KR102635166B1 - Manufacturing method of cosmetic composition containing pine needle extract and deep ocean water - Google Patents

Abstract

The present invention relates to a method for producing a cosmetic composition containing pine needle extract and deep sea water, and more specifically, to a pine needle extract manufacturing step of producing a pine needle extract using deep ocean water, and a pine needle extract prepared through the pine needle extract manufacturing step. It consists of a fermentation step of inoculating and fermenting lactic acid bacteria and a raw material mixing step of mixing a skin improver and vegetable oil with the pine needle fermentation product produced through the fermentation step.
The cosmetic composition prepared through the above process has improved physiological activities such as antioxidant, inflammation relieving, and moisturizing performance, providing a cosmetic that exhibits effects such as skin moisturizing, skin wrinkle improvement, skin whitening, and acne improvement.

Description

Method for producing a cosmetic composition containing pine needle extract and deep ocean water {MANUFACTURING METHOD OF COSMETIC COMPOSITION CONTAINING PINE NEEDLE EXTRACT AND DEEP OCEAN WATER}

The present invention relates to a method for producing a cosmetic composition containing pine needle extract and deep sea water. More specifically, the present invention relates to a method of manufacturing a cosmetic composition containing pine needle extract and deep sea water, and more specifically, to improve physiological activities such as antioxidant, inflammation relief and moisturizing, thereby improving skin moisturization, skin wrinkle improvement, skin whitening and acne. It relates to a method for producing a cosmetic composition containing pine needle extract and deep sea water, which provides a cosmetic with the following effects.

Skin is a membrane that covers the outside of the body and performs various physiological functions to protect the body from environmental factors such as various external stimuli, obstacles, and dryness, and plays a role in protecting and regulating internal organs and other organs of the body. do.

However, as the skin ages, its physiological functions deteriorate, the secretion of various hormones that regulate metabolism decreases, and the function and activity of immune cells decrease. In addition, the appearance or function of the skin changes due to repeated exposure to light or heat. As a result, free radicals and active harmful oxygen increase, excessive physical and chemical stimulation and stress lead to a decrease in the normal function of the skin and blemishes due to melanin deposition. , it damages the skin by promoting the formation of freckles and skin aging phenomenon.

In order to prevent skin aging and damage and maintain healthier and more beautiful skin, physiologically active substances obtained from various animals, plants, and microorganisms are added to cosmetics to maintain the skin's inherent functions and activate skin cells to promote skin renewal. Efforts to maintain skin health by promoting metabolism are continuing, and cosmetics and external skin agents are being developed accordingly.

Meanwhile, pine (Pinus densiflora Seibold et Zuccarini) is an evergreen coniferous tree growing wild in the mountains of Korea. It mainly consists of red pine (Yuk pine), which grows abundantly in inland regions, as well as pine pine, Rigida pine, Bear pine (Sea pine), and white pine. Pine needles, which are the leaves of the pine tree, have been used for medicinal purposes in oriental medicine or folk medicine or as a health food since ancient times. According to Donguibogam, pine needles are known to be effective in treating gastrointestinal diseases, stroke, high blood pressure, neuralgia, and asthma.

These pharmacological effects of pine needles include essential oil components, protein, vitamin A, vitamin C, vitamin K, vitamin P (rutin), phosphorus, iron, enzymes, tannin, chlorophyll, bitter substances, and flavonoids contained in pine needles. It is made up of functional substances, and in particular, vitamin P (rutin) has an excellent effect in promoting blood circulation and preventing high blood pressure and aging, and the volatile essential oil of pine needles plays a role in relieving fatigue during forest bathing.

Methods for extracting these functional substances from pine needles include a method of extracting extract from pine needles without going through a fermentation process and a method of fermenting pine needles to obtain a fermented broth. However, the method using general natural fermentation has the problem of low physiological and nutritional functionality due to the dilute concentration of pine needle extract. Therefore, there is a need for methods to improve the physiological components and activities of pine needle extract.

Korean Patent Registration No. 10-1315638 (2013.09.30.) Korean Patent Registration No. 10-1686399 (2016.12.08.)

The object of the present invention is to provide a cosmetic composition containing pine needle extract and deep sea water that improves physiological activities such as antioxidant, inflammation relief and moisturizing, thereby providing a cosmetic that exhibits effects such as skin moisturizing, skin wrinkle improvement, skin whitening and acne improvement. To provide a manufacturing method.

