CN114982791A - Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof - Google Patents
Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof Download PDFInfo
- Publication number
- CN114982791A CN114982791A CN202210484139.2A CN202210484139A CN114982791A CN 114982791 A CN114982791 A CN 114982791A CN 202210484139 A CN202210484139 A CN 202210484139A CN 114982791 A CN114982791 A CN 114982791A
- Authority
- CN
- China
- Prior art keywords
- stirring
- reactor
- green
- agent
- free biological
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000607479 Yersinia pestis Species 0.000 title claims abstract description 29
- 241000238631 Hexapoda Species 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 35
- 240000002234 Allium sativum Species 0.000 claims abstract description 30
- 235000004611 garlic Nutrition 0.000 claims abstract description 30
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 24
- 239000000843 powder Substances 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 21
- 239000003755 preservative agent Substances 0.000 claims abstract description 21
- 230000002335 preservative effect Effects 0.000 claims abstract description 21
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 19
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 19
- 238000001816 cooling Methods 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 239000003349 gelling agent Substances 0.000 claims abstract description 9
- 238000009924 canning Methods 0.000 claims abstract description 7
- 238000007599 discharging Methods 0.000 claims abstract description 7
- 239000011259 mixed solution Substances 0.000 claims abstract description 7
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 12
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 8
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims description 6
- 239000004330 calcium propionate Substances 0.000 claims description 6
- 235000010331 calcium propionate Nutrition 0.000 claims description 6
- 239000000679 carrageenan Substances 0.000 claims description 6
- 229940113118 carrageenan Drugs 0.000 claims description 6
- 229920001525 carrageenan Polymers 0.000 claims description 6
- 239000001103 potassium chloride Substances 0.000 claims description 6
- 235000011164 potassium chloride Nutrition 0.000 claims description 6
- 229920002545 silicone oil Polymers 0.000 claims description 6
- 229920002752 Konjac Polymers 0.000 claims description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 5
- 239000000252 konjac Substances 0.000 claims description 5
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 5
- 229920000053 polysorbate 80 Polymers 0.000 claims description 5
- 230000001846 repelling effect Effects 0.000 claims description 5
- 239000005711 Benzoic acid Substances 0.000 claims description 4
- 239000004283 Sodium sorbate Substances 0.000 claims description 4
- 235000010233 benzoic acid Nutrition 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- LROWVYNUWKVTCU-STWYSWDKSA-M sodium sorbate Chemical compound [Na+].C\C=C\C=C\C([O-])=O LROWVYNUWKVTCU-STWYSWDKSA-M 0.000 claims description 4
- 235000019250 sodium sorbate Nutrition 0.000 claims description 4
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims description 3
- 235000010199 sorbic acid Nutrition 0.000 claims description 3
- 239000004334 sorbic acid Substances 0.000 claims description 3
- 229940075582 sorbic acid Drugs 0.000 claims description 3
- QHZLMUACJMDIAE-UHFFFAOYSA-N 1-monopalmitoylglycerol Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(O)CO QHZLMUACJMDIAE-UHFFFAOYSA-N 0.000 claims description 2
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 2
- 235000021355 Stearic acid Nutrition 0.000 claims description 2
- 235000010418 carrageenan Nutrition 0.000 claims description 2
- 229940096898 glyceryl palmitate Drugs 0.000 claims description 2
- 235000019823 konjac gum Nutrition 0.000 claims description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 2
- 235000010241 potassium sorbate Nutrition 0.000 claims description 2
- 239000004302 potassium sorbate Substances 0.000 claims description 2
- 229940069338 potassium sorbate Drugs 0.000 claims description 2
- 239000008117 stearic acid Substances 0.000 claims description 2
- 238000013268 sustained release Methods 0.000 claims description 2
- 239000012730 sustained-release form Substances 0.000 claims description 2
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 2
- 238000009472 formulation Methods 0.000 claims 6
- 238000013270 controlled release Methods 0.000 claims 4
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 239000000499 gel Substances 0.000 description 14
- 239000000796 flavoring agent Substances 0.000 description 12
- 235000019634 flavors Nutrition 0.000 description 12
