CN114948828A - Whole-plant anhydrous lip glaze and preparation method thereof - Google Patents
Whole-plant anhydrous lip glaze and preparation method thereof Download PDFInfo
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- CN114948828A CN114948828A CN202210534648.1A CN202210534648A CN114948828A CN 114948828 A CN114948828 A CN 114948828A CN 202210534648 A CN202210534648 A CN 202210534648A CN 114948828 A CN114948828 A CN 114948828A
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Abstract
The application discloses a full-plant anhydrous lip glaze and a preparation method thereof. The whole-plant anhydrous lip glaze provided by the application comprises the following components in percentage by weight: vegetable oil and fat: 40% -60%, vegetable wax: 0.1-5%, plant powder: 10% -30%, plant dispersant: 10% -30%, plant antioxidant: 0.1% -1%, plant preservative: 0.1% -1%, plant essential oil: 0.1% -1%, plant extract: 0.1 to 1 percent. The application provides a full-plant anhydrous lip glaze, the texture is fine and smooth, the color is even, possesses good moisturizing and moistening effect, and anticorrosive, anti-inflammatory performance is strong, and the security is high. In addition, the preparation method of the all-plant anhydrous lip glaze provided by the application is simple in process, short in time consumption, low in equipment requirement, well compatible with the existing process and extremely high in large-scale application potential.
Description
Technical Field
The application belongs to the technical field of daily cosmetics, and particularly relates to a full-plant anhydrous lip glaze and a preparation method thereof.
Background
The lip beautifying product is one kind of lip beautifying and color making up product for women to make lips ruddy and glossy, moisten and maintain lips, color lip, raise face's aesthetic feeling and correct lip contour. The lip glaze is one of lip beautifying products, can combine the saturated color of the lipstick and the brightness texture of the lip color into a whole, and realizes the brand new progress of color cosmetics.
With the improvement of living standard and the accumulation of human scientific knowledge, people have higher and higher requirements on the safety of cosmetics, and lip glaze containing natural plant components is widely favored. However, most of the currently asserted plant lip gloss (natural lip gloss) products are only introduced with partial plant-derived raw materials, and non-plant-derived grease, polymer-based functional raw materials, non-natural preservatives, coloring agents and the like still exist. The raw materials which are not of plant origin have complex components, are easy to cause anaphylactic reaction, such as lip mucosa chapping, peeling, cheilitis and the like, even contain carcinogen and seriously harm the body health.
Disclosure of Invention
In view of the above, the application provides a full-plant anhydrous lip glaze and a preparation method thereof, aiming at solving the problems that the lip glaze contains non-plant raw materials and is low in safety.
On one hand, the embodiment of the application provides a lip glaze with all plant components, which comprises the following components in percentage by weight:
vegetable oil and fat: 40 to 60 percent of the total weight of the mixture,
vegetable wax: 0.1 to 5 percent of the total weight of the mixture,
plant powder: 10 to 30 percent of the total weight of the mixture,
plant dispersant: 10 to 30 percent of the total weight of the mixture,
plant antioxidant: 0.1 to 1 percent of the total weight of the mixture,
plant preservative: 0.1 to 1 percent of the total weight of the mixture,
plant essential oil: 0.1 to 1 percent of the total weight of the mixture,
plant extract: 0.1 to 1 percent.
According to an embodiment of one aspect of the application, the vegetable oil or fat is selected from one or more of the plants squalane, jojoba oil, sunflower seed oil, castor oil, meadowfoam seed oil, coconut oil, shea butter, grape seed oil, macadamia nut oil, olive oil, palm oil, cocoa butter, jojoba butter, sugar gum, octyldodecanol, caprylic capric triglyceride and coco-caprylic capric triglyceride.
According to an embodiment of one aspect of the application, the vegetable wax is selected from one or more of candelilla wax, sunflower wax, carnauba wax, rice bran wax, jasmine wax, dextrin palmitate and dextrin isostearate.
According to an embodiment of one aspect of the present application, the plant powder includes an oil-soluble toner and a filler,
wherein the oil-soluble toner is selected from one or more of lycopene, beet red, safflower red, purple sweet potato, elderberry and radish red;
the filler is selected from corn starch and/or rice starch.
According to an embodiment of one aspect of the application, the vegetable dispersant is selected from one or more of the group consisting of soy lecithin, polyglycerol-3 diisostearate, polyglycerol-2 triisostearate, polyglycerol 2-dipolyhydroxystearate and oleic/linoleic/linolenic polyglyceryl esters.
According to an embodiment of one aspect of the application, the plant antioxidant is selected from one or more of vitamin E, tea polyphenols and rice bran oil.
According to an embodiment of one aspect of the application, the plant preservative is selected from one or more of anisic acid, peony root bark extract and magnolia bark extract.
According to an embodiment of one aspect of the application, the plant essential oil is selected from one or more of tea tree essential oil, rose essential oil, jasmine essential oil, sweet orange essential oil, chamomile essential oil and lavender essential oil.
According to an embodiment of one aspect of the present application, the plant extract is selected from one or more of jasmine extract, camellia extract, bletilla striata root extract, ampelopsis japonica root extract, atractylodes macrocephala root extract, peach blossom extract, cherry extract and opuntia ficus-indica stem extract.