The purpose of the present invention is a pine needle extract manufacturing step of producing pine needle extract using deep sea water, a fermentation step of inoculating and fermenting the pine needle extract prepared through the pine needle extract manufacturing step with lactic acid bacteria, and fermenting the pine needle produced through the fermentation step. This is achieved by providing a method for producing a cosmetic composition containing pine needle extract and deep sea water, which consists of a raw material mixing step of mixing a skin improver and vegetable oil with water.

According to a preferred feature of the present invention, the pine needle extract manufacturing step is accomplished by mixing 100 parts by weight of pine needle powder with 800 to 1,000 parts by weight of deep ocean water and heating at a temperature of 85 to 95 ° C. for 60 to 120 minutes.

According to a more preferred feature of the present invention, the fermentation step is performed by inoculating 0.01 to 0.1 parts by weight of lactic acid bacteria into 100 parts by weight of the pine needle extract prepared through the pine needle extract manufacturing step and then inoculating the lactic acid bacteria at a temperature of 36 to 38° C. for 45 to 50 hours. It is made by fermentation.

According to a more preferred feature of the present invention, the lactic acid bacteria are composed of one or more selected from the group consisting of Lactobacillus sakei, Lactobacillus plantarum, Lactobacillus brevis, and Pediococcus esidilactici.

According to an even more preferred feature of the present invention, the raw material mixing step is performed by mixing 5 to 10 parts by weight of a skin improvement agent and 1 to 3 parts by weight of vegetable oil with 100 parts by weight of the pine needle fermentation product prepared through the fermentation step.

According to an even more preferred feature of the present invention, the skin improving agent is composed of one or more selected from the group consisting of brewer's yeast extract, field bean extract, green tea extract, and edelweiss extract.

According to an even more preferred feature of the present invention, the vegetable oil is made of one or more selected from the group consisting of argan kernel oil, jojoba seed oil, coconut palm oil, olive oil, and parmesan oil.

The method for producing a cosmetic composition containing pine needle extract and deep sea water according to the present invention improves physiological activities such as antioxidant, inflammation relief, and moisturizing, and produces a cosmetic that exhibits effects such as skin moisturizing, skin wrinkle improvement, skin whitening, and acne improvement. It provides excellent effects.

Figure 1 is a flowchart showing a method for producing a cosmetic composition containing pine needle extract and deep sea water according to the present invention.

Below, preferred embodiments of the present invention and the physical properties of each component are described in detail, but are intended to be described in detail so that those skilled in the art can easily practice the invention. This does not mean that the technical idea and scope of the present invention are limited.

The method for producing a cosmetic composition containing pine needle extract and deep sea water according to the present invention includes a pine needle extract manufacturing step (S101) of producing a pine needle extract using deep ocean water, and a pine needle extract prepared through the pine needle extract manufacturing step (S101). It consists of a fermentation step (S103) of inoculating and fermenting lactic acid bacteria and a raw material mixing step (S105) of mixing a skin improver and vegetable oil with the pine needle fermentation product produced through the fermentation step (S103).

The pine needle extract manufacturing step (S101) is a step of producing pine needle extract using deep ocean water, mixing 800 to 1000 parts by weight of deep ocean water with 100 parts by weight of pine needle powder and heating at a temperature of 85 to 95° C. for 60 to 120 minutes. It is desirable to do so.

The pine needles contain a large amount of 3-carene, limonene, and terpinolene, and the pine needle extract prepared through the above process serves to provide antioxidant and inflammation-relieving effects.

In addition, the various functions and efficacy of deep ocean water have already been proven through experiments and epidemiological investigations, and in this invention, deep ocean water taken from the sea of Goseong, Gangwon-do was used.

Deep ocean water exists at a depth of more than 200m where sunlight does not reach. It has almost no organic matter or pathogens, maintains a stable low temperature throughout the year, and is rich in nutrients essential for the growth of marine plants. It is a seawater resource that has matured for a long time. In Greenland in the North Atlantic, it subsides due to temperature and salinity differences between seawater and ice to form deep water. It is unique water that circulates through the ocean (Atlantic → Indian Ocean → Pacific) and does not mix vertically. There is no phytoplankton in the deep sea where deep ocean water is collected. Since photosynthesis does not occur, it is rich in inorganic nutrients such as nitrogen, phosphorus, and silicic acid, and a large amount of various minerals such as sodium, magnesium, calcium, and potassium, and trace elements such as zinc, selenium, and manganese exist in stable form. In addition, there is no pollution from the air or inflow water, and the number of viable bacteria is not high compared to surface water. It is not polluted by general bacteria, so it has superior cleanliness compared to surface water or groundwater, and has an excellent scavenging effect on active oxygen due to the action of dissolved metal ions. It is known to have a magnesium and calcium content of 3:1, so it has a balance close to that of human blood.

