CN114848563A - Pore-shrinking composition and preparation method and application thereof - Google Patents
Pore-shrinking composition and preparation method and application thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention provides a pore-shrinking composition and a preparation method and application thereof. The prepared composition can adjust and balance the microecology of the skin of the face, adjust and balance the key flora of each part of the face, improve the whole skin condition, promote the skin metabolism, mildly strip old horny layer, also has the moisturizing effect, further balances the microecology of the skin, reduces the secretion of grease, promotes the regeneration of the horny layer and prevents photoaging to improve the problem of large pores.
Description
Technical Field
The invention relates to the field of skin care products and cosmetics, in particular to the technical field of A61K8/9789, and more particularly relates to a pore shrinking composition and a preparation method and application thereof.
Background
At present, the components for shrinking pores mainly comprise alcohols, acids, enzymes, plant extracts and the like, wherein the alcohols can inhibit oil secretion, the acids can inhibit hair follicle hyperkeratosis, the enzymes can decompose keratin, and tannic acid contained in the plant extracts has a certain convergence effect on skin. However, the cosmetic has a limited residence time on the skin, and only temporarily acts to constrict pores, and cannot completely solve the problem of large pores. Moreover, long-term use of products containing alcohol and small molecular acids can make the skin sensitive and irritate the skin. Some powder products containing oil and fat can temporarily cover pores, but after the pores are closed, anaerobic bacteria can start to propagate to cause inflammation and pox.
Compared with the female, the male has longer outdoor activity time, the skin is irradiated by ultraviolet rays for a longer time, skin photoaging can cause skin collagen loss, cells around pores are also shrunk due to the collagen loss, oil secretion is increased, and the pores are more and more obvious due to improper daily nursing of the male. Chinese patent CN107789308A discloses a mild oil-controlling acne-removing essence suitable for men, which contains effective components such as Hamamelis virginiana extract, lactobacillus/mung bean seed extract fermentation product filtrate, phellodendron amurense bark extract, peony root extract and the like, and can show the effects of balancing oil and shrinking pores. Chinese patent CN111568849B discloses a male oil control composition which contains active components such as pseudoalteromonas ferment product extract, witch hazel extract and carboxymethyl beta-dextran sodium and has the effects of controlling oil, preserving moisture and repairing.
The invention provides a pore-shrinking composition, a preparation method and application thereof, which can achieve the effects of controlling oil, shrinking pores, preventing aging and the like by adjusting the microecology of skin.
Disclosure of Invention
The invention provides a composition for shrinking pores, which comprises 5-13 parts of plant extract, 5-10 parts of plant fermentation product and 0.5-2 parts of chitin and derivatives thereof in parts by weight.
In a preferred embodiment, the plant extract is selected from at least one of hamamelis extract, salsola extract, mentha extract, aloe extract, seaweed extract (icnsargasum fusiformesh), horse chestnut extract.
In a preferred embodiment, the plant extract is a combination of Hamamelis extract and Epilobium extract.
In a preferred embodiment, the plant EXTRACTs are hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) and Salix furiosaefolia flower/leaf/stem EXTRACT. More preferably, the weight ratio of the hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) to the willowherb flower/leaf/stem EXTRACT is (1-3): (3-7).
In a preferred embodiment, the weight ratio of Hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) to Salix veitchii flower/leaf/stem EXTRACT is (2-3): (3-7). More preferably, the weight ratio of the Hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) to the willowherb flower/leaf/stem EXTRACT is 3: 7.
The salix leaf/stem extract is added into the composition, so that the facial skin micro-ecology can be regulated and balanced, the whole skin condition is improved, the symptoms such as large pores, skin inflammation and irritation are relieved by controlling staphylococcus capitis, corynebacterium coeruleum, propionibacterium avicularis and corynebacterium tuberculosa, the skin microorganism self-defense is promoted, the growth and the colonization of pathogenic bacteria are prevented by promoting staphylococcus epidermidis, staphylococcus hominis and micrococcus yunnanensis, the activity of 5 alpha-reductase is inhibited, the generation of sebum is effectively reduced, and the skin is helped to recover the healthy appearance. The Hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) rich in tannin is added, and the tannin has astringent property to solidify protoplasm of microorganism, has antibacterial effect, and can regulate sebum secretion, astringe pores, promote cutin regeneration, and improve pore size. In the experimental process, the applicant finds that when the mass ratio of the added witch hazel extract to the added flower/leaf/stem extract of salix flexuosa is 3:7, the skin condition can be further improved, the oil secretion can be reduced, and the pore size can be improved through the synergistic regulation and control effect of the two plant extracts.