- 241000255925 Diptera Species 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000000575 pesticide Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- 239000002386 air freshener Substances 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 239000000686 essence Substances 0.000 description 5
- 239000000341 volatile oil Substances 0.000 description 5
- 230000006378 damage Effects 0.000 description 4
- 239000000645 desinfectant Substances 0.000 description 4
- 235000015110 jellies Nutrition 0.000 description 4
- 239000008274 jelly Substances 0.000 description 4
- 244000247812 Amorphophallus rivieri Species 0.000 description 3
- 235000001206 Amorphophallus rivieri Nutrition 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 3
- 239000002781 deodorant agent Substances 0.000 description 3
- 235000010485 konjac Nutrition 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 231100000331 toxic Toxicity 0.000 description 3
- 230000002588 toxic effect Effects 0.000 description 3
- OYPRJOBELJOOCE-IGMARMGPSA-N Calcium-40 Chemical compound [40Ca] OYPRJOBELJOOCE-IGMARMGPSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 241000255777 Lepidoptera Species 0.000 description 2
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 description 2
- MCFVRESNTICQSJ-RJNTXXOISA-L calcium sorbate Chemical compound [Ca+2].C\C=C\C=C\C([O-])=O.C\C=C\C=C\C([O-])=O MCFVRESNTICQSJ-RJNTXXOISA-L 0.000 description 2
- 235000010244 calcium sorbate Nutrition 0.000 description 2
- 239000004303 calcium sorbate Substances 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 239000002341 toxic gas Substances 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- 206010067484 Adverse reaction Diseases 0.000 description 1
- 201000002045 Ancylostomiasis Diseases 0.000 description 1
- 208000033211 Ankylostomiasis Diseases 0.000 description 1
- 241000271566 Aves Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241001674044 Blattodea Species 0.000 description 1
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 1
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010016952 Food poisoning Diseases 0.000 description 1
- 208000019331 Foodborne disease Diseases 0.000 description 1
- 244000303040 Glycyrrhiza glabra Species 0.000 description 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 description 1
- 235000017443 Hedysarum boreale Nutrition 0.000 description 1
- 235000007858 Hedysarum occidentale Nutrition 0.000 description 1
- 241000545744 Hirudinea Species 0.000 description 1
- 206010020376 Hookworm infection Diseases 0.000 description 1
- 208000019637 Infantile Diarrhea Diseases 0.000 description 1
- 240000003553 Leptospermum scoparium Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 241000699666 Mus <mouse, genus> Species 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 229920001214 Polysorbate 60 Polymers 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 235000017803 cinnamon Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000013530 defoamer Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000001784 detoxification Methods 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 206010014881 enterobiasis Diseases 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 229940075507 glyceryl monostearate Drugs 0.000 description 1
- 239000001947 glycyrrhiza glabra rhizome/root Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 235000021579 juice concentrates Nutrition 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000000447 pesticide residue Substances 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P17/00—Pest repellants
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Chemical & Material Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Toxicology (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a green pollution-free biological slow release agent for expelling insect pests and a preparation method thereof. The biological slow release agent comprises gel powder, a preservative, a defoaming agent, an emulsifier, garlic concentrated juice and water. The preparation method comprises the following steps: adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 10-20 minutes, and uniformly dispersing; heating the reactor to 80-95 ℃, stopping heating and preserving heat, maintaining stirring for 10-30 minutes, and then cooling to 70-80 ℃; adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly; naturally cooling the reactor to 50-70 deg.C, stirring while maintaining the temperature, discharging, and canning. The invention uses the garlic concentrated juice to replace essence to produce a nontoxic, harmless, green and nuisanceless biological slow release agent for expelling insect pests, which has low price and the use time of about 45 days.
Description
Technical Field
The invention relates to a green pollution-free biological slow release agent for expelling insect pests and a preparation method thereof, belonging to the technical field of organic agriculture.
