
As shown in fig. 1, the preparation method of the multifunctional water-soluble fertilizer provided by the embodiment of the invention comprises the following steps:
s101, preparing compound vitamins: weighing vitamin C, vitamin B6, vitamin B12, nicotinamide, vitamin B1, vitamin B2, vitamin B9, vitamin H, pantothenic acid and inositol, mixing, adding into a stirring kettle, and preparing compound vitamin;
s102, preparing the insecticidal additive: respectively preparing marigold extract and chinaberry root extract, then mixing the marigold extract, the chinaberry root extract, the marigold extract and the chinaberry root extract, and stirring uniformly to obtain the insecticidal additive;
s103, chelating reaction: weighing and mixing the composite vitamin insecticidal additive, glucose, sugar alcohol and amino-oligosaccharin according to the weight proportion of the formula, and simultaneously adding the mixture into a chelation reaction kettle for chelation reaction;
s104, adjusting the temperature of the reaction kettle to 50 +/-5 ℃, sequentially adding urea, potassium sulfate, potassium dihydrogen phosphate, magnesium sulfate, ammonium sulfate, biochemical fulvic acid, compound sodium nitrophenolate, sodium naphthylacetate and sodium dodecyl benzene sulfonate, and stirring for 30-50 min; then adding an auxiliary agent to carry out pH value test;
s105, when the pH value is 6-8, inputting all the products into a cooling tank, continuously stirring, cooling with water, and inputting the products into a storage tank after the temperature is reduced to room temperature;
s106, granulating and forming: uniformly distributing the product stored in the storage tank on a steel belt of a rotary belt type condensation granulator moving at a constant speed below the storage tank by virtue of a material pump and a material distributor;
s107, while the product moves on the steel belt, the spraying device cools and solidifies the product to form a particle finished product, and the multifunctional water-soluble fertilizer can be obtained.
In step S105 provided in the embodiment of the present invention, the cooling includes: and (3) inputting the product into a cooling tank, and introducing refrigerating fluid into an interlayer of the cooling tank to perform cooling reaction until the temperature is room temperature.
In step S106 provided by the embodiment of the invention, the temperature of the inlet of the distributing device is controlled to be 80-120 ℃, the rotating speed of a steel belt is controlled to be 15-50 r/min, the temperature of the cooling water inlet of the spraying device is less than or equal to 40 ℃, the pressure of the cooling water inlet is 0.2-0.6 MPa, the pressure of the cooling water outlet is normal pressure, and the return water temperature is controlled to be 25-45 ℃.
As shown in fig. 2, in step S101, the preparation of the multivitamin includes:
s201, mixing vitamin C, vitamin B6, vitamin B12 and niacinamide according to a ratio of 1: 1: 1: 1, adding the mixture into a stirring kettle, and mixing and stirring for 10-20 min to form a mixture A;
s202, mixing vitamin B1, vitamin B2, vitamin B9, vitamin H, pantothenic acid and inositol in a ratio of 1: 1: 2: 3, weighing the components according to the weight ratio, adding the components into another stirring kettle, and stirring for 10-20 min to form a mixture B;
s203, simultaneously adding the mixture A and the mixture B into a third stirring kettle, and stirring for 20-30 min to complete the preparation of the multivitamin, so as to obtain the multivitamin for later use;
as shown in fig. 3, in step S102 provided in the embodiment of the present invention, the preparing of the marigold extracting solution includes:
s301, weighing marigold, crushing, putting into a flash extractor, adding 70-85% ethanol solution which is 5-12 times of the weight of the marigold, performing flash extraction, and filtering to obtain an extracting solution;
s302, performing ultrafiltration concentration on the extracting solution through an ultrafiltration membrane, and performing reduced pressure concentration and drying to obtain a crude extract; separating and purifying the crude extract by liquid chromatography, and collecting the marigold;
s303, carrying out vacuum concentration on the marigold components, separating out crystals, filtering, washing and drying to obtain the marigold extracting solution.
As shown in fig. 4, in step S102, the preparing of the neem root extracting solution according to the embodiment of the present invention includes:
s401, weighing chinaberry roots, crushing, putting into a flash extractor, adding 70-85% ethanol solution which is 5-12 times of the weight of the chinaberry roots, performing flash extraction, and filtering to obtain an extracting solution;
s402, performing ultrafiltration concentration on the extracting solution through an ultrafiltration membrane, and performing reduced pressure concentration and drying to obtain a crude extract; separating and purifying the crude extract by liquid chromatography, and collecting the component of the root of Melia azedarach;
s403, carrying out vacuum concentration on the chinaberry root component, separating out crystals, filtering, washing and drying to obtain the chinaberry root extract.