In a preferred embodiment, the plant fermentation product is selected from at least one of rice fermentation product, malt fermentation product, pomegranate fermentation product, rhodiola fermentation product, rice bran fermentation product.
In a preferred embodiment, the fermentation bacteria of the plant fermentation product are selected from at least one of lactobacillus, bifidobacterium, lactobacillus rhamnosus, yeast and lactobacillus.
In a preferred embodiment, the plant fermentation product is a LACTOBACILLUS/rice fermentation product (lactuca/RICE FERMENT).
In a preferred embodiment, the chitin and its derivatives are acetyl chitosamines.
In a preferred embodiment, the mass ratio of LACTOBACILLUS/rice fermentation product (lactuca/RICE FERMENT) to chitosamine is (2-8): 1.
more preferably, the mass ratio of the LACTOBACILLUS/rice fermentation product (lactobasillus/RICE FERMENT) to the chitosamine is (2-4): 1.
most preferably, the LACTOBACILLUS/rice fermentation product (lactuca/RICE FERMENT) and the acetyl chitosamine are in a mass ratio of 4: 1.5.
The LACTOBACILLUS/rice fermentation product (Lactobacillus/RICE FERMENT) can gently exfoliate old horny layer and promote skin renewal, has excellent moisturizing effect, and can be used together with the flower/leaf/stem extract of Salix fusca to further help skin balance microecology, resist interference of foreign bacteria, promote growth of beneficial bacteria, and strengthen skin barrier. The acetyl chitosamine can be combined with lectin-like glycoprotein on the keratin to interfere the combination and adhesion of keratinocytes, thereby promoting normal exfoliation of aged stratum corneum, promoting skin metabolism, and refining pores. The acetyl chitosamine can also prevent photoaging, and reduce the activity of matrix metalloproteinase induced by ultraviolet radiation by inhibiting calcium-dependent signal channel, thereby inhibiting the degradation of collagen and extracellular matrix by metalloproteinase, and relieving skin relaxation. The applicant found in the experimental process that when the mass ratio of lactobacillus/rice fermentation product to the acetyl chitosamine added to the composition is 4:1.5, the skin metabolism can be further promoted, and the skin can be further balanced and microecological.
In a preferred embodiment, the composition further comprises an emollient, a polyol, a preservative, deionized water.
In a preferred embodiment, the composition further comprises 1.5-5 parts of an emollient, 5-10 parts of a polyol, 0.1-1 part of a preservative and deionized water to make up to 100 parts by weight.
More preferably, the composition further comprises 2 parts of an emollient, 8 parts of a polyol, 0.3 part of a preservative and deionized water, wherein the total weight is 100 parts.
In a preferred embodiment, the emollient is selected from at least one of squalane, squalene, PEG-6 caprylic/capric triglyceride, ethylhexyl palmitate, and myristyl myristate.
In a preferred embodiment, the emollient is squalane.
In a preferred embodiment, the polyol is selected from at least one of glycerol, propylene glycol, 1, 2-butanediol, 1, 3-butanediol, 1, 4-butanediol, methyl propylene glycol, polyglycerol ether polyol. More preferably, the polyalcohol is glycerol and 1, 2-butanediol, and the mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
In the present application, the kind of the preservative is not particularly limited, and the preservative may be selected from at least one of phenoxyethanol, paraben, sorbitol, hexylene glycol, caprylyl glycol, and cason.
In a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing emollient and polyalcohol uniformly, adding deionized water and antiseptic, adding plant extract, plant fermentation product, chitin and its derivatives, and mixing uniformly to obtain the composition.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Compared with the prior art, the invention has the following beneficial effects:
1. the composition prepared by the invention aims at solving the problems of much skin oil secretion, insufficient pore supporting and large pores caused by cell atrophy around the pores due to skin aging, and can improve the problem of large pores by reducing oil secretion, promoting cutin renewal and preventing photoaging.
2. The composition prepared by the invention can adjust and balance the microecology of the facial skin, adjust and balance key flora of each part of the face and improve the whole skin condition.
3. The composition prepared by the invention can promote skin metabolism, can gently strip old horny layers, also has a moisturizing effect, and further balances skin micro-ecology.
4. The composition prepared by the invention can be applied to cosmetics and skin care products with oil control and anti-aging effects, and particularly has obvious effects of controlling oil, keeping moisture, balancing skin micro-ecology and promoting skin metabolism for men's skin.