Background
Aiming at the prevention and control of agricultural diseases and pests, the prior art mainly takes pesticide prevention and control as a main part, is popular among farmers due to quick effect, obvious effect and income increase, but has particularly prominent side effect. The pesticide mainly kills pests in the aspect of preventing and controlling pests, and the pesticide by-product slightly treated can remain over standard to cause food poisoning; even if a trace amount of highly toxic pesticide is ingested, the highly toxic pesticide can cause diarrhea, vomiting, dizziness and the like of people and even seriously threaten the life safety of people; the excessive use of the pesticide can also cause damage to the ecological environment to a certain extent.
In addition, for a long time, the animal husbandry is also often plagued by pests which are not seen by people, such as mice, cockroaches, mosquitoes, flies, butterflies and the like. At present, mosquito incense, mouse traps, fly lamps and other modes are mostly used for preventing and controlling the pests, but the instant effect is lacked, for example, poor quality mosquito incense used for animals can generate toxic gases such as formaldehyde, acetaldehyde, benzene, polycyclic aromatic hydrocarbon and the like when being burnt, and human bodies can be poisoned and pathogenic if being in the environment for a long time, so that the health of the human bodies is injured.
The air fresheners sold in the market at present are mainly composed of volatile ethanol, essence, deionized water and other components, can cover or lighten uncomfortable feelings of people on environmental peculiar smell through the emitted faint scent, and are divided into three forms, namely solid, liquid and gas. Solid air fresheners, which were first introduced in the early 70 foreign countries, were used primarily in automobiles, home bedrooms or living rooms, hotels and restaurants, and other public places of entertainment. The basic preparation principle of the product is as follows: the essence, the deodorant and the disinfectant are mixed with the components of water, the thickening agent, the preservative, the emulsifier and the like, the water and the thickening agent form a solid jelly, the solid jelly contains the essence, the deodorant and the disinfectant, and when the solid jelly is placed in the air, the volume is slowly reduced along with the volatilization of water in the solid jelly, and the essence, the deodorant and the disinfectant are slowly diffused into the air, so that the aim of making the air fragrant and fresh is fulfilled.
In daily life, garlic is used as an edible seasoning, and has remarkable application in aspects of life, production and disease treatment, such as clinically mainly treating ancylostomiasis and enterobiasis; in ancient times, garlic is pounded and externally applied to the soles of two feet to treat infantile diarrhea and dysentery; the theory of garlic detoxification and the efficacy of expelling parasites are also introduced in rural areas. Peasants are puzzled by leeches and mosquitoes deeply when going to the field, because the garlic concentrated juice can emit unpleasant and strong garlic flavor, various pests can not avoid the pest in time, clever workers smash the garlic and mix with some clear water, and the clear water containing the garlic flavor has obvious insect expelling effect when being coated on the whole body.
The research on air fresheners at home and abroad is more specific, but generally belongs to the field of improving air quality in family toilets and other occasions, and the research on products for replacing highly toxic pesticides to drive insect pests in modern organic agriculture is rare. For example, patent document CN111643705A discloses an essential oil composition and its application in preparing air freshener, in which an essential oil composition composed of cinnamon essential oil, tea tree essential oil, and licorice root essential oil is added with tween and hydrogenated castor oil. The air freshener adopts natural plant sources, cannot damage the environment, and has biological activities of antibiosis, antioxidation, disinsection, mosquito repelling and the like, but the method has the defects of difficult extraction of spice, high production cost, poor scale applicability, fast fragrance exertion speed, no durability, limited application and the like.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: provides a nontoxic and harmless biological slow release agent for expelling pests, which is used for producing pollution-free high-quality agricultural products in modern organic agriculture.
In order to solve the technical problems, the invention adopts the following technical scheme:
a green pollution-free biological slow release agent for expelling insect pests comprises 1-3% of gel agent powder, 0.01-0.2% of preservative, 0.01-0.2% of defoaming agent and the balance of water by mass percent, and also comprises 0.5-3% of emulsifier and 1-5% of garlic concentrated juice by volume after all the raw materials are mixed.