The voltage of flash extraction provided by the embodiment of the invention is 120-160V, and the extraction time is 60-120 s; the operating pressure of the ultrafiltration concentration is 0.5-2.5 MPa.
As shown in fig. 5, in step S103 provided in the embodiment of the present invention, the chelation reaction includes:
s501, weighing and matching the prepared compound vitamin and the prepared insecticidal additive with glucose, sugar alcohol and amino-oligosaccharin according to the weight proportion of the formula;
s502, adding the weighed and compatible raw materials into a chelation reaction kettle, carrying out heating reaction and stirring;
s503, when the temperature of the reaction kettle reaches 40 ℃, carrying out constant temperature control, stirring for 20-30 min under the constant temperature state, and finishing the chelation reaction.
The constant temperature control provided by the embodiment of the invention comprises the following steps: the chelation reaction kettle is heated in an electric heating mode, and when the temperature of the chelation reaction kettle reaches the specified temperature, the temperature of the chelation reaction kettle is controlled by a thermostat.
The chelation reaction kettle provided by the embodiment of the invention is a closed kettle body, a heating jacket is arranged outside the kettle body, and a stirring paddle is arranged on the inner side of the kettle body.
The above description is only for the purpose of illustrating the present invention and the appended claims are not to be construed as limiting the scope of the invention, which is intended to cover all modifications, equivalents and improvements that are within the spirit and scope of the invention as defined by the appended claims.
Claims (10)
1. The preparation method of the multifunctional water-soluble fertilizer is characterized by comprising the following steps:
step one, preparing compound vitamin: mixing vitamin C, vitamin B6, vitamin B12 and nicotinamide according to a ratio of 1: 1: 1: 1, adding the mixture into a stirring kettle, and mixing and stirring for 10-20 min to form a mixture A; meanwhile, vitamin B1, vitamin B2, vitamin B9, vitamin H, pantothenic acid and inositol were mixed in a ratio of 1: 1: 2: 3, weighing the components according to the weight ratio, adding the components into another stirring kettle, and stirring for 10-20 min to form a mixture B; simultaneously adding the mixture A and the mixture B into a third stirring kettle, and stirring for 20-30 min to complete the preparation of the multivitamin, so as to obtain the multivitamin for later use;
step two, preparation of the insecticidal additive: weighing marigold and chinaberry root respectively, crushing, putting into a flash extractor, adding 70-85% ethanol solution which is 5-12 times of that of the marigold and chinaberry root, performing flash extraction respectively, and filtering to obtain extract; ultrafiltering the extractive solution with ultrafiltration membrane, concentrating under reduced pressure, and drying to obtain crude extract; separating and purifying the crude extract by liquid chromatography, and collecting marigold and chinaberry root components respectively; vacuum concentrating marigold and cortex Meliae root respectively, crystallizing, filtering, washing, and drying to obtain marigold extractive solution and cortex Meliae root extractive solution; mixing flos Tagetis Erectae extract, cortex Meliae extract, flos Tagetis Erectae extract and cortex Meliae extract, and stirring to obtain pesticide additive;
step three, chelation reaction: weighing and matching the multivitamins prepared in the step one and the insecticidal additive prepared in the step two with glucose, sugar alcohol and amino-oligosaccharin according to the weight ratio of the formula, simultaneously adding the mixture into a chelation reaction kettle, and carrying out heating reaction and stirring; when the temperature of the reaction kettle reaches 40 ℃, carrying out constant temperature control, stirring for 20-30 min under the constant temperature state, and finishing the chelation reaction; the chelation reaction kettle is a closed kettle body, a heating jacket is arranged outside the kettle body, and a stirring paddle is arranged on the inner side of the kettle body;
regulating the temperature of the reaction kettle to 50 +/-5 ℃, sequentially adding urea, potassium sulfate, potassium dihydrogen phosphate, magnesium sulfate, ammonium sulfate, biochemical fulvic acid, compound sodium nitrophenolate, sodium naphthylacetate and sodium dodecyl benzene sulfonate, and stirring for 30-50 min; then adding an auxiliary agent to carry out pH value test; when the pH value is 6-8, completely inputting the product into a cooling tank, continuously stirring, cooling with water, and inputting the product into a storage tank after the temperature is reduced to room temperature;
step five, granulating and forming: uniformly distributing the product stored in the storage tank on a steel belt of a rotary belt type condensation granulator moving at a constant speed below the storage tank by a material pump and a material distributor; and (3) cooling and solidifying the product by a spraying device to form a particle finished product while the product moves on the steel belt, so as to obtain the multifunctional water-soluble fertilizer.
2. The preparation method of the multifunctional water-soluble fertilizer as claimed in claim 1, wherein in the second step, the voltage of flash extraction is 120-160V, and the extraction time is 60-120 s; the operating pressure of the ultrafiltration concentration is 0.5-2.5 MPa.