Detailed Description
Example 1
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 1 part of ottelia acuminata flower/leaf/stem extract, 4 parts of lactobacillus/rice fermentation product, 3 parts of witch hazel extract, 1 part of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 2
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 1 part of ottelia acuminata flower/leaf/stem extract, 6 parts of lactobacillus/rice fermentation product, 5 parts of witch hazel extract, 1.5 parts of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 3
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 1 part of a Fleckea frutescens flower/leaf/stem extract, 8 parts of a lactobacillus/rice fermentation product, 7 parts of a witch hazel extract, 2 parts of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 4
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 2 parts of a flower/leaf/stem extract of salix flexuosa, 4 parts of a lactobacillus/rice fermentation product, 5 parts of a witch hazel extract, 2 parts of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 5
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 2 parts of a flower/leaf/stem extract of salix formosana, 6 parts of a lactobacillus/rice fermentation product, 7 parts of a witch hazel extract, 1 part of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 6
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 2 parts of a flower/leaf/stem extract of salix flexuosa, 8 parts of a lactobacillus/rice fermentation product, 3 parts of a witch hazel extract, 1.5 parts of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 7
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 3 parts of a Fries willow flower/leaf/stem extract, 4 parts of a lactobacillus/rice fermentation product, 7 parts of a witch hazel extract, 1.5 parts of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flos Salicis Babylonicae/leaf/stem extract, radix Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 8
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 3 parts of a flower/leaf/stem extract of salix flexuosa, 6 parts of a lactobacillus/rice fermentation product, 3 parts of a witch hazel extract, 2 parts of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Example 9
The invention provides a composition for shrinking pores, which is prepared from the following raw materials, by weight, 3 parts of a flower/leaf/stem extract of salix flexuosa, 8 parts of a lactobacillus/rice fermentation product, 5 parts of a witch hazel extract, 1 part of acetyl chitosamine, a compound substance of 2 parts of squalane, 8 parts of glycerol and 1, 2-butanediol, 0.3 part of phenoxyethanol and deionized water, wherein the balance is 100 parts.
The extract of flowers/leaves/stems of Salix purpurea was purchased from Implemn vitamin (Shanghai) Co., Ltd under the name of
-SEBUM；
Lactobacillus/Rice fermentation product (Lactobacillus/RICE FERMENT) was purchased from Biotech Inc., of Tokyo, Wan, Chuang (Beijing);
hamamelis virginiana EXTRACT (HAMAMELIS VIRGINIANA EXTRACT) was purchased from Guangzhou ballad brocade chemical Co., Ltd;
acetochitosamine was purchased from Cipanochon sp.
The mass ratio of the glycerol to the 1, 2-butanediol is 1: 1.
in a second aspect, the present invention provides a method for preparing a composition for shrinking pores, comprising the following steps: mixing squalane, glycerol and 1, 2-butanediol, adding deionized water and phenoxyethanol, adding flower/leaf/stem extract of Salix purpurea, Hamamelis mollis extract, lactobacillus/rice fermentation product, and acetyl chitosamine, and mixing.
In a third aspect, the invention provides application of a pore-shrinking composition, wherein the pore-shrinking composition is applied to cosmetics and skin care products with oil control and anti-aging effects.
Performance testing
1. And (3) safety testing: the chick embryo chorioallantoic membrane was used for safety testing.
Eggs hatched to 9 days old are peeled off with tweezers from their air cell ends, the inner membrane is infiltrated with 0.9% physiological saline, the egg membrane is carefully peeled off from the edge, and the chorioallantoic membrane leaks out. 0.3mL of the composition of the example was taken with a pipette and dropped on the membrane, and after 3min, the change of blood vessels in the chorioallantoic membrane was observed. Each sample was tested in parallel 6 times, and 0.1mol/L NaOH was set as a positive control, and 0.9% NaCl by mass concentration was set as a negative control. The data are recorded in table 2.
Chick embryo scores were the average of the scores of single chick embryos in 6 experiments, where the single chick embryo score was the sum of the extent of bleeding, clotting and vascular thawing observed in each chick embryo, and the results retained the last two decimal places. Chick embryo scoring criteria are shown in Table 1.