Preferably, the gelling agent powder comprises at least one of carrageenan, konjac gum and potassium chloride.
Preferably, the preservative comprises at least one of sorbic acid, potassium sorbate, sodium sorbate, calcium propionate, benzoic acid.
Preferably, the defoamer comprises at least one of calcium carbonate and silicone oil.
Preferably, the emulsifier comprises at least one of tween-80, glyceryl palmitate, and monostearate.
Preferably, the biological slow release agent is in the form of solid gel.
The invention also provides a preparation method of the green pollution-free biological slow release agent for expelling pests, which comprises the following steps:
step 1): adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 10-20 minutes, and uniformly dispersing;
step 2): heating the reactor to 80-95 ℃, stopping heating and preserving heat, maintaining stirring for 10-30 minutes, and then cooling to 70-80 ℃;
step 3): adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly;
step 4): naturally cooling the reactor to 50-70 deg.C, stirring while maintaining the temperature, discharging, and canning.
The invention uses the garlic concentrated juice to replace essence to produce a nontoxic, harmless, green and nuisanceless biological slow release agent for expelling insect pests, which has low price and the use time of about 45 days.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention has low cost, wide raw material source and low price. The garlic is planted all over the country and is an important crop product, the sources of the garlic widely realize the universality of the production of the invention, and the garlic can be produced in all places. The production process provided by the invention is simple and easy to implement, has stronger universality no matter household production or factory large-scale production, has no limit to raw materials, and does not exclude the use of other various spices to replace garlic concentrated juice so as to achieve the purpose of removing insect pests;
2. the natural garlic concentrated juice is adopted as the raw material, so that the environment and the ecological system are not damaged, the aim of green and healthy life is effectively fulfilled, no pesticide residue is generated, no toxic gases such as formaldehyde, acetaldehyde, benzene and polycyclic aromatic hydrocarbon are generated, no harm is caused to human bodies, and the action mechanism is that the smell expels various pests;
3. the invention solves the practical problems of the farming and animal husbandry industry and purposefully solves the problems of birds, mosquitoes, butterflies and the like, the product coverage range of the invention is wide, and the effective insect expelling range of a solid crude drug insect pest expelling slow-release agent is 30-50m 2 In addition, the product can be used as a solid release retardant in a gel mode, has strong durability, and generally lasts for about 45 days;
4. the product of the invention has certain sterilization capability, does not need to add disinfectant components like other air fresheners, has low pollution rate in the production process, has simple and mature process, is suitable for batch production, is safe and controllable in the production process, and can quickly form scale effect.
Detailed Description
In order to make the invention more comprehensible, preferred embodiments are described in detail below.
Example 1
A green pollution-free biological slow release agent for expelling pests comprises 1.2 percent of gel agent powder, 0.15 percent of preservative, 0.05 percent of defoaming agent, 98.6 percent of water, 2 percent of emulsifier and 3 percent of garlic concentrated juice according to the volume after all the raw materials are mixed.
The preparation method comprises the following steps:
step 1): adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 20 minutes, and uniformly dispersing;
step 2): heating the reactor to 90 ℃, stopping heating, keeping the temperature, maintaining stirring for 20 minutes, and then cooling to 75 ℃;
step 3): adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly;
step 4): naturally cooling the reactor to 55 ℃, preserving heat, stirring, discharging and canning.
The gel comprises 40% of konjac powder, 50% of K-carrageenan powder and 10% of potassium chloride in percentage by mass.
The defoaming agent comprises 75% of calcium carbonate and 25% of silicone oil in percentage by mass.
The preservative comprises 10% of sodium sorbate, 50% of calcium propionate and 40% of calcium sorbate in percentage by mass.
The emulsifier is tween-80.
Example 2
A green pollution-free biological slow release agent for expelling pests comprises 2.5% of gel agent powder, 0.1% of preservative, 0.05% of defoaming agent, 97.35% of water, 0.5% of emulsifier and 3% of garlic concentrated juice according to the volume after all the raw materials are mixed.