In addition, since the deep sea water is superior to purified water in eluting the active ingredients contained in pine needles, the effects of the cosmetic composition prepared through the present invention, such as skin moisturizing, skin wrinkle improvement, skin whitening, and acne improvement, are further enhanced. will improve.

In the pine needle extract manufacturing step (S101), if the content of deep ocean water is less than 800 parts by weight, the above effect is minimal, and if the content of deep ocean water exceeds 1000 parts by weight, the above effect is not significantly improved and is added to the deep ocean water. This is undesirable because the concentration of the active ingredient in the eluted pine needles is excessively low.

In addition, in the pine needle extract manufacturing step (S101), if the heating temperature is less than 85°C or the heating time is less than 60 minutes, the elution amount of the active ingredient contained in the pine needles decreases, and if the heating temperature exceeds 95°C or the heating time is 120 minutes. If the amount is exceeded, it is undesirable because the eluted active ingredient may be destroyed without significantly improving the amount of elution of the active ingredient contained in the pine needles.

The fermentation step (S103) is a step of inoculating and fermenting the pine needle extract prepared through the pine needle extract manufacturing step (S101) with lactic acid bacteria. Lactic acid bacteria are added to 100 parts by weight of the pine needle extract prepared through the pine needle extract manufacturing step (S101). It is preferable to inoculate 0.01 to 0.1 parts by weight and then ferment at a temperature of 36 to 38°C for 45 to 50 hours.

The pine needle extract fermented through the above process increases the content of various amino acids, organic acids, and antioxidant substances that are good for the skin, promoting skin metabolism and smoothing the skin texture. Through the fermentation process, the particles of the active ingredient become smaller. Toxic substances such as heavy metals are decomposed, improving skin absorption of active ingredients, enhancing physiological activity, and suppressing or alleviating side effects such as skin troubles and allergies.

At this time, the lactic acid bacteria are one or more selected from the group consisting of Lactobacillus sakei , Lactobacillus plantarum , Lactobacillus brevis , and Pediococcus acidilactici . It is desirable to consist of

If the inoculum of lactic acid bacteria consisting of the above components is less than 0.01 part by weight, fermentation of the pine needle extract does not proceed properly, and if the inoculum of the lactic acid bacteria exceeds 0.1 part by weight, the fermentation speed of the pine needle extract is not significantly improved and the manufacturing cost is excessively high. This is undesirable because it increases

The raw material mixing step (S105) is a step of mixing a skin improver and vegetable oil with the pine needle fermentation product prepared through the fermentation step (S103). 100 parts by weight of the pine needle fermentation product prepared through the fermentation step (S103) It is preferably made by mixing 5 to 10 parts by weight of a skin improving agent and 1 to 3 parts by weight of vegetable oil.

The skin improving agent contains 5 to 10 parts by weight and consists of one or more selected from the group consisting of brewer's yeast extract, field bean extract, green tea extract, and edelweiss extract, where brewer's yeast extract, field bean extract, green tea extract, and edelweiss extract are 1. It is more preferable to mix them in a ratio of :1:1:1 by weight.

The skin improvement agent composed of the above ingredients provides a moisturizing effect to the skin and plays a role in improving skin health. The beer yeast extract is extracted from yeast fermenting during the manufacturing process of beer, and contains various nutrients, minerals, vitamins, amino acids and Contains antioxidant ingredients to provide anti-aging effects, provides nutrients and moisture to the skin, improves skin, and plays a role in preventing and relieving skin troubles.

In addition, the field bean extract serves to provide elastic and shiny skin by supplying protein ingredients to the skin.

In addition, the green tea extract contains a number of active ingredients, including catechin, a polyphenolic compound, and has excellent various pharmacological effects, and is especially excellent in antioxidant properties, removing free radicals generated by stress inside and outside the body, thereby protecting the skin. It plays a role in preventing aging and reducing stress.