In another aspect, the embodiment of the application provides a preparation method of a full-plant anhydrous lip glaze, which comprises the following steps:
heating vegetable oil and vegetable wax to 60-90 ℃, adding the mixture containing the vegetable oil, the vegetable powder and the vegetable dispersant, stirring and cooling to 40-45 ℃, adding the vegetable antioxidant, the vegetable preservative, the vegetable essential oil and the vegetable extract, and uniformly stirring to obtain the all-plant anhydrous lip glaze.
Compared with the prior art, the application has at least the following beneficial effects:
(1) the application provides a whole-plant anhydrous lip glaze, the texture is exquisite, the colour is even, possesses good moisturizing and moistening effect, and anticorrosive, anti-inflammatory performance are strong, and the security is high, also very friendly to the user of sensitive flesh, very agrees with the notion of "pure beautiful makeup" at present.
Firstly, the whole-plant anhydrous lip glaze takes 100% of materials from whole plants as raw materials, replaces chemical synthesis or non-natural ingredients in the traditional makeup product, is safer, and meets the requirements of consumers on natural products. Secondly, because the raw materials of the all-plant anhydrous lip glaze contain no water phase components, the problems of uneven color, poor moisturizing effect and the like caused by the difficulty in mutual dissolution of water and oil phases do not exist. In addition, the stability of the whole-plant anhydrous lip glaze can be improved and the color saturation of the whole-plant anhydrous lip glaze can be improved by adding efficient plant powder and plant dispersing agent; meanwhile, the use of the plant preservative can further improve the safety level of the whole-plant anhydrous lip glaze.
(2) The preparation method of the all-plant anhydrous lip glaze provided by the application is simple in process, short in time consumption, low in equipment requirement, capable of being well compatible with the existing process and extremely high in large-scale application potential.
Detailed Description
In order to make the application purpose, technical solution and beneficial technical effects of the present application clearer, the present application is further described in detail with reference to the following embodiments. It should be understood that the embodiments described in this specification are only for the purpose of explaining the present application and are not intended to limit the present application.
For the sake of brevity, only a few numerical ranges are explicitly disclosed herein. However, any lower limit may be combined with any upper limit to form ranges not explicitly recited; and any lower limit may be combined with any other lower limit to form a range not explicitly recited, and similarly any upper limit may be combined with any other upper limit to form a range not explicitly recited. Also, although not explicitly recited, each point or individual value between endpoints of a range is encompassed within the range. Thus, each point or individual value may, as its lower or upper limit, be combined with any other point or individual value or with other lower or upper limits to form ranges not explicitly recited.
In the description of the present application, it is to be noted that, unless otherwise specified, "above" and "below" are inclusive of the present number, and "plural" of "one or more" means two or more.
The above summary of the present application is not intended to describe each disclosed embodiment or every implementation of the present application. The following description more particularly exemplifies illustrative embodiments. At various points throughout this application, guidance is provided through a list of embodiments that can be used in various combinations. In each instance, the list is merely a representative group and should not be construed as exhaustive.
The existing lip glaze has complex raw material components, often contains more chemically synthesized or non-natural components, has low safety, is easy to cause anaphylactic reaction such as lip mucosa chapping, peeling, cheilitis and the like, even contains carcinogenic substances and seriously harms the body health.
Based on the above, the inventor conducts a great deal of research, and finds that the safety performance of the lip glaze can be improved by preparing the non-aqueous plant non-aqueous lip glaze, and the non-aqueous plant non-aqueous lip glaze has excellent safety, skin-sticking property, ductility and smoothness under the synergistic action of all plant components.
Full-plant anhydrous lip glaze
In one aspect, the embodiment of the application provides a full-plant anhydrous lip glaze, which comprises the following components in percentage by weight:
vegetable oil and fat: 40 to 60 percent of the total weight of the mixture,
vegetable wax: 0.1 to 5 percent of the total weight of the mixture,
plant powder: 10 to 30 percent of the total weight of the mixture,
plant dispersant: 10 to 30 percent of the total weight of the mixture,
plant antioxidant: 0.1 to 1 percent of the total weight of the mixture,
plant preservative: 0.1 to 1 percent of the total weight of the mixture,
plant essential oil: 0.1 to 1 percent of the total weight of the mixture,
plant extracts: 0.1 to 1 percent.
According to the embodiment of the application, the all-plant anhydrous lip glaze is prepared by adding plant wax, plant powder, plant dispersing agent and other plant raw materials with a certain content into a plant oil main body, so that the all-plant anhydrous lip glaze with fine texture, uniform color, moisture retention and high safety can be obtained.
According to the embodiment of the application, the all-plant anhydrous lip glaze takes 100% of all-plant-derived materials as raw materials, chemical synthesis or non-natural ingredients in the traditional makeup product are replaced, the lip glaze is safer, and the requirements of consumers on natural products are met. Secondly, the raw materials of the all-plant anhydrous lip glaze contain no water, so that the problems of uneven color, poor moistening effect and the like caused by difficult mutual dissolution of water and oil do not exist.
In some embodiments, the vegetable oil or fat may be selected from one or more of the plants squalane, jojoba oil, sunflower seed oil, castor oil, meadowfoam seed oil, coconut oil, shea butter, grape seed oil, macadamia nut oil, olive oil, palm oil, cocoa butter, jojoba butter, chicle, octyldodecanol, caprylic capric triglyceride and coco-caprylic capric triglyceride. The vegetable oil can be sugar gum, coconut oil, a mixture of caprylic capric triglyceride and cocol-caprylic capric triglyceride, or a mixture of sunflower seed oil, castor oil and coconut oil. The vegetable oil and fat can also be selected from any one of the vegetable oil and fat or a mixture of any more of the vegetable oil and fat.
According to the embodiment of the application, the grease is an essential component in the lip glaze, the grease listed above is vegetable grease extracted from plants, and the vegetable grease can ensure the safety, the moistening property, the fluidity and the ductility of the all-plant anhydrous lip glaze and ensure the moisturizing effect of the lip glaze.
According to the embodiment of the application, the carbohydrate gum in the vegetable oil has excellent solubility and compatibility, the water binding capacity is strong, and the water absorption effect is good even in a low-humidity environment, so that the skin moisture can be prevented from evaporating again, and the instant and long-acting water replenishing and moisturizing effect is achieved. In application, the carbohydrate gum not only has the effects of moisturizing and relieving, but also can endow the cosmetic product with soft silky skin feeling; in addition, the volatilization speed of the essence can be reduced, and the advantage of lasting fragrance is brought to the product. Meanwhile, the sugar gum has certain viscosity, is matched with solid vegetable oil and vegetable wax, has a plasticity effect, and can improve the use texture of the lip glaze; meanwhile, a breathable sugar film can be formed on the surface layer of the skin, so that better color development can be realized, and natural gloss from inside to outside can be provided.
According to the embodiment of the application, the octyl dodecanol belongs to isomeric alcohols, has smooth skin feel and moisturizing effect, has far better dispersion capacity on plant toner than many traditional oils, and can promote the absorption of functional active substances by the skin.
According to the embodiment of the application, the caprylic/capric triglyceride is vegetable oil with good skin feel, has good ductility, can make the skin have a smooth but not greasy feeling, and has a good effect of improving the uniform fineness of lip glaze.
According to the embodiment of the application, the coconut oil alcohol-caprylic capric triglyceride is a mixture of natural coconut oil, caprylic acid and capric acid, is a very good-ductility emollient and emollient, and can be used as a substitute of cyclomethicone volatile silicone. The coconut oil alcohol-caprylic capric triglyceride can provide extra oil for skin, reduce water evaporation in the skin, enhance skin hydration, make the skin soft and elastic, and make the whole plant anhydrous lip glaze easier to be smeared.
In some embodiments, the vegetable wax may be selected from one or more of candelilla wax, sunflower wax, carnauba wax, rice bran wax, jasmine wax, dextrin palmitate, and dextrin isostearate. Illustratively, the vegetable wax may be candelilla wax, jasmine wax, or a mixture of dextrin palmitate and dextrin isostearate. The vegetable wax may also be selected from any of the above vegetable waxes or a mixture of any of the above vegetable waxes.
According to the embodiment of the present application, the vegetable wax is a pure natural material extracted from plants by a method such as squeezing and extraction, has high safety in use, causes little damage to the skin, has a high degree of conformity with the skin, and is one of important raw materials for maintaining the coagulability and moisturizing property of the whole plant anhydrous lip gloss.
According to the examples of the present application, dextrin palmitate and dextrin isostearate are composed of dextrin and higher fatty acid ester extracted from starch, and when the amount thereof is less in lip glaze (2-4 wt%), the viscosity of the lip glaze system can be increased; when the dosage is larger (5-15 wt%), the liquid vegetable oil ester can form a semitransparent to transparent heat reversible gel, and the affinity of the whole plant anhydrous lip glaze to the skin and the extensibility during smearing are improved.
In some embodiments, the plant powder may include an oil-soluble toner selected from one or more of lycopene, beet red, safflower red, purple sweet potato, elderberry and radish red, and a filler selected from corn starch and/or rice starch.
According to the embodiment of the application, the oil-soluble toner has strong hydrophilicity, has good dispersibility in vegetable oil after being subjected to hydrophobic coating modification, and is high in color development chromaticity and not easy to discolor.
In some embodiments, the vegetable dispersant may be selected from one or more of the group consisting of soy lecithin, polyglyceryl-3 diisostearate, polyglyceryl-2 triisostearate, polyglyceryl 2-dipolyhydroxystearate and oleic/linoleic/linolenic polyglyceryl esters.
According to the embodiment of the application, the polyglycerol-3 diisostearate, the polyglycerol-2 triisostearate and the polyglycerol 2-dipolyhydroxystearate can be compatible with oil phase systems with various polarities, have good toner dispersing capacity, and are suitable for anhydrous and waterproof material systems. The oleic acid/linoleic acid/linolenic acid polyglycerol ester is a natural product derived from plants, and has excellent sensory effect, deep moisture retention, water resistance and anti-wrinkle effect.
In some embodiments, the plant antioxidant may be selected from one or more of vitamin E, tea polyphenols and rice bran oil.
According to the embodiment of the application, the plant antioxidant can prevent or delay the oxidation of unsaturated components in the whole plant anhydrous lip glaze and prolong the service life of the whole plant anhydrous lip glaze.
In some embodiments, the plant preservative may be selected from one or more of anisic acid, peony root bark extract and magnolia bark extract.
According to the embodiment of the application, the plant preservative can inhibit the growth and reproduction of microorganisms in the whole-plant anhydrous lip glaze, the property of the whole-plant anhydrous lip glaze is kept stable, the whole-plant anhydrous lip glaze is not easy to deteriorate after being uncovered, and the storage time is prolonged. Wherein, the anisic acid has better antiseptic effect under the acidic condition. The peony root bark extract has certain inhibition effect on bacteria, mold and fungus microorganisms such as escherichia coli, staphylococcus aureus, salmonella, aspergillus niger, candida, acne pathogenic bacteria and the like. The main active ingredients of the magnolia bark extract are magnolol and honokiol, and the magnolia bark extract has good inhibition effect on escherichia coli, staphylococcus aureus, bacillus subtilis and the like.
In some embodiments, the plant essential oil may be selected from one or more of tea tree essential oil, rose essential oil, jasmine essential oil, sweet orange essential oil, chamomile essential oil, and lavender essential oil.
According to the embodiment of the application, the plant essential oil can enhance the moisturizing and lustering feeling of the whole-plant anhydrous lip glaze, has a good repairing effect, can timely nourish and relieve the drying and peeling conditions of skin, and can endow the whole-plant anhydrous lip glaze with a specific fragrance.
In some embodiments, the plant extract may be selected from one or more of jasmine extract, camellia extract, bletilla striata root extract, ampelopsis japonica root extract, atractylodes macrocephala root extract, peach blossom extract, cherry extract, and prickly pear stem extract.
According to the embodiment of the application, the plant extract can prevent the skin from generating inflammation, can moisten the skin keratinocytes and is helpful for keeping the skin in a moist state.
According to the embodiment of the application, the whole-plant anhydrous lip glaze provided by the application is fine and smooth in texture, uniform in color, good in moisturizing and moistening effects, strong in anti-corrosion and anti-inflammatory performance, high in safety and very friendly to a user of sensitive muscles.
Preparation method of full-plant anhydrous lip glaze
The application also provides a preparation method of the whole-plant anhydrous lip glaze, which comprises the following steps:
heating vegetable oil and vegetable wax to 60-90 ℃, adding the mixture containing the vegetable oil, the vegetable powder and the vegetable dispersant, stirring and cooling to 40-45 ℃, adding the vegetable antioxidant, the vegetable preservative, the vegetable essential oil and the vegetable extract, and uniformly stirring to obtain the all-plant anhydrous lip glaze.
The preparation method of the all-plant anhydrous lip glaze provided by the application is simple in process, short in time consumption, low in equipment requirement, capable of being well compatible with the existing process and extremely high in large-scale application potential.
Examples
The present disclosure is more particularly described in the following examples that are intended as illustrative only, since various modifications and changes within the scope of the present disclosure will be apparent to those skilled in the art. Unless otherwise indicated, all parts, percentages, and ratios reported in the following examples are on a weight basis, and all reagents used in the examples are commercially available or synthesized according to conventional methods and can be used directly without further treatment, and the equipment used in the examples is commercially available.
Example 1
A whole-plant anhydrous lip glaze comprises the following components, by mass, 36% of carbohydrate gum, 10% of plant squalane, 2% of sunflower seed oil, 4.7% of jojoba fat, 1.4% of sunflower wax, 12% of polyglycerol-3 diisostearate, 10% of coconut oil alcohol-caprylic/capric triglyceride, 17% of elderberry toner, 6% of corn starch, 0.4% of rice bran oil, 0.05% of anisic acid, 0.15% of peony root bark extract, 0.1% of jasmine essential oil and 0.2% of camellia extract;
the preparation method of the all-plant anhydrous lip glaze comprises the following steps:
(1) dispersing elderberry powder and corn starch in a mixture of polyglycerol-3 diisostearate, coconut oil alcohol-caprylic/capric triglyceride and plant squalane, and uniformly stirring;
(2) heating sugar gum, sunflower seed oil, jojoba fat and sunflower wax to 70 ℃, adding the heated sugar gum, sunflower seed oil, jojoba fat and sunflower wax into the color paste obtained in the step (1), and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding rice bran oil, anisic acid, a peony root bark extract, jasmine essential oil and a camellia extract, and uniformly mixing to obtain the anhydrous lip glaze with a whole plant source.
Example 2
A whole-plant anhydrous lip glaze comprises the following components, by mass, 24% of sugar gum, 8% of plant squalane, 6% of jojoba oil, 19.4% of jojoba fat, 0.2% of sunflower wax, 10% of polyglycerol-2 triisostearate, 1% of dextrin palmitate, 12% of caprylic/capric triglyceride, 12.5% of radish red powder, 6% of corn starch, 0.4% of tea polyphenol, 0.05% of anisic acid, 0.15% of cortex magnoliae officinalis extract, 0.1% of rose essential oil and 0.2% of rhizoma atractylodis macrocephalae extract;
the preparation method of the all-plant anhydrous lip glaze comprises the following steps:
(1) dispersing radish red powder and corn starch in a mixture of polyglycerol-2 triisostearate, dextrin palmitate, caprylic/capric triglyceride and plant squalane, and uniformly stirring;
(2) heating sugar gum, jojoba oil, jojoba grease and sunflower wax to 65 ℃, adding the mixture into the color paste obtained in the step (1), and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding tea polyphenol, anisic acid, a magnolia bark extract, rose essential oil and a bighead atractylodes rhizome extract, and uniformly mixing to obtain the full-plant anhydrous lip glaze.
Example 3
A full-plant anhydrous lip glaze comprises the following components, by mass, 30% of sugar gum, 10% of jojoba oil, 6% of castor oil, 6.7% of cocoa butter, 0.5% of candelilla wax, 12% of polyglycerol-3 diisostearate, 10% of octyl dodecanol, 20% of purple sweet potato toner, 4% of rice starch, 0.4% of tea polyphenol, 0.1% of peony root bark extract, 0.1% of magnolia bark extract, 0.1% of sweet orange essential oil and 0.1% of cherry extract;
the preparation method of the all-plant anhydrous lip glaze comprises the following steps:
(1) dispersing purple sweet potato toner and rice starch in a mixture of polyglycerol-3 diisostearate, octyl dodecanol and jojoba oil, and uniformly stirring;
(2) heating sugar gum, castor oil, cocoa butter and candelilla wax to 70 ℃, adding the heated sugar gum, castor oil, cocoa butter and candelilla wax into the color paste obtained in the step (1), and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding tea polyphenol, peony root bark extract, magnolia bark extract, sweet orange essential oil and cherry extract into the mixture, and uniformly mixing to obtain the whole-plant anhydrous lip glaze.
Example 4
A full-plant anhydrous lip glaze comprises the following components, by mass, 26% of carbohydrate gum, 10% of plant squalane, 8% of meadowfoam seed oil, 14% of jojoba fat, 0.2% of carnauba wax, 8% of polyglycerol 2-dipolyhydroxystearate, 1% of dextrin isostearate, 8% of coconut oil alcohol-caprylic/capric triglyceride, 1% of soybean lecithin, 20% of lycopene, 3% of rice starch, 0.4% of tea polyphenol, 0.05% of anisic acid, 0.15% of magnolia bark extract, 0.1% of lavender essential oil and 0.1% of opuntia ficus stem extract;
the preparation method of the anhydrous lip glaze with all plant sources in the embodiment is as follows:
(1) dispersing lycopene and rice starch in mixture of polyglyceryl 2-dipolyhydroxystearate, dextrin isostearate, coconut oil alcohol-caprylic/capric triglyceride, soybean lecithin and plant squalane, and stirring;
(2) heating the sugar gum, the chinlon oil, the jojoba grease and the carnauba wax to 75 ℃, adding the mixture into the color paste obtained in the step (1), and uniformly stirring;
(3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding tea polyphenol, anisic acid, cortex magnoliae officinalis extract, lavender essential oil and twisted cactus stem extract, and uniformly mixing to obtain the whole-plant anhydrous lip glaze.
Comparative example
Comparative example 1
A non-whole plant anhydrous lip glaze comprises the following components, by mass, 36% of carbohydrate gum, 11.25% of hydrogenated polyisobutene, 2% of isododecane, 11.7% of polydimethylsiloxane, 4.4% of synthetic wax, 2.0% of cetyl polyethylene glycol/polypropylene glycol-10/1 dimethyl siloxane, 10% of octyldodecanol, 17% of red iron oxide, 6% of nylon powder, 0.05% of anisic acid, 0.15% of peony root bark extract, 0.15% of jasmine essential oil and 0.2% of camellia extract;
the preparation method of the all-plant anhydrous lip glaze comprises the following steps:
(1) dispersing red ferric oxide and nylon powder in a mixture of cetyl polyethylene glycol/polypropylene glycol-10/1 dimethyl siloxane and octyl dodecanol, and uniformly stirring;
(2) heating sugar gum, hydrogenated polyisobutene, isododecane, polydimethylsiloxane and synthetic wax to 70 ℃, adding the heated materials into the color paste obtained in the step (1), and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding anisic acid, the peony root and bark extract, jasmine essential oil and the camellia extract, and uniformly mixing to obtain the non-whole plant source anhydrous lip glaze.
Comparative example 2
A non-whole plant anhydrous lip glaze comprises the following components, by mass, 36% of carbohydrate gum, 10% of olive oil squalane, 2% of sunflower seed oil, 4.7% of jojoba fat, 1.4% of sunflower wax, 12% of polyglycerol-3 diisostearate, 10% of coconut oil alcohol-caprylic/capric triglyceride, 17% of elderberry toner, 5.5% of corn starch, 0.4% of rice bran oil, 0.05% of caprylyl glycol, 0.15% of phenoxy ethanol, 0.5% of ethylhexyl glycerol, 0.1% of jasmine essential oil and 0.2% of camellia extract;
the preparation method of the all-plant anhydrous lip glaze comprises the following steps:
(1) dispersing elderberry powder and corn starch in a mixture of polyglycerol-3 diisostearate, coconut oil alcohol-caprylic/capric triglyceride and olive oil squalane, and stirring uniformly;
(2) heating sugar gum, sunflower seed oil, jojoba fat and sunflower wax to 70 ℃, adding the heated sugar gum, sunflower seed oil, jojoba fat and sunflower wax into the color paste obtained in the step (1), and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding rice bran oil, caprylyl glycol, phenoxyethanol, ethylhexyl glycerol, jasmine essential oil and camellia extract, and uniformly mixing to obtain the anhydrous lip glaze with a non-plant preservative source.
Comparative example 3
A non-whole plant anhydrous lip glaze comprises the following components, by mass, 35% of octyl dodecanol, 10% of polydimethylsiloxane, 9% of hydrogenated polyisobutene, 4.7% of synthetic wax, 6.4% of microcrystalline wax, 2% of cetyl polyethylene glycol/polypropylene glycol-10/1 dimethyl siloxane, 15% of caprylic/capric triglyceride, 10% of red ferric oxide, 6% of talcum powder, 0.4% of tocopherol, 0.5% of phenoxyethanol and 1% of ethylhexyl glycerol;
the preparation method of the all-plant anhydrous lip glaze comprises the following steps:
(1) dispersing red ferric oxide and talcum powder in a mixture of cetyl polyethylene glycol/polypropylene glycol-10/1 dimethyl siloxane and caprylic/capric triglyceride, and uniformly stirring;
(2) heating octyl dodecanol, polydimethylsiloxane, hydrogenated polyisobutene, synthetic wax and microcrystalline wax to 70 ℃, adding the heated mixture into the color paste obtained in the step (1), and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2) to 40-45 ℃, adding tocopherol, phenoxyethanol and ethylhexyl glycerol, and uniformly mixing to obtain the non-plant-source anhydrous lip glaze.
In comparison with example 1, comparative example 1 contained non-plant materials, comparative example 2 contained non-plant materials and no plant preservatives, and comparative example 3 contained non-plant materials and no plant extracts.
Test section
1) And (3) stability testing: (1) placing in an electric heating constant temperature incubator at 40-50 deg.C for 30-50 days, and observing after recovering room temperature; (2) changing frequently between 0-50 ℃ within 24h, repeating the operation for 15-30 days, and observing after recovering the room temperature, (3) storing at-5 ℃ and 40 ℃ for 3 times in a circulating way, respectively storing for 24h each time, namely storing for 24h at-5 ℃, storing for 24h at the room temperature, then storing in a constant temperature box at 40 ℃ for 24h, and circulating for 3 times in sequence to observe the stability. (4) The stability was observed after 1 week storage at-5 ℃.
2) The centrifugal test method comprises the following steps: and (3) adding the sample into a centrifuge, rotating at 10000rpm for 10-15min or 3000rpm for 30min or 300rpm for 1h, and observing the layering and separation conditions of the liquid to obtain the results shown in the following table 1.
The all-plant anhydrous lip glazes of the above examples 1 to 4 and comparative examples 1 to 3 were subjected to relevant performance tests. The test results of examples 1 to 4 and comparative examples 1 to 3 are shown in Table 1 below.
TABLE 1 Performance test results of all-plant anhydrous lip glaze of examples 1 to 4 and comparative examples 1 to 3
| Sample (I) | Heat resistance | Cold-resistant | Stability of |
| Example 1 | Without obvious change | Without obvious change | Without phenomenon of delamination |
| Example 2 | Without obvious change | Without obvious change | Without phenomenon of delamination |
| Example 3 | Without obvious change | Without obvious change | Without phenomenon of delamination |
| Example 4 | Without obvious change | Without obvious change | Without phenomenon of delamination |
| Comparative example 1 | Without obvious change | Without obvious change | Without phenomenon of delamination |
| Comparative example 2 | Without obvious change | Without obvious change | Without phenomenon of delamination |
| Comparative example 3 | Without obvious change | Without obvious change | Without phenomenon of delamination |
From the test results in table 1 above, it can be seen that the all-plant anhydrous lip glazes of examples 1 to 4 have good heat resistance, cold resistance and stability, and can achieve the same effect as the non-all-plant anhydrous lip glazes of comparative examples 1 to 3.
3) And (3) testing the corrosion resistance:
the selected strains are five strains of staphylococcus aureus, escherichia coli, pseudomonas aeruginosa, candida albicans and aspergillus niger.
The culture medium is beef extract peptone culture medium and agar culture medium.
Preparation of a test bacterial solution:
(1) preparation of Standard suspension
9.9mL of 1% sulfuric acid and 0.1mL of 1% barium chloride were mixed to prepare a suspension with a concentration of 3X 10 8 cfu/mL, and this suspension was diluted 3-fold.
(2) Preparation of bacterial suspension
Before the experiment, the strain is inoculated on each culture medium slant and cultured at the constant temperature of 36 ℃ for 48 h. Washing the cultured active strains in a sterilized conical flask by using sterilized normal saline, and fully shaking and shaking uniformly. The suspension was diluted by pipetting from the flask with a pipette to obtain turbidity and turbidity of the standard suspension (3 x 10) 8 cfu/mL) until they are the same;
at this time, the diluted bacteria solution was further diluted by 3 times, i.e., the concentration was 1 x 10 8 Determining the bacterial number of the bacterial suspension of cfu/mL.
(3) Preparation of mould suspension
Washing the cultured active strains in a sterilized conical flask by using sterilized normal saline, and fully oscillating and shaking up; the bacteria liquid is sucked from the conical flask by a pipette gun to be diluted by 10 times, the count of each dilution is carried out by a blood counting plate, the total number of the molds in 5 middle lattices is 190-210, and the bacteria suspension falling in the range is 1 x 10 that is required by us 8 cfu/mL of mold suspension, and determining the mold number.
Inoculation:
the inoculation mode is single-bacterium inoculation: the sensitivity of each microorganism to the preservative system is readily understood by performing an experiment with each test strain alone.
The inoculation times are one-time inoculation: only one inoculation was performed at the beginning of the experiment, and the whole experiment period was 28 days (one bacterial-added 28-day microbial experiment).
The operation method comprises the following steps:
weighing 30g of sample to be tested, and correspondingly adding 0.3mL of sample with concentration of 1 x 10 7 ～1*10 8 The bacterial suspension and the mould suspension of cfu/mL are evenly stirred by a sterile key and then covered with a preservative film, the bacteria are cultured in an incubator at 32.5 +/-2.5 ℃, and the mould is cultured in an incubator at 22.5 +/-2.5 ℃.
Because the samples are oil-soluble, 10g of the samples are taken, 10mL of sterile Tween-80, 10mL of sterile white mineral oil and 70mL of sterile normal saline are added, and a sterile glass rod is used for fully and uniformly mixing;
sucking 1mL of diluted sample solution, adding into 9mL of sterilized normal saline, and sequentially diluting to 10 -1 、10 -2 、10 -3 、10 -4 、10 -5 、10 -6 And 10 -7 Equal dilution; three samples with appropriate dilution are taken, 1mL of the sample is respectively sucked and added into a sterilized plate, colony counting is carried out, and two samples are carried out in parallel.
Culturing:
culturing the bacteria in an incubator at 32.5 +/-2.5 ℃;
culturing mould in 22.5 + -2.5 deg.C incubator;
the mixed bacteria were cultured in an incubator at 28 ℃.
And (3) counting colonies:
after the total number of live bacteria and mold in the sample is separated and calculated on 0, 7, 14, 21 and 28 days, the plate is put back into the incubator for the next observation, and the plate is not opened during the observation so as to avoid burning bacteria and make the next observation impossible.
Standard methods for colony enumeration:
1. firstly, selecting a plate with the average colony number of 30-300 as a total bacterial colony number measuring range, and selecting a plate with the average colony number of 5-50 as a total mould colony number measuring range;
2. two dilutions are 30-300, and the ratio is calculated. If the ratio is less than or equal to 2, reporting the average number, and if the ratio is more than 2, calculating the total number of bacteria according to the smaller dilution;
3. all dilutions were greater than 300, calculated as the average colony with the highest dilution;
4. all dilutions were less than 30, calculated as the number of evaluated colonies with the lowest dilution;
5. all dilutions are outside 30-300, one of them is greater than 300, and the adjacent plus one dilution is less than 30, calculated as the average colony number closest to 30 or 300;
6. if the plate contains colonies which are connected into sheets or flower dot samples and grow, calculation is not suitable;
7. if the plate colonies are less than half of the plate and the colonies are uniform in the other half, the plate colonies can be counted 2 a later to report the number of colonies on the full plate.
The all-plant anhydrous lip glazes of the above examples 1 to 4 and comparative examples 1 to 3 were subjected to relevant performance tests. The test results of examples 1 to 4 and comparative examples 1 to 3 are shown in Table 2 below.
TABLE 2 Performance test results of the all-plant anhydrous lip glaze of examples 1 to 4 and comparative examples 1 to 3
The test results in the table 2 show that the all-plant anhydrous lip glaze 1d in the examples 1-4 reaches the standard of the anticorrosion effect of the cosmetics. The non-all-plant anhydrous lip glaze in the comparative examples 1-3 can meet the anti-corrosion requirements of cosmetics, but has low safety performance and can cause cheilitis and other problems.
4) Anti-inflammatory assay
Healthy male SD rats were randomly divided into a model group, an indomethacin group, and an example sample group, 10 animals per group. The skin was dosed continuously for 3d and the model group was dosed with deionized water. The rat's right hind footpad was injected subcutaneously with 0.05mL of 1% carrageenan slurry 1h after the last dose to cause inflammation. The diameter of the area 0.5cm below the naked joint of the right hind limb of each rat was measured at 8-fold magnification at 1, 2, 4, 6, and 24 hours before and after the onset of inflammation, respectively, and the difference in swelling at different time points before and after the onset of inflammation was used as the swelling degree.
The all-plant anhydrous lip glazes of the above examples 1 to 4 and comparative examples 1 to 3 were subjected to relevant performance tests. The test results of examples 1 to 4 and comparative examples 1 to 3 are shown in Table 3 below.
Table 3 results of performance test of all-plant anhydrous lip glaze in examples 1 to 4 and comparative examples 1 to 3
As can be seen from table 3 above, the all-plant anhydrous lip glaze of examples 1 to 4 has a good anti-inflammatory effect, while the non-all-plant anhydrous lip glaze of comparative examples 1 to 3 has a low anti-inflammatory effect and is not beneficial to sensitive muscle consumers because the all-plant anhydrous lip glaze of comparative examples 1 to 3 does not contain substances having an anti-inflammatory effect, such as plant extracts, and the swelling degree of the naked joint of the right hind limb of a rat is large.
From the test results, the all-plant anhydrous lip glaze of the embodiments 1 to 4 has good heat resistance, cold resistance and stability, and the anticorrosive and anti-inflammatory effects can meet the actual requirements, so that the all-plant anhydrous lip glaze has innovativeness and novelty in the cosmetic market and has strong product competitiveness. The test results of the comparative examples 1 to 3 show that the stability, corrosion resistance, anti-inflammation and other safety performances of the non-all-plant anhydrous lip glaze are poor.
To sum up, the whole-plant anhydrous lip glaze takes 100% of materials from whole plants as raw materials, replaces chemical synthesis or non-natural ingredients in the traditional makeup product, can make the lip glaze safer, and meets the requirements of consumers on natural products. Secondly, the raw materials of the all-plant anhydrous lip glaze contain no water, so that the problems of uneven color, poor moistening effect and the like caused by difficult mutual dissolution of water and oil do not exist. In addition, the stability of the all-plant anhydrous lip glaze can be improved and the color saturation of the all-plant anhydrous lip glaze can be improved by adding the efficient plant powder and the plant dispersing agent; meanwhile, the use of the plant preservative can further improve the safety level of the whole-plant anhydrous lip glaze.
While the invention has been described with reference to specific embodiments, the scope of the invention is not limited thereto, and those skilled in the art can easily conceive various equivalent modifications or substitutions within the technical scope of the invention. Therefore, the protection scope of the present application shall be subject to the protection scope of the claims.
Claims (10)
1. The all-plant anhydrous lip glaze is characterized by comprising the following components in percentage by weight:
vegetable oil and fat: 40 to 60 percent of the total weight of the mixture,
vegetable wax: 0.1-5% of the total weight of the mixture,
plant powder: 10 to 30 percent of the total weight of the mixture,
plant dispersant: 10 to 30 percent of the total weight of the mixture,
plant antioxidant: 0.1 to 1 percent of the total weight of the mixture,
plant preservative: 0.1 to 1 percent of the total weight of the mixture,
plant essential oil: 0.1 to 1 percent of the total weight of the mixture,
plant extracts: 0.1 to 1 percent.
2. The all-plant anhydrous lip glaze according to claim 1, wherein the vegetable oil and fat is selected from one or more of plant squalane, jojoba oil, sunflower seed oil, castor oil, meadowfoam seed oil, coconut oil, shea butter, grape seed oil, macadamia nut oil, olive oil, palm oil, cocoa butter, jojoba butter, sugar gum, octyl dodecanol, caprylic capric triglyceride and cocol-caprylic capric triglyceride.
3. The all-plant anhydrous lip glaze according to claim 1, wherein the plant wax is selected from one or more of candelilla wax, sunflower wax, carnauba wax, rice bran wax, jasmine wax, dextrin palmitate and dextrin isostearate.
4. The all-plant anhydrous lip glaze according to claim 1, wherein the plant powder comprises oil-soluble toner and filler,
wherein the oil-soluble toner is selected from one or more of lycopene, beet red, safflower red, purple sweet potato, elderberry and radish red;
the filler is selected from corn starch and/or rice starch.
5. The whole plant anhydrous lip glaze according to claim 1, wherein the plant dispersing agent is selected from one or more of soybean lecithin, polyglycerol-3 diisostearate, polyglycerol-2 triisostearate, polyglycerol 2-dipolyhydroxystearate and oleic/linoleic/linolenic polyglyceryl esters.
6. The full-plant anhydrous lip glaze according to claim 1, wherein the plant antioxidant is selected from one or more of vitamin E, tea polyphenol and rice bran oil.
7. The all-plant anhydrous lip glaze according to claim 1, wherein the plant preservative is selected from one or more of anisic acid, peony root bark extract and magnolia bark extract.
8. The all-plant anhydrous lip glaze according to claim 1, wherein the plant essential oil is one or more selected from tea tree essential oil, rose essential oil, jasmine essential oil, sweet orange essential oil, chamomile essential oil and lavender essential oil.
9. The whole plant anhydrous lip glaze according to claim 1, wherein the plant extract is selected from one or more of jasmine extract, camellia extract, bletilla striata root extract, ampelopsis japonica root extract, atractylodes macrocephala root extract, peach blossom extract, cherry extract and opuntia ficus-indica stem extract.
10. A process for preparing a whole plant anhydrous lip glaze according to any one of claims 1 to 9, comprising:
heating the vegetable oil and the vegetable wax to 60-90 ℃, adding the mixture containing the vegetable oil, the vegetable powder and the vegetable dispersant, stirring and cooling to 40-45 ℃, adding the vegetable antioxidant, the vegetable preservative, the vegetable essential oil and the vegetable extract, and uniformly stirring to obtain the all-plant anhydrous lip glaze.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120308500A1 (en) * | 2011-05-13 | 2012-12-06 | Mary Kay, Inc. | Lip stick |
| CN104738033A (en) * | 2015-02-02 | 2015-07-01 | 广东工业大学 | Preservative composition derived from plants |
| CN105055244A (en) * | 2015-08-24 | 2015-11-18 | 上海东晟源日化有限公司 | Organic natural plant preservative |
| CN111671676A (en) * | 2020-06-30 | 2020-09-18 | 广州卡洛莱化妆品有限公司 | Moisturizing aromatic lip balm and preparation method thereof |
| CN112451443A (en) * | 2020-12-11 | 2021-03-09 | 山西娇禾生物科技有限公司 | Lipstick prepared by extracting pure natural rose and preparation method thereof |
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2022
- 2022-05-17 CN CN202210534648.1A patent/CN114948828A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120308500A1 (en) * | 2011-05-13 | 2012-12-06 | Mary Kay, Inc. | Lip stick |
| CN104738033A (en) * | 2015-02-02 | 2015-07-01 | 广东工业大学 | Preservative composition derived from plants |
| CN105055244A (en) * | 2015-08-24 | 2015-11-18 | 上海东晟源日化有限公司 | Organic natural plant preservative |
| CN111671676A (en) * | 2020-06-30 | 2020-09-18 | 广州卡洛莱化妆品有限公司 | Moisturizing aromatic lip balm and preparation method thereof |
| CN112451443A (en) * | 2020-12-11 | 2021-03-09 | 山西娇禾生物科技有限公司 | Lipstick prepared by extracting pure natural rose and preparation method thereof |
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