The preparation method comprises the following steps:
step 1): adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 20 minutes, and uniformly dispersing;
step 2): heating the reactor to 95 ℃, stopping heating, keeping the temperature, keeping stirring for 15 minutes, and then cooling to 70 ℃;
step 3): adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly;
step 4): naturally cooling the reactor to 60 ℃, preserving heat, stirring, discharging and canning.
The gel comprises 40% of konjac powder, 50% of K-carrageenan powder and 10% of potassium chloride in percentage by mass.
The defoaming agent is 100% silicone oil.
The preservative comprises 25% of sorbic acid and 75% of calcium propionate in percentage by mass.
The emulsifier comprises 40% of tween-80 and 60% of stearic acid in percentage by mass.
Example 3
A green pollution-free biological slow release agent for expelling pests comprises 2% of gel agent powder, 0.05% of preservative, 0.05% of defoaming agent, 97.9% of water, 1.2% of emulsifier and 4% of garlic concentrated juice by volume after all the raw materials are mixed.
The preparation method comprises the following steps:
step 1): adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 10 minutes, and uniformly dispersing;
step 2): heating the reactor to 95 ℃, stopping heating, keeping the temperature, maintaining stirring for 10 minutes, and then cooling to 75 ℃;
step 3): adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly;
step 4): naturally cooling the reactor to 70 ℃, preserving heat, stirring, discharging and canning.
The gel comprises 85 percent of K-carrageenan refined powder and 15 percent of potassium chloride by mass percentage.
The defoaming agent comprises 50% of silicone oil and 50% of calcium carbonate in percentage by mass.
The preservative comprises 30% of calcium sorbate, 30% of calcium propionate and 40% of benzoic acid in percentage by mass.
The emulsifier is tween-80.
Example 4
A green pollution-free biological slow release agent for expelling pests comprises 3% of gel agent powder, 0.02% of preservative, 0.2% of defoaming agent, 96.78% of water, 2.5% of emulsifier and 4.8% of garlic concentrated juice according to the volume percentage after all the raw materials are mixed.
The preparation method comprises the following steps:
step 1): adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 10 minutes, and uniformly dispersing;
step 2): heating the reactor to 95 ℃, stopping heating, keeping the temperature, maintaining stirring for 10 minutes, and then cooling to 75 ℃;
step 3): adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly;
step 4): naturally cooling the reactor to 70 ℃, preserving heat, stirring, discharging and canning.
The gel comprises 10% of konjac powder, 75% of K-carrageenan powder and 15% of potassium chloride in percentage by mass.
The defoaming agent comprises 80% of silicone oil and 20% of calcium carbonate in percentage by mass.
The preservative comprises 20% of sodium sorbate, 50% of calcium propionate and 30% of benzoic acid in percentage by mass.
The emulsifier is palmitic glyceride.
Comparative example
A sustained-release agent for controlling insect pests of crude drug without toxicity, harm, greenness and public nuisance is prepared by the same method as in example 1 except that the raw material does not contain garlic juice concentrate.
Water loss test
TABLE 2
| 5d | 10d | 20d | 30d | 40d | 50d | 60d | |
| Example 1 | 3.52％ | 6.72％ | 10.25％ | 14.41％ | 25.42％ | 38.70％ | 50.22％ |
| Example 2 | 2.48％ | 5.59％ | 10.03％ | 15.87％ | 24.33％ | 34.63％ | 43.71％ |
| Example 3 | 1.44％ | 4.24％ | 8.68％ | 13.94％ | 27.48％ | 36.16％ | 48.20％ |
| Example 4 | 4.03％ | 7.15％ | 12.74％ | 16.78％ | 28.37％ | 39.24％ | 47.77％ |
| Comparative example | 3.25％ | 8.25％ | 13.52％ | 18.72％ | 32.74％ | 45.63％ | 59.26％ |
Odor, bacteriostasis and insect expelling test
20 volunteers were searched and divided into 5 groups, each group was responsible for olfactory observation of each example and comparative example, the investigation time was 60 days, the volunteers were required to be sensitive to odor without adverse reaction of garlic, and objective evaluation was given to odor. The evaluation is divided into five categories, namely, heavy, light, very light and slightly inaudible. And (5) visually checking the bacteria growing condition on the surface of the gel. The gel is placed in a farmland, and the number of mosquitoes in the gel range is regularly observed. The results of the experiment are shown in table 2.