In addition, the edelweiss extract removes sebum components and various foreign substances remaining on the skin, makes the skin healthy and clear, and suppresses and improves the occurrence of skin inflammation.

If the content of the skin improver is less than 5 parts by weight, the effect is minimal, and if the content of the skin improver exceeds 10 parts by weight, the effect is not significantly improved and the formulation stability of the cosmetic composition may be reduced. It is not desirable.

In addition, the vegetable oil contains 1 to 3 parts by weight and provides nutrients and moisturizing effects to the skin, prevents aging by improving blood circulation, improves wrinkles, and promotes skin health. Argan kernel oil , consisting of one or more selected from the group consisting of jojoba seed oil, coconut palm oil, olive oil, and parmesan oil, and argan kernel oil, jojoba seed oil, coconut palm oil, olive oil, and parmesan oil in a ratio of 1:1:1. It is preferable to mix them in a ratio of :1:1 by weight.

The argan kernel oil is rich in unsaturated fatty acids, which has the effect of improving blood vessel health and blood circulation. It is rich in tocopherol, an antioxidant, which not only provides antioxidant effects, but also improves the preservability of cosmetic compositions.

In addition, the jojoba seed oil has a chemical structure similar to human sebum, so it easily penetrates into the skin. It has an excellent moisturizing effect and not only improves skin inflammation through antibacterial action, but also contains vitamin E to strengthen the skin barrier and It has a skin regenerative effect and has the effect of soothing dead skin cells to provide smooth skin.

In addition, the coconut palm oil is rich in vitamins, minerals, lauric acid, and caprylic acid, and has effects such as moisturizing, improving skin immunity, and protecting the skin barrier.

In addition, the olive oil contains oleic acid, linoleic acid, and vitamins A, D, E, and K, which relieves skin inflammation and pain through antibacterial and anti-inflammatory effects. It is useful for dry skin or winter skin care due to its moisturizing effect, and is an antioxidant. Due to its action, it has anti-aging and wrinkle improvement effects.

In addition, the parmesan oil is rich in triglycerides, linolenic acid, etc., showing anti-aging and wrinkle improvement effects.

If the content of the vegetable oil is less than 1 part by weight, the above effect is minimal, and if the content of the vegetable oil exceeds 3 parts by weight, the above effect is not significantly improved, but slipperiness is excessively increased and the preference is lowered, This is undesirable because it excessively increases manufacturing costs.

Hereinafter, the method for producing a cosmetic composition containing pine needle extract and deep sea water according to the present invention and the physical properties of the cosmetic composition produced by the method will be described through examples.

<Preparation Example 1> Preparation of pine needle extract

Pine needle extract was prepared by mixing 100 parts by weight of pine needle powder with 800 to 1,000 parts by weight of deep ocean water (water taken from a depth of 600 m or more off the coast of Goseong, Gangwon-do) and heating at a temperature of 85 to 95°C for 60 to 120 minutes.

<Preparation Example 2> Preparation of fermented pine needles

Fermented pine needles were prepared by inoculating 0.05 parts by weight of lactic acid bacteria (Lactobacillus sakei) into 100 parts by weight of the pine needle extract prepared through Preparation Example 1 and fermenting at a temperature of 37°C for 48 hours.

<Example 1>

7.5 parts by weight of skin improving agent (breer's yeast extract, wild bean extract, green tea extract, and edelweiss extract mixed in a weight ratio of 1:1:1:1) and vegetable oil ( Prepare a cosmetic composition containing pine needle extract and deep sea water by mixing 2 parts by weight of argan kernel oil, jojoba seed oil, coconut palm oil, olive oil, and parmesan oil in a ratio of 1:1:1:1:1 by weight. did.

<Example 2>

Proceeding in the same manner as Example 1, a cosmetic composition containing pine needle extract and deep sea water was prepared by mixing 5 parts by weight of a skin improving agent and 1 part by weight of vegetable oil.

<Example 3>

Proceeding in the same manner as Example 1, a cosmetic composition containing pine needle extract and deep sea water was prepared by mixing 10 parts by weight of a skin improving agent and 3 parts by weight of vegetable oil.

<Comparative Example 1>

A cosmetic composition was prepared by mixing 100 parts by weight of pine needle powder with 800 to 1,000 parts by weight of purified water and heating at a temperature of 85 to 95°C for 60 to 120 minutes.