TABLE 1
| Chick embryo scoring | Irritation property |
| ES≤12 | No/mild irritation |
| 12＜ES＜16 | Moderate irritation |
| ES≥16 | Strong irritation/corrosion |
TABLE 2
| Examples | Chick embryo scoring | Irritation property |
| 1 | 0.00 | Has no irritation |
| 2 | 0.00 | Has no irritation |
| 3 | 0.00 | Has no irritation |
| 4 | 0.00 | Has no irritation |
| 5 | 0.00 | Has no irritation |
| 6 | 1.00 | Has no irritation |
| 7 | 0.00 | Has no irritation |
| 8 | 0.00 | Has no irritation |
| 9 | 0.67 | Has no irritation |
| Negative control | 0.00 | Has no irritation |
| Positive control | 18.00 | Strong stimulation |
2. Pore shrinkage test:
screening 9 groups of healthy subjects with the age of 20-45 years, wherein skin pores are large, and each group has 20 subjects; after the subjects had used the cleansing product and sat still for more than 20 minutes between constant temperature and humidity, the subjects' facial condition was evaluated by the panelists and photographed using VISIA 7 and the skin condition before sample application was recorded. The product was then used under the direction of the experimenter, dispensing the sample and instructions for use, and the subject's facial condition was again assessed on days 14 and 28 of sample use and analyzed by photograph analysis with VISIA 7 to assess the pore-shrinking effect of the sample. The data are recorded in table 3. The blackhead removal effect was analyzed using a VISIA skin detector.
The calculation formula of the pore shrinking effect is as follows: a ═ a (A2-A1)/A1X 100%
Note: a is pore change rate,%;
a2 is the score of pores after use of the sample;
a1 is the score of the pore before using the sample;
TABLE 3
The pore-shrinking test results show that the composition prepared in example 7 has the best effect on pore shrinkage, and the pore score of the subject is reduced by 15.90% after the subject uses the composition for 28 days.
Claims (10)
1. The composition for shrinking pores is characterized by comprising 5-13 parts of plant extracts, 5-10 parts of plant fermentation products and 0.5-2 parts of chitin and derivatives thereof in parts by weight.
2. The pore-shrinking composition of claim 1, wherein the plant extract is selected from at least one of hamamelis extract, salsifera extract, mentha extract, aloe extract, seaweed extract, horse chestnut extract.
3. The pore-shrinking composition according to claim 2, wherein the plant extract is a complex of a hamamelis extract and a salsola extract.
4. The pore-shrinking composition according to claim 1, wherein the plant fermentation product is at least one selected from the group consisting of rice fermentation product, malt fermentation product, pomegranate fermentation product, rhodiola fermentation product, and rice bran fermentation product.
5. The composition for shrinking pores according to claim 4, wherein the fermentation bacteria of the plant fermentation product are at least one selected from the group consisting of lactobacillus, bifidobacterium, lactobacillus rhamnosus, yeast and lactobacillus.
6. The composition for shrinking pores according to claim 1, wherein said chitin and its derivatives are acetyl chitosamine.
7. The pore-shrinking composition of claim 1, wherein the mass ratio of the plant fermentation product to the chitin and the derivatives thereof is (2-8): 1.
8. the pore-shrinking composition according to any one of claims 1 to 7, further comprising an emollient, a polyol, a preservative, deionized water.
9. A method of preparing a pore-shrinking composition according to claim 8, comprising the steps of: mixing emollient and polyalcohol uniformly, adding deionized water and antiseptic, adding plant extract, plant fermentation product, chitin and its derivatives, and mixing uniformly to obtain the composition.
10. The use of the pore-shrinking composition according to claim 8, wherein the pore-shrinking composition is used in cosmetics and skin care products with oil-control and anti-aging effects.
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| CN108096107A (en) * | 2018-01-05 | 2018-06-01 | 佛山市汇汾化妆品科技有限公司 | A kind of pore refining composition |
| CN109431825A (en) * | 2018-12-18 | 2019-03-08 | 珠海水信生物科技有限公司 | A kind of collagen peptide is spraying |
| CN110917061A (en) * | 2019-12-26 | 2020-03-27 | 华熙生物科技股份有限公司 | Composition containing ergothioneine extracting solution, brown rice fermentation filtrate and acetyl chitosamine and application thereof |
| CN111053728A (en) * | 2020-01-15 | 2020-04-24 | 广州极男化妆品有限公司 | Composition for regulating water-oil balance of skin and cosmetic thereof |
| CN113143834A (en) * | 2021-05-24 | 2021-07-23 | 建昌帮药业有限公司 | Acne-removing skin-care composition and preparation method thereof |
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2021
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| CN108096107A (en) * | 2018-01-05 | 2018-06-01 | 佛山市汇汾化妆品科技有限公司 | A kind of pore refining composition |
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