TABLE 2
| 5d | 10d | 20d | 30d | 40d | 50d | 60d | |
| Example 1 | Rich in flavor | Rich in flavor | Is relatively rich | Is relatively rich | Is relatively light | Is relatively light | Very light |
| Example 2 | Rich in flavor | Rich in flavor | Is relatively rich | Is relatively rich | Is relatively light | Is relatively light | Very light |
| Example 3 | Rich in flavor | Rich in flavor | Rich in flavor | Is relatively rich | Is relatively rich | Is relatively light | Is relatively light |
| Example 4 | Rich in flavor | Rich in flavor | Rich in flavor | Is relatively rich | Is relatively rich | Is relatively light | Is relatively light |
| Comparative example | Slightly smelling | Slightly smelling | Slightly smelling | Slightly smelling | Slightly smelling | Has peculiar smell | Has peculiar smell |
The comparative example showed growth after 40 days, and examples 1 to 4 showed no growth. Example 40 days later, a certain concentration of odor release was maintained. Examples 1 to 4 all had very strong insect repelling ability, and the corresponding water loss rate was slightly higher than that in the water loss test, about 10%, and it was judged that the effect of natural wind was exerted, and examples 1 to 4 all had the effect of reducing mosquitoes compared to the comparative examples.
Claims (7)
1. A green pollution-free biological slow release agent for expelling pests is characterized by comprising 1-3% of gel agent powder, 0.01-0.2% of preservative, 0.01-0.2% of defoaming agent and the balance of water by mass percent, and further comprising 0.5-3% of emulsifier and 1-5% of garlic concentrated juice by volume after all the raw materials are mixed.
2. The green pollution-free biological slow-release agent for repelling insects according to claim 1, wherein the gelling agent powder comprises at least one of carrageenan, konjac gum and potassium chloride.
3. The green nuisance-free biological controlled-release formulation for combating insect pests of claim 1, wherein said preservative comprises at least one of sorbic acid, potassium sorbate, sodium sorbate, calcium propionate, benzoic acid.
4. The green nuisance-free biological controlled-release formulation for controlling insect pests according to claim 1, wherein the antifoaming agent comprises at least one of calcium carbonate and silicone oil.
5. The green pollution-free biological slow-release formulation for repelling insects according to claim 1, wherein the emulsifier comprises at least one of tween-80, glyceryl palmitate and stearic acid.
6. The green nuisance-free biological controlled-release formulation for repelling insects of claim 1 wherein said biological controlled-release formulation is in the form of a solid gel.