3. The preparation method of the multifunctional water-soluble fertilizer as claimed in claim 1, wherein in the third step, the constant temperature control comprises the following steps:
the chelation reaction kettle is heated in an electric heating mode, and when the temperature of the chelation reaction kettle reaches the specified temperature, the temperature of the chelation reaction kettle is controlled by a thermostat.
4. The preparation method of the multifunctional water-soluble fertilizer as claimed in claim 1, wherein in the fourth step, the cooling comprises the following steps: and (3) inputting the product into a cooling tank, and introducing refrigerating fluid into an interlayer of the cooling tank to perform cooling reaction until the temperature is room temperature.
5. The preparation method of the multifunctional water-soluble fertilizer as claimed in claim 1, wherein in the fifth step, the temperature of the inlet of the distributor is controlled to be 80-120 ℃, the rotating speed of the steel belt is controlled to be 15-50 r/min, the temperature of the cooling water inlet of the spraying device is less than or equal to 40 ℃, the pressure of the cooling water inlet is 0.2-0.6 MPa, the pressure of the cooling water outlet is normal pressure, and the temperature of the return water is controlled to be 25-45 ℃.
6. The multifunctional water-soluble fertilizer prepared by the preparation method of the multifunctional water-soluble fertilizer as claimed in any one of claims 1 to 5, which is characterized by comprising, by weight, 30-50% of urea, 20-30% of potassium sulfate, 20-30% of organic matters, 10-20% of potassium dihydrogen phosphate, 3-7% of vitamin complex, 3-7% of magnesium sulfate, 4-8% of ammonium sulfate, 2-4% of biochemical fulvic acid, 0.1-0.2% of compound sodium nitrophenolate, 0.04-0.06% of sodium naphthalene acetate, 0.3-0.5% of sodium dodecyl benzene sulfonate, 0.2-0.5% of auxiliaries and 0.01-0.03% of insecticidal additives.
7. The multifunctional water-soluble fertilizer as claimed in claim 6, wherein the organic matter comprises, by weight, 10% -20% of amino-oligosaccharin, 40% -50% of sugar alcohol and 40% -50% of glucose.
8. The multifunctional water-soluble fertilizer as claimed in claim 6, wherein the vitamin complex comprises, by weight, 15% -25% of vitamin C, 115% -25% of vitamin B, 20.5% -6% of vitamin B, 615% -25% of vitamin B, 90.5% -6% of vitamin B, 120.5% -6% of vitamin B, 0.5% -6% of vitamin H, 0.5% -6% of pantothenic acid, 15% -25% of nicotinamide and 0.5% -6% of inositol.
9. The multifunctional water-soluble fertilizer as claimed in claim 6, wherein the insecticidal additive comprises 40-50% by weight of marigold extract, 30-40% by weight of chinaberry root extract and 20-25% by weight of concentrated molasses.
10. The multifunctional water-soluble fertilizer as claimed in claim 6, wherein the auxiliary agent comprises 50-60% by weight of penetrant and 50-60% by weight of synergist; the penetrant is a wetting agent, and the synergist is one or a combination of yeast powder or yeast concentrated solution.
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| CN105315063A (en) * | 2014-08-19 | 2016-02-10 | 杨凌德尔生物科技有限公司 | Vitamin multifunctional water-soluble fertilizer |
| CN106106544A (en) * | 2016-06-27 | 2016-11-16 | 武汉维斯康生物科技有限公司 | The water-soluble fertilizer insecticidal additive of Citrus root-knot nematode, water-soluble fertilizer and preparation method thereof and using method can be killed |
| CN109258726A (en) * | 2018-09-29 | 2019-01-25 | 绩溪农华生物科技有限公司 | A kind of Pesticide with Chinese medicinal material and preparation method thereof |
| CN109336694A (en) * | 2018-12-04 | 2019-02-15 | 徐州聚友信息技术有限公司 | A kind of a great number of elements Water soluble fertilizer and preparation method thereof |
| CN112876312A (en) * | 2021-04-09 | 2021-06-01 | 杨粉莉 | Multifunctional water-soluble fertilizer and preparation method thereof |
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2022
- 2022-06-22 CN CN202210709636.8A patent/CN115028495A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105315063A (en) * | 2014-08-19 | 2016-02-10 | 杨凌德尔生物科技有限公司 | Vitamin multifunctional water-soluble fertilizer |
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| CN109258726A (en) * | 2018-09-29 | 2019-01-25 | 绩溪农华生物科技有限公司 | A kind of Pesticide with Chinese medicinal material and preparation method thereof |
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| CN112876312A (en) * | 2021-04-09 | 2021-06-01 | 杨粉莉 | Multifunctional water-soluble fertilizer and preparation method thereof |
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Application publication date: 20220909 |