<Comparative Example 2>

Proceed in the same manner as Example 1, but using pine needle extract prepared by mixing 800 to 1000 parts by weight of purified water with 100 parts by weight of pine needle powder and heating at a temperature of 85 to 95 ° C. for 60 to 120 minutes to obtain a product containing pine needle extract. A cosmetic composition was prepared.

The effects of the cosmetic compositions prepared through Examples 1 to 3 and Comparative Examples 1 to 2 on skin moisturizing, skin wrinkle improvement, skin whitening, and acne improvement were measured and are shown in Table 1 below.

{However, skin moisturizing, skin wrinkle improvement, and skin whitening were tested on 50 test subjects. 2 mL of the prepared cosmetic composition was applied to the skin per day, then surveyed using a 5-point scale, and the average value was used.

5 points: very improved, 4 points: improved, 3 points: no improvement, 2 points: worsened, 1 point: very worsened

In addition, the acne improvement effect was tested on 20 test subjects with acne-prone skin, and the prepared cosmetic composition was applied to the skin in an amount of 2 mL per day, then surveyed using a 5-point scale and expressed as the average value.

5 points: very improved, 4 points: improved, 3 points: no improvement, 2 points: worsened, 1 point: very worsened}

<Table 1>

As shown in Table 1, it can be seen that the cosmetics prepared through Examples 1 to 3 of the present invention have superior skin moisturizing, skin wrinkle improvement, skin whitening and acne improvement effects compared to the cosmetics of Comparative Examples 1 and 2. .

In addition, the degree of slipperiness of the cosmetic compositions prepared through Examples 1 to 3 and Comparative Examples 1 to 2 was measured and shown in Table 2 below.

{However, the degree of slipperiness of the cosmetic composition was surveyed using a 3-point scale method for 50 test subjects and then expressed as an average value.

3 points: Very slippery, 2 points: Slightly slippery, 1 point: Not slippery}

<Table 2>

As shown in Table 2, it can be seen that the cosmetic compositions prepared through Examples 1 and 2 of the present invention have less slipperiness. In Example 3, it can be seen that the content of vegetable oil increases, making it relatively more slippery.

Therefore, the method for producing a cosmetic composition containing pine needle extract and marine seaweed according to the present invention improves physiological activities such as antioxidant, inflammation relief, and moisturizing, thereby providing effects such as skin moisturizing, skin wrinkle improvement, skin whitening, and acne improvement. It provides a cosmetic composition that is less slippery.

S101 ; Pine needle extract manufacturing steps
S103 ; Fermentation stage
S105 ; Raw material mixing stage

Claims (7)

A pine needle extract manufacturing step of producing pine needle extract using deep ocean water;
A fermentation step of inoculating and fermenting lactic acid bacteria into the pine needle extract prepared through the pine needle extract manufacturing step; and
It consists of a raw material mixing step of mixing 5 to 10 parts by weight of a skin improver and 1 to 3 parts by weight of vegetable oil with 100 parts by weight of the pine needle fermentation product prepared through the fermentation step,
The skin improving agent consists of one or more selected from the group consisting of brewer's yeast extract, field bean extract, and edelweiss extract,
A method for producing a cosmetic composition containing pine needle extract and deep sea water, wherein the vegetable oil consists of one or more selected from the group consisting of jojoba seed oil and parmesan oil.
In claim 1,
The pine needle extract manufacturing step is a cosmetic composition containing pine needle extract and deep ocean water, characterized in that it is achieved by mixing 800 to 1,000 parts by weight of deep sea water with 100 parts by weight of pine needle powder and heating at a temperature of 85 to 95 ° C. for 60 to 120 minutes. Manufacturing method.
In claim 1,
The fermentation step is a pine needle extract characterized by inoculating 0.01 to 0.1 parts by weight of lactic acid bacteria into 100 parts by weight of the pine needle extract prepared through the pine needle extract manufacturing step and then fermenting the pine needle extract at a temperature of 36 to 38° C. for 45 to 50 hours. and a method for producing a cosmetic composition containing deep sea water.
In claim 1 or 3,
Preparation of a cosmetic composition containing pine needle extract and deep sea water, wherein the lactic acid bacteria are one or more selected from the group consisting of Lactobacillus sakei, Lactobacillus plantarum, Lactobacillus brevis, and Pediococcus esidilactisi. method.
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