7. The method for preparing a green nuisance-free biological sustained-release formulation for controlling insect pests according to any one of claims 1 to 6, comprising the steps of:
step 1): adding water into a reactor, adding the gelling agent powder under the stirring condition, stirring for 10-20 minutes, and uniformly dispersing;
step 2): heating the reactor to 80-95 ℃, stopping heating and preserving heat, maintaining stirring for 10-30 minutes, and then cooling to 70-80 ℃;
step 3): adding a defoaming agent and a preservative into a reactor, simultaneously adding a mixed solution of the garlic concentrated juice and an emulsifier, and stirring uniformly;
step 4): naturally cooling the reactor to 50-70 deg.C, stirring while maintaining the temperature, discharging, and canning.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210484139.2A CN114982791A (en) | 2022-05-06 | 2022-05-06 | Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210484139.2A CN114982791A (en) | 2022-05-06 | 2022-05-06 | Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114982791A true CN114982791A (en) | 2022-09-02 |
Family
ID=83025511
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210484139.2A Pending CN114982791A (en) | 2022-05-06 | 2022-05-06 | Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114982791A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115643919A (en) * | 2022-10-27 | 2023-01-31 | 东盛生态科技股份有限公司 | Method for quickly forming silk-cotton wood grafted golden sun-silk-cotton wood and Qiu Zi silk-cotton wood |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102334520A (en) * | 2010-07-18 | 2012-02-01 | 招远市天星塑料制品厂 | Mosquito repellent liquid and preparation method thereof |
| CN106668923A (en) * | 2017-03-29 | 2017-05-17 | 武汉朗克环境科技有限公司 | Mosquito repellent odor-removing agent and preparation method thereof |
-
2022
- 2022-05-06 CN CN202210484139.2A patent/CN114982791A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102334520A (en) * | 2010-07-18 | 2012-02-01 | 招远市天星塑料制品厂 | Mosquito repellent liquid and preparation method thereof |
| CN106668923A (en) * | 2017-03-29 | 2017-05-17 | 武汉朗克环境科技有限公司 | Mosquito repellent odor-removing agent and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115643919A (en) * | 2022-10-27 | 2023-01-31 | 东盛生态科技股份有限公司 | Method for quickly forming silk-cotton wood grafted golden sun-silk-cotton wood and Qiu Zi silk-cotton wood |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103739408A (en) | Biogas slurry composite pesticide for preventing and treating cotton bollworm | |
| CN114982791A (en) | Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof | |
| CN107873701A (en) | A kind of aerosol for expelling parasite, sterilizing and mite killing and preparation method thereof | |
| CN106726871A (en) | Sweet wormwood mosquito-expelling and antipruritic floral water and preparation method thereof | |
| CN103772066A (en) | Biogas slurry composite pesticide for preventing and controlling stem borers | |
| KR101954909B1 (en) | Natural pest control composition using vegetable oils and manufacturing method thereof | |
| CN109221108B (en) | Fumigation composition and application thereof in prevention and control of straw mushroom pests | |
| KR102374312B1 (en) | Eco-friendly snake repellant | |
| CN113749130B (en) | Sugarcane organism seed stem coating agent and preparation method thereof | |
| CN112219844B (en) | Botanical mosquito repellent and preparation method thereof | |
| CN1153599A (en) | Plant pesticide | |
| KR101761471B1 (en) | Vegetable oil mixture with excellent anti-insect and deodorization | |
| KR100512871B1 (en) | Agent for expelling noxious insects and worms and toilet paper produced using the agent | |
| KR20110009321A (en) | Insecticidal vegeteble composition | |
| CN111011401A (en) | Mosquito killing medicament and preparation process thereof | |
| CN1158927C (en) | Prepn. of incense used as herbal mosquito repelling agent | |
| CN1045047C (en) | Pesticide No.1 for plant, and prodn. method therefor | |
| CN111264570B (en) | Plant mosquito-repellent incense and preparation method thereof | |
| CN103755471A (en) | Biogas slurry compound bactericide for preventing and treating leaf mold | |
| CN113598184B (en) | Solid bait capable of preventing and treating solenopsis invicta | |
| CN115474608B (en) | Composition for controlling Wuta-tsai diseases and application thereof | |
| KR100753964B1 (en) | Smoke-insecticide using the mixture composition of natural oil | |
| CN114903058A (en) | Electric mosquito repellent liquid and preparation method thereof | |
| KR20090102378A (en) | Natural germicide for mugwort and method of manufacturing thereof | |
| CN113519515A (en) | Rat repelling and odor removing incense composition, preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Deng Nianxiang Inventor after: Xiao Zhihao Inventor after: Chen Xiaoli Inventor after: Zhou Jixing Inventor before: Xiao Zhihao Inventor before: Deng Nianxiang Inventor before: Chen Xiaoli Inventor before: Zhou Jixing |
|
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20